Alkylresorcinols of rye (Secale cereale L.) caryopses. IV. Three-step preparation of 5-n-alkylresorcinols

Whole rye or wheat grains were extracted with acetone at room temperature. The extracts were pooled and acetone was evaporated. The remaining acetone oil was washed out with n-pentane until a colourless filtrate was obtained. The residue was dried, then dissolved in chloroform-acetone (95:5) mixture...

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Published inActa Societatis Botanicorum Poloniae Vol. 47; no. 4; pp. 379 - 389
Main Authors Mejbaum-Katzenellenbogen, W, Tluscik, F, Kozubek, A
Format Journal Article
LanguageEnglish
Published Warsaw Polish Botanical Society 1978
Subjects
Acetone
Chloroform
Chromatography
Column chromatography
field crops
n-Hexane
Pentane
plant biochemistry
plant physiology
Resorcinol
Silica
Silica gel
Thin-layer chromatography
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Abstract Whole rye or wheat grains were extracted with acetone at room temperature. The extracts were pooled and acetone was evaporated. The remaining acetone oil was washed out with n-pentane until a colourless filtrate was obtained. The residue was dried, then dissolved in chloroform-acetone (95:5) mixture and separated by column chromatography on silica gel. The fractions containing 5-n-alkylresorcinols were pooled, condensed and crystallised from n-hexane. The preparation obtained was homogeneous in thin-layer chromatography and gave the UV spectrum characteristic for 5-n-alkyl derivatives of resorcinol.
AbstractList Whole rye or wheat grains were extracted with acetone at room temperature. The extracts were pooled and acetone was evaporated. The remaining acetone oil was washed out with n-pentane until a colourless filtrate was obtained. The residue was dried, then dissolved in chloroform-acetone (95:5) mixture and separated by column chromatography on silica gel. The fractions containing 5-n-alkylresorcinols were pooled, condensed and crystallised from n-hexane. The preparation obtained was homogeneous in thin-layer chromatography and gave the UV spectrum characteristic for 5-n-alkyl derivatives of resorcinol.
Author Kozubek, A
Tluscik, F
Mejbaum-Katzenellenbogen, W
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CitedBy_id crossref_primary_10_1080_10575639508043199
crossref_primary_10_1021_cr970464o
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ContentType Journal Article
Copyright Copyright (c) 2015 W. Mejbaum-Katzenellenbogen, F. Tłuścik, A. Kozubek. This work is licensed under the Creative Commons Attribution License http://creativecommons.org/licenses/by/3.0 (the “License”). Notwithstanding the ProQuest Terms and conditions, you may use this content in accordance with the terms of the License.
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SubjectTerms Acetone
Chloroform
Chromatography
Column chromatography
field crops
n-Hexane
Pentane
plant biochemistry
plant physiology
Resorcinol
Silica
Silica gel
Thin-layer chromatography
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Title Alkylresorcinols of rye (Secale cereale L.) caryopses. IV. Three-step preparation of 5-n-alkylresorcinols
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