Degradation mechanism of surface hydrophobicity by ferrous ions in the sulfidization flotation system of smithsonite
Metal ions commonly exist in the flotation pulp, which will affect the mineral surface properties and lead to a change in the mineral floatability. In this work, the effect of Fe2+ on the flotation behavior of smithsonite was investigated, and the interaction mechanism of Fe2+ with the smithsonite s...
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| Published in | Colloids and surfaces. A, Physicochemical and engineering aspects Vol. 648; p. 129119 |
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| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
05.09.2022
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| Subjects | |
| Online Access | Get full text |
| ISSN | 0927-7757 1873-4359 |
| DOI | 10.1016/j.colsurfa.2022.129119 |
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| Abstract | Metal ions commonly exist in the flotation pulp, which will affect the mineral surface properties and lead to a change in the mineral floatability. In this work, the effect of Fe2+ on the flotation behavior of smithsonite was investigated, and the interaction mechanism of Fe2+ with the smithsonite surface in the sulfidization flotation system was clarified. The results of microflotation tests showed that the presence of Fe2+ can greatly reduce the flotation recovery of smithsonite. The results of zeta-potential measurement, time-of-flight secondary-ion mass spectrometry, and X-ray photoelectron spectroscopy indicated that addition of Fe2+ before sulfidization generated FeOOH species and hindered formation of active sulfide species on smithsonite. The results of infrared spectroscopy and contact-angle measurement showed that addition of Fe2+ was harmful for adsorption of the collector on smithsonite, and it was difficult to obtain hydrophobic smithsonite surfaces in the Fe2+–sulfidization–xanthate flotation system. Considering the above results, the presence of Fe2+ depressed adsorption of sulfide ions and the collector on smithsonite, making smithsonite show poor floatability, and it was difficult to obtain the ideal flotation recovery of smithsonite.
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•Fe2+ an generate iron species with spatial depth on the smithsonite surface.•Addition of Fe2+ decreased the number of active sites on the smithsonite surface.•The content of sulfide on the smithsonite surface decreased after addition of Fe2+.•Adsorption of xanthate on the smithsonite surface was hindered by Fe2+. |
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| AbstractList | Metal ions commonly exist in the flotation pulp, which will affect the mineral surface properties and lead to a change in the mineral floatability. In this work, the effect of Fe²⁺ on the flotation behavior of smithsonite was investigated, and the interaction mechanism of Fe²⁺ with the smithsonite surface in the sulfidization flotation system was clarified. The results of microflotation tests showed that the presence of Fe²⁺ can greatly reduce the flotation recovery of smithsonite. The results of zeta-potential measurement, time-of-flight secondary-ion mass spectrometry, and X-ray photoelectron spectroscopy indicated that addition of Fe²⁺ before sulfidization generated FeOOH species and hindered formation of active sulfide species on smithsonite. The results of infrared spectroscopy and contact-angle measurement showed that addition of Fe²⁺ was harmful for adsorption of the collector on smithsonite, and it was difficult to obtain hydrophobic smithsonite surfaces in the Fe²⁺–sulfidization–xanthate flotation system. Considering the above results, the presence of Fe²⁺ depressed adsorption of sulfide ions and the collector on smithsonite, making smithsonite show poor floatability, and it was difficult to obtain the ideal flotation recovery of smithsonite. Metal ions commonly exist in the flotation pulp, which will affect the mineral surface properties and lead to a change in the mineral floatability. In this work, the effect of Fe2+ on the flotation behavior of smithsonite was investigated, and the interaction mechanism of Fe2+ with the smithsonite surface in the sulfidization flotation system was clarified. The results of microflotation tests showed that the presence of Fe2+ can greatly reduce the flotation recovery of smithsonite. The results of zeta-potential measurement, time-of-flight secondary-ion mass spectrometry, and X-ray photoelectron spectroscopy indicated that addition of Fe2+ before sulfidization generated FeOOH species and hindered formation of active sulfide species on smithsonite. The results of infrared spectroscopy and contact-angle measurement showed that addition of Fe2+ was harmful for adsorption of the collector on smithsonite, and it was difficult to obtain hydrophobic smithsonite surfaces in the Fe2+–sulfidization–xanthate flotation system. Considering the above results, the presence of Fe2+ depressed adsorption of sulfide ions and the collector on smithsonite, making smithsonite show poor floatability, and it was difficult to obtain the ideal flotation recovery of smithsonite. [Display omitted] •Fe2+ an generate iron species with spatial depth on the smithsonite surface.•Addition of Fe2+ decreased the number of active sites on the smithsonite surface.•The content of sulfide on the smithsonite surface decreased after addition of Fe2+.•Adsorption of xanthate on the smithsonite surface was hindered by Fe2+. |
| ArticleNumber | 129119 |
| Author | Zhang, Ga Han, Guang Feng, Qicheng Zhao, Wenjuan Zhao, Guanghu |
| Author_xml | – sequence: 1 givenname: Qicheng surname: Feng fullname: Feng, Qicheng organization: State Key Laboratory of Complex Nonferrous Metal Resources Clean Utilization, Faculty of Land Resource Engineering, Kunming University of Science and Technology, Kunming 650093, China – sequence: 2 givenname: Guanghu surname: Zhao fullname: Zhao, Guanghu organization: State Key Laboratory of Complex Nonferrous Metal Resources Clean Utilization, Faculty of Land Resource Engineering, Kunming University of Science and Technology, Kunming 650093, China – sequence: 3 givenname: Ga surname: Zhang fullname: Zhang, Ga organization: State Key Laboratory of Complex Nonferrous Metal Resources Clean Utilization, Faculty of Land Resource Engineering, Kunming University of Science and Technology, Kunming 650093, China – sequence: 4 givenname: Wenjuan surname: Zhao fullname: Zhao, Wenjuan email: zwjkust@126.com organization: State Key Laboratory of Complex Nonferrous Metal Resources Clean Utilization, Faculty of Land Resource Engineering, Kunming University of Science and Technology, Kunming 650093, China – sequence: 5 givenname: Guang surname: Han fullname: Han, Guang email: ghkmust@126.com organization: State Key Laboratory of Complex Nonferrous Metal Resources Clean Utilization, Faculty of Land Resource Engineering, Kunming University of Science and Technology, Kunming 650093, China |
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| Keywords | Smithsonite Surface hydrophobicity Sulfidization flotation Fe2+ species |
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| SubjectTerms | adsorption contact angle Fe2+ species hydrophobicity infrared spectroscopy mass spectrometry pulp Smithsonite sulfides Sulfidization flotation Surface hydrophobicity X-ray photoelectron spectroscopy zeta potential |
| Title | Degradation mechanism of surface hydrophobicity by ferrous ions in the sulfidization flotation system of smithsonite |
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