Fabrication of high proton conducting composite membranes from amino group functionalized MOF and semi-fluorinated sulfonated poly(arylene ether sulfone)s

[Display omitted] A series of polymer-metal–organic frameworks (MOF) hybrid composite membranes have been prepared with an amino group functionalized MOF (Cu-SAT) and phthalimidine-based aromatic fluorinated sulfonated poly(arylene ether sulfone)s (PAQSH-XX). The MOF was incorporated within the poly...

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Published inEuropean polymer journal Vol. 179; p. 111574
Main Authors Kamble, Riddhi, Ghorai, Arijit, Ghanti, Bholanath, Pradhan, Debabrata, Banerjee, Susanta
Format Journal Article
LanguageEnglish
Published Oxford Elsevier Ltd 05.10.2022
Elsevier BV
Subjects
Composite materials
Copolymers
Electron microscopy
Fluorination
Hybrid composites
Membranes
Metal-organic frameworks
Microscopy
MOF-Polymer hybrid composite
Polymers
Proton conductivity
Proton exchange membrane
Protons
SAXS analysis
Solution blending
Sulfonated poly(arylene ether sulfone)s
Sulfuric acid
Thermal analysis
X-ray scattering
Proton conductivity
MOF-Polymer hybrid composite
SAXS analysis
Sulfonated poly(arylene ether sulfone)s
Proton exchange membrane
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Abstract [Display omitted] A series of polymer-metal–organic frameworks (MOF) hybrid composite membranes have been prepared with an amino group functionalized MOF (Cu-SAT) and phthalimidine-based aromatic fluorinated sulfonated poly(arylene ether sulfone)s (PAQSH-XX). The MOF was incorporated within the polymer matrix by solution blending method and a series with membranes having 10 wt% of the MOF in PAQSH-XX of varied DS (degree of sulfonation) was prepared. The acid form of the membranes was successfully obtained by treating them with sulfuric acid. The properties of these hybrid membranes PAQSH-XX/ Cu-MOF (XX = 30 to 60) were studied and compared to that of the corresponding pristine PAQSH membranes. The copolymer and the hybrid membranes were characterized using FT-IR and thermal analysis. The membranes showed high solubility in all commonly used solvents. The uniform dispersion of the MOF within the polymer matrix was observed from scanning electron microscopy (SEM). Atomic force microscopy (AFM) images of the membranes showed well-separated phases which were confirmed by transmission electron microscopy (TEM) and small angle X-ray scattering (SAXS). The membranes also showed desirable improvements in the proton conductivities, water uptake, and swelling without affecting the oxidative stability values.
AbstractList [Display omitted] A series of polymer-metal–organic frameworks (MOF) hybrid composite membranes have been prepared with an amino group functionalized MOF (Cu-SAT) and phthalimidine-based aromatic fluorinated sulfonated poly(arylene ether sulfone)s (PAQSH-XX). The MOF was incorporated within the polymer matrix by solution blending method and a series with membranes having 10 wt% of the MOF in PAQSH-XX of varied DS (degree of sulfonation) was prepared. The acid form of the membranes was successfully obtained by treating them with sulfuric acid. The properties of these hybrid membranes PAQSH-XX/ Cu-MOF (XX = 30 to 60) were studied and compared to that of the corresponding pristine PAQSH membranes. The copolymer and the hybrid membranes were characterized using FT-IR and thermal analysis. The membranes showed high solubility in all commonly used solvents. The uniform dispersion of the MOF within the polymer matrix was observed from scanning electron microscopy (SEM). Atomic force microscopy (AFM) images of the membranes showed well-separated phases which were confirmed by transmission electron microscopy (TEM) and small angle X-ray scattering (SAXS). The membranes also showed desirable improvements in the proton conductivities, water uptake, and swelling without affecting the oxidative stability values.
A series of polymer-metal–organic frameworks (MOF) hybrid composite membranes have been prepared with an amino group functionalized MOF (Cu-SAT) and phthalimidine-based aromatic fluorinated sulfonated poly(arylene ether sulfone)s (PAQSH-XX). The MOF was incorporated within the polymer matrix by solution blending method and a series with membranes having 10 wt% of the MOF in PAQSH-XX of varied DS (degree of sulfonation) was prepared. The acid form of the membranes was successfully obtained by treating them with sulfuric acid. The properties of these hybrid membranes PAQSH-XX/ Cu-MOF (XX = 30 to 60) were studied and compared to that of the corresponding pristine PAQSH membranes. The copolymer and the hybrid membranes were characterized using FT-IR and thermal analysis. The membranes showed high solubility in all commonly used solvents. The uniform dispersion of the MOF within the polymer matrix was observed from scanning electron microscopy (SEM). Atomic force microscopy (AFM) images of the membranes showed well-separated phases which were confirmed by transmission electron microscopy (TEM) and small angle X-ray scattering (SAXS). The membranes also showed desirable improvements in the proton conductivities, water uptake, and swelling without affecting the oxidative stability values.
ArticleNumber 111574
Author Ghanti, Bholanath
Ghorai, Arijit
Banerjee, Susanta
Kamble, Riddhi
Pradhan, Debabrata
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CitedBy_id crossref_primary_10_1016_j_eurpolymj_2023_112641
crossref_primary_10_1016_j_ijhydene_2023_07_148
crossref_primary_10_1016_j_micromeso_2022_112314
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Keywords Proton conductivity
MOF-Polymer hybrid composite
SAXS analysis
Sulfonated poly(arylene ether sulfone)s
Proton exchange membrane
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Snippet [Display omitted] A series of polymer-metal–organic frameworks (MOF) hybrid composite membranes have been prepared with an amino group functionalized MOF...
A series of polymer-metal–organic frameworks (MOF) hybrid composite membranes have been prepared with an amino group functionalized MOF (Cu-SAT) and...
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SubjectTerms Composite materials
Copolymers
Electron microscopy
Fluorination
Hybrid composites
Membranes
Metal-organic frameworks
Microscopy
MOF-Polymer hybrid composite
Polymers
Proton conductivity
Proton exchange membrane
Protons
SAXS analysis
Solution blending
Sulfonated poly(arylene ether sulfone)s
Sulfuric acid
Thermal analysis
X-ray scattering
Title Fabrication of high proton conducting composite membranes from amino group functionalized MOF and semi-fluorinated sulfonated poly(arylene ether sulfone)s
URI https://dx.doi.org/10.1016/j.eurpolymj.2022.111574
https://www.proquest.com/docview/2731475164
Volume 179
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