Hydrothermal synthesis of Fe2O3 nanoparticles and their electrochemical application
In the present investigation, we report on Iron oxide (α-Fe 2 O 3 ) nanoparticles synthesized by simple hydrothermal method with different reaction times as 6 h (H1) and 8 h (H2) for supercapacitor application. The significance of varying the reaction time on structural, morphological, and vibration...
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Published in | Journal of materials science. Materials in electronics Vol. 35; no. 3; p. 230 |
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Main Authors | , , , , |
Format | Journal Article |
Language | English |
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2024
Springer Nature B.V |
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Abstract | In the present investigation, we report on Iron oxide (α-Fe
2
O
3
) nanoparticles synthesized by simple hydrothermal method with different reaction times as 6 h (H1) and 8 h (H2) for supercapacitor application. The significance of varying the reaction time on structural, morphological, and vibrational properties of α-Fe
2
O
3
was explored. XRD, FTIR, and Raman study affirmed that the products consist of only the rhombohedral phase of α-Fe
2
O
3
nanoparticles. SEM image infers that with a change in reaction time the surface morphology of α-Fe
2
O
3
changed from spherical to octahedra. The size of nanoparticles reduced with reaction time. XPS spectra again confirmed the growth of α-Fe
2
O
3
nanoparticles. The electrochemical characteristics of the fabricated H2 electrode exhibited excellent performance in a 2 M KOH electrolyte solution. The specific capacitance (Cs) achieved from CV and GCD curves were 299.4 F g
−1
, and 351.3 F g
−
1. The R
ct
acquired via electrochemical impedance (EIS) reduced from 11.2 to 9.18 Ω demonstrating the rise in the conductivity of the prepared electrodes. Remarkable capacitance retention of 92% was accomplished, even after 1000 cycles, thus making α-Fe
2
O
3
nanoparticles a most promising electrode for the fabrication of energy storage devices. |
---|---|
AbstractList | In the present investigation, we report on Iron oxide (α-Fe
2
O
3
) nanoparticles synthesized by simple hydrothermal method with different reaction times as 6 h (H1) and 8 h (H2) for supercapacitor application. The significance of varying the reaction time on structural, morphological, and vibrational properties of α-Fe
2
O
3
was explored. XRD, FTIR, and Raman study affirmed that the products consist of only the rhombohedral phase of α-Fe
2
O
3
nanoparticles. SEM image infers that with a change in reaction time the surface morphology of α-Fe
2
O
3
changed from spherical to octahedra. The size of nanoparticles reduced with reaction time. XPS spectra again confirmed the growth of α-Fe
2
O
3
nanoparticles. The electrochemical characteristics of the fabricated H2 electrode exhibited excellent performance in a 2 M KOH electrolyte solution. The specific capacitance (Cs) achieved from CV and GCD curves were 299.4 F g
−1
, and 351.3 F g
−
1. The R
ct
acquired via electrochemical impedance (EIS) reduced from 11.2 to 9.18 Ω demonstrating the rise in the conductivity of the prepared electrodes. Remarkable capacitance retention of 92% was accomplished, even after 1000 cycles, thus making α-Fe
2
O
3
nanoparticles a most promising electrode for the fabrication of energy storage devices. In the present investigation, we report on Iron oxide (α-Fe2O3) nanoparticles synthesized by simple hydrothermal method with different reaction times as 6 h (H1) and 8 h (H2) for supercapacitor application. The significance of varying the reaction time on structural, morphological, and vibrational properties of α-Fe2O3 was explored. XRD, FTIR, and Raman study affirmed that the products consist of only the rhombohedral phase of α-Fe2O3 nanoparticles. SEM image infers that with a change in reaction time the surface morphology of α-Fe2O3 changed from spherical to octahedra. The size of nanoparticles reduced with reaction time. XPS spectra again confirmed the growth of α-Fe2O3 nanoparticles. The electrochemical characteristics of the fabricated H2 electrode exhibited excellent performance in a 2 M KOH electrolyte solution. The specific capacitance (Cs) achieved from CV and GCD curves were 299.4 F g−1, and 351.3 F g−1. The Rct acquired via electrochemical impedance (EIS) reduced from 11.2 to 9.18 Ω demonstrating the rise in the conductivity of the prepared electrodes. Remarkable capacitance retention of 92% was accomplished, even after 1000 cycles, thus making α-Fe2O3 nanoparticles a most promising electrode for the fabrication of energy storage devices. |
ArticleNumber | 230 |
Author | Ravi, G. Usha, K. S. Vijaya Prasath, G. Selvamurugan, M. Vivekanandan, J. |
Author_xml | – sequence: 1 givenname: J. surname: Vivekanandan fullname: Vivekanandan, J. organization: Department of Physics, Bannari Amman Institute of Technology – sequence: 2 givenname: G. orcidid: 0000-0002-1940-1889 surname: Vijaya Prasath fullname: Vijaya Prasath, G. email: vijayprasath86@gmail.com organization: PG & Research, Department of Physics, Sree Sevugan Annamalai College – sequence: 3 givenname: M. surname: Selvamurugan fullname: Selvamurugan, M. organization: PG & Research, Department of Chemistry, Thiagarajar College – sequence: 4 givenname: K. S. surname: Usha fullname: Usha, K. S. organization: Department of Electronic Engineering, Gachon University, Gachon Advanced Institute of Semiconductor Technology, Gachon University – sequence: 5 givenname: G. surname: Ravi fullname: Ravi, G. organization: Department of Physics, Alagappa University |
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Snippet | In the present investigation, we report on Iron oxide (α-Fe
2
O
3
) nanoparticles synthesized by simple hydrothermal method with different reaction times as... In the present investigation, we report on Iron oxide (α-Fe2O3) nanoparticles synthesized by simple hydrothermal method with different reaction times as 6 h... |
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SubjectTerms | Capacitance Characterization and Evaluation of Materials Chemistry and Materials Science Electrodes Energy storage Ferric oxide Iron oxides Materials Science Morphology Nanoparticles Optical and Electronic Materials Reaction time |
Title | Hydrothermal synthesis of Fe2O3 nanoparticles and their electrochemical application |
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