The effect of hydroxide ions on the electrocatalysis of glucose at single platinum nanoparticles
Glucose oxidation on platinum nanoparticles (Pt NPs) at varying potentials (from − 0.7 V to 0.2 V) was investigated using single entity electrochemistry. The active chemisorption model was found to be valid only at potentials below − 0.6 V, while the incipient hydrous oxide/adatom mediator (IHOAM) m...
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| Published in | Journal of applied electrochemistry Vol. 53; no. 10; pp. 1991 - 1999 |
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| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
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01.10.2023
Springer Nature B.V |
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| Abstract | Glucose oxidation on platinum nanoparticles (Pt NPs) at varying potentials (from − 0.7 V to 0.2 V) was investigated using single entity electrochemistry. The active chemisorption model was found to be valid only at potentials below − 0.6 V, while the incipient hydrous oxide/adatom mediator (IHOAM) model was confirmed for potentials above − 0.6 V. In both cases, hydrous ions significantly improved glucose oxidation by freeing up active sites on the Pt NPs. The potential for glucose sensing at − 0.4 V, where continuous glucose oxidation took place, was assessed. Although the linearity was limited (0.1–0.6 mM), the high sensitivity of 423.056 µA mM
− 1
cm
− 2
and limit of detection (LOD) of 25.63 µM demonstrated promising prospects for glucose sensing at − 0.4 V, particularly for samples with low glucose concentrations.
Graphical abstract |
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| AbstractList | Glucose oxidation on platinum nanoparticles (Pt NPs) at varying potentials (from − 0.7 V to 0.2 V) was investigated using single entity electrochemistry. The active chemisorption model was found to be valid only at potentials below − 0.6 V, while the incipient hydrous oxide/adatom mediator (IHOAM) model was confirmed for potentials above − 0.6 V. In both cases, hydrous ions significantly improved glucose oxidation by freeing up active sites on the Pt NPs. The potential for glucose sensing at − 0.4 V, where continuous glucose oxidation took place, was assessed. Although the linearity was limited (0.1–0.6 mM), the high sensitivity of 423.056 µA mM− 1 cm− 2 and limit of detection (LOD) of 25.63 µM demonstrated promising prospects for glucose sensing at − 0.4 V, particularly for samples with low glucose concentrations. Glucose oxidation on platinum nanoparticles (Pt NPs) at varying potentials (from − 0.7 V to 0.2 V) was investigated using single entity electrochemistry. The active chemisorption model was found to be valid only at potentials below − 0.6 V, while the incipient hydrous oxide/adatom mediator (IHOAM) model was confirmed for potentials above − 0.6 V. In both cases, hydrous ions significantly improved glucose oxidation by freeing up active sites on the Pt NPs. The potential for glucose sensing at − 0.4 V, where continuous glucose oxidation took place, was assessed. Although the linearity was limited (0.1–0.6 mM), the high sensitivity of 423.056 µA mM − 1 cm − 2 and limit of detection (LOD) of 25.63 µM demonstrated promising prospects for glucose sensing at − 0.4 V, particularly for samples with low glucose concentrations. Graphical abstract |
| Author | Zhang, Dong Lin, Jun Li, Shuang Zhao, Wenbin Zang, Yue Wang, Jun Xin, Qing |
| Author_xml | – sequence: 1 givenname: Jun surname: Lin fullname: Lin, Jun email: junlin@hdu.edu.cn organization: Institute of Carbon Neutrality and New Energy, School of Electronics and Information, Hangzhou Dianzi University – sequence: 2 givenname: Jun surname: Wang fullname: Wang, Jun organization: Institute of Carbon Neutrality and New Energy, School of Electronics and Information, Hangzhou Dianzi University – sequence: 3 givenname: Shuang surname: Li fullname: Li, Shuang organization: Zhejiang Energy Technology Co., Ltd – sequence: 4 givenname: Wenbin surname: Zhao fullname: Zhao, Wenbin organization: Institute of Carbon Neutrality and New Energy, School of Electronics and Information, Hangzhou Dianzi University – sequence: 5 givenname: Dong surname: Zhang fullname: Zhang, Dong organization: College of Materials and Environmental Engineering, Hangzhou Dianzi University – sequence: 6 givenname: Yue surname: Zang fullname: Zang, Yue organization: Institute of Carbon Neutrality and New Energy, School of Electronics and Information, Hangzhou Dianzi University – sequence: 7 givenname: Qing surname: Xin fullname: Xin, Qing organization: Institute of Carbon Neutrality and New Energy, School of Electronics and Information, Hangzhou Dianzi University |
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| Snippet | Glucose oxidation on platinum nanoparticles (Pt NPs) at varying potentials (from − 0.7 V to 0.2 V) was investigated using single entity electrochemistry. The... Glucose oxidation on platinum nanoparticles (Pt NPs) at varying potentials (from − 0.7 V to 0.2 V) was investigated using single entity electrochemistry. The... |
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| SubjectTerms | Chemisorption Chemistry Chemistry and Materials Science Electrochemistry Glucose Industrial Chemistry/Chemical Engineering Nanoparticles Oxidation Physical Chemistry Platinum Research Article |
| Title | The effect of hydroxide ions on the electrocatalysis of glucose at single platinum nanoparticles |
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