Densification study of sodium zirconium phosphate-type ceramic for immobilizing radionuclides of Sr prepared with microwave sintering from uranium tailing sand
Strontium zirconium phosphate (SrZr 4 (PO 4 ) 6 ) ceramics has high density and chemical inertness, which can safely and effectively immobilize the divalent fission product Sr in the ceramic matrix. In this study, a novel SrZr 4 (PO 4 ) 6 ceramic was synthesized using microwave sintering of uranium...
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| Published in | Journal of radioanalytical and nuclear chemistry Vol. 333; no. 3; pp. 1275 - 1285 |
|---|---|
| Main Authors | , , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Cham
Springer International Publishing
01.03.2024
Springer Nature B.V |
| Subjects | |
| Online Access | Get full text |
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| Abstract | Strontium zirconium phosphate (SrZr
4
(PO
4
)
6
) ceramics has high density and chemical inertness, which can safely and effectively immobilize the divalent fission product Sr in the ceramic matrix. In this study, a novel SrZr
4
(PO
4
)
6
ceramic was synthesized using microwave sintering of uranium tailings. This method features shorter sintering times and efficient energy use. Sr replaces Na in sodium zirconium phosphate (NaZr
2
(PO
4
)
3
) due to similar ionic radii, transforming it into SrZr
4
(PO
4
)
6
ceramics. The results showed that the sintered samples prepared by holding at 1200 °C for 50 min, which the density of the solidified body reached up to 3.2 g/cm
3
.The ceramics showcase outstanding leach resistance, with Sr leaching rates far below the nuclear industry standard (1 × 10
−2
g m
−2
d
−1
). Similarly, the leaching rates for Na, Zr, P, and Si (10
–4
–10
–6
, 10
–6
–10
–8
, 10
–3
–10
–4
, and 10
–2
–10
−3
g m
−2
d
−1
) are significantly lower than industry standards. |
|---|---|
| AbstractList | Strontium zirconium phosphate (SrZr
4
(PO
4
)
6
) ceramics has high density and chemical inertness, which can safely and effectively immobilize the divalent fission product Sr in the ceramic matrix. In this study, a novel SrZr
4
(PO
4
)
6
ceramic was synthesized using microwave sintering of uranium tailings. This method features shorter sintering times and efficient energy use. Sr replaces Na in sodium zirconium phosphate (NaZr
2
(PO
4
)
3
) due to similar ionic radii, transforming it into SrZr
4
(PO
4
)
6
ceramics. The results showed that the sintered samples prepared by holding at 1200 °C for 50 min, which the density of the solidified body reached up to 3.2 g/cm
3
.The ceramics showcase outstanding leach resistance, with Sr leaching rates far below the nuclear industry standard (1 × 10
−2
g m
−2
d
−1
). Similarly, the leaching rates for Na, Zr, P, and Si (10
–4
–10
–6
, 10
–6
–10
–8
, 10
–3
–10
–4
, and 10
–2
–10
−3
g m
−2
d
−1
) are significantly lower than industry standards. Strontium zirconium phosphate (SrZr4(PO4)6) ceramics has high density and chemical inertness, which can safely and effectively immobilize the divalent fission product Sr in the ceramic matrix. In this study, a novel SrZr4(PO4)6 ceramic was synthesized using microwave sintering of uranium tailings. This method features shorter sintering times and efficient energy use. Sr replaces Na in sodium zirconium phosphate (NaZr2(PO4)3) due to similar ionic radii, transforming it into SrZr4(PO4)6 ceramics. The results showed that the sintered samples prepared by holding at 1200 °C for 50 min, which the density of the solidified body reached up to 3.2 g/cm3.The ceramics showcase outstanding leach resistance, with Sr leaching rates far below the nuclear industry standard (1 × 10−2 g m−2 d−1). Similarly, the leaching rates for Na, Zr, P, and Si (10–4–10–6, 10–6–10–8, 10–3–10–4, and 10–2–10−3 g m−2 d−1) are significantly lower than industry standards. |
| Author | Zhang, Tiejun Zhang, QiuCai Zhou, Tao Shi, Keyou Li, Jiawei Liu, Yong Yang, Yang Chen, Gaiyuan Xie, Yupeng Huang, Kun Mai, Yuzhen |
| Author_xml | – sequence: 1 givenname: Jiawei orcidid: 0009-0003-0952-8434 surname: Li fullname: Li, Jiawei organization: School of Resource Environment and Safety Engineering, University of South China – sequence: 2 givenname: Gaiyuan surname: Chen fullname: Chen, Gaiyuan organization: School of Resource Environment and Safety Engineering, University of South China – sequence: 3 givenname: QiuCai surname: Zhang fullname: Zhang, QiuCai email: zqiucai@163.com organization: School of Resource Environment and Safety Engineering, University of South China – sequence: 4 givenname: Keyou surname: Shi fullname: Shi, Keyou organization: School of Resource Environment and Safety Engineering, University of South China – sequence: 5 givenname: Tiejun surname: Zhang fullname: Zhang, Tiejun organization: School of Resource Environment and Safety Engineering, University of South China – sequence: 6 givenname: Yupeng surname: Xie fullname: Xie, Yupeng organization: School of Resource Environment and Safety Engineering, University of South China – sequence: 7 givenname: Yang surname: Yang fullname: Yang, Yang organization: School of Resource Environment and Safety Engineering, University of South China – sequence: 8 givenname: Tao surname: Zhou fullname: Zhou, Tao organization: School of Resource Environment and Safety Engineering, University of South China – sequence: 9 givenname: Kun surname: Huang fullname: Huang, Kun organization: School of Resource Environment and Safety Engineering, University of South China – sequence: 10 givenname: Yuzhen surname: Mai fullname: Mai, Yuzhen organization: School of Resource Environment and Safety Engineering, University of South China – sequence: 11 givenname: Yong surname: Liu fullname: Liu, Yong email: liuyong81668@163.com organization: School of Resource Environment and Safety Engineering, University of South China, College of Physics and Optoelectronic Engineering, Shenzhen University |
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| ContentType | Journal Article |
| Copyright | Akadémiai Kiadó, Budapest, Hungary 2024. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law. |
| Copyright_xml | – notice: Akadémiai Kiadó, Budapest, Hungary 2024. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law. |
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| Keywords | Immobilization Microwave sintering Sodium zirconium phosphate Uranium tailings |
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| Snippet | Strontium zirconium phosphate (SrZr
4
(PO
4
)
6
) ceramics has high density and chemical inertness, which can safely and effectively immobilize the divalent... Strontium zirconium phosphate (SrZr4(PO4)6) ceramics has high density and chemical inertness, which can safely and effectively immobilize the divalent fission... |
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| SubjectTerms | Ceramics Chemistry Chemistry and Materials Science Densification Density Diagnostic Radiology Energy consumption Fission products Hadrons Heavy Ions Industry standards Inorganic Chemistry Leaching Microwave sintering Nuclear Chemistry Nuclear Physics Physical Chemistry Radioisotopes Sodium Sodium zirconium phosphate Tailings Uranium |
| Title | Densification study of sodium zirconium phosphate-type ceramic for immobilizing radionuclides of Sr prepared with microwave sintering from uranium tailing sand |
| URI | https://link.springer.com/article/10.1007/s10967-024-09372-2 https://www.proquest.com/docview/2973435292/abstract/ |
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