Directional Reconstruction of Iron Oxides to Active Sites for Superior Water Oxidation
Rationally constructing and manipulating the in situ formed catalytically active surface of catalysts remains a tremendous challenge for a highly efficient water electrolysis. Herein, an anion and cation co‐induced strategy is presented to modulate in situ catalyst dissolution‐redeposition and to ac...
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| Published in | Advanced functional materials Vol. 33; no. 43 |
|---|---|
| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
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18.10.2023
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| Abstract | Rationally constructing and manipulating the in situ formed catalytically active surface of catalysts remains a tremendous challenge for a highly efficient water electrolysis. Herein, an anion and cation co‐induced strategy is presented to modulate in situ catalyst dissolution‐redeposition and to achieve the directional reconstruction of Zn and S co‐doped Fe
2
O
3
and Fe
3
O
4
on iron foams (Zn,S‐Fe
2
O
3
‐Fe
3
O
4
/IF), for oxygen evolution reaction (OER). Benefiting from Zn, S co‐doping and the presence of Fe
3
O
4
, a directionally reconstructed surface is obtained. The Fe
2
O
3
in the Zn,S‐Fe
2
O
3
‐Fe
3
O
4
/IF is directionally reconstructed into FeOOH (Zn,S‐Fe
3
O
4
‐FeOOH/IF), in which the S leaching promotes the Fe dissolution and the Zn co‐deposition regulates the activity of the obtained FeOOH. Moreover, the presence of Fe
3
O
4
provides a stable site for FeOOH deposition, and thus causes more FeOOH active components to be formed. Directionally reconstructed Zn,S‐Fe
3
O
4
‐FeOOH/IF outperformes many state‐of‐the‐art OER catalysts and demonstrates a remarkable stability. The experimental and density functional theory (DFT) calculation results show that the introduction of Zn‐doped FeOOH with abundant oxygen vacancies through directional reconstruction has activated lattice O atoms, facilitating the OER process on the heterojunction surface following the lattice oxygen mechanism (LOM) pathway. This work makes a stride in co‐induced strategy modulating directional reconstruction. |
|---|---|
| AbstractList | Rationally constructing and manipulating the in situ formed catalytically active surface of catalysts remains a tremendous challenge for a highly efficient water electrolysis. Herein, an anion and cation co‐induced strategy is presented to modulate in situ catalyst dissolution‐redeposition and to achieve the directional reconstruction of Zn and S co‐doped Fe
2
O
3
and Fe
3
O
4
on iron foams (Zn,S‐Fe
2
O
3
‐Fe
3
O
4
/IF), for oxygen evolution reaction (OER). Benefiting from Zn, S co‐doping and the presence of Fe
3
O
4
, a directionally reconstructed surface is obtained. The Fe
2
O
3
in the Zn,S‐Fe
2
O
3
‐Fe
3
O
4
/IF is directionally reconstructed into FeOOH (Zn,S‐Fe
3
O
4
‐FeOOH/IF), in which the S leaching promotes the Fe dissolution and the Zn co‐deposition regulates the activity of the obtained FeOOH. Moreover, the presence of Fe
3
O
4
provides a stable site for FeOOH deposition, and thus causes more FeOOH active components to be formed. Directionally reconstructed Zn,S‐Fe
3
O
4
‐FeOOH/IF outperformes many state‐of‐the‐art OER catalysts and demonstrates a remarkable stability. The experimental and density functional theory (DFT) calculation results show that the introduction of Zn‐doped FeOOH with abundant oxygen vacancies through directional reconstruction has activated lattice O atoms, facilitating the OER process on the heterojunction surface following the lattice oxygen mechanism (LOM) pathway. This work makes a stride in co‐induced strategy modulating directional reconstruction. Rationally constructing and manipulating the in situ formed catalytically active surface of catalysts remains a tremendous challenge for a highly efficient water electrolysis. Herein, an anion and cation co‐induced strategy is presented to modulate in situ catalyst dissolution‐redeposition and to achieve the directional reconstruction of Zn and S co‐doped Fe2O3 and Fe3O4 on iron foams (Zn,S‐Fe2O3‐Fe3O4/IF), for oxygen evolution reaction (OER). Benefiting from Zn, S co‐doping and the presence of Fe3O4, a directionally reconstructed surface is obtained. The Fe2O3 in the Zn,S‐Fe2O3‐Fe3O4/IF is directionally reconstructed into FeOOH (Zn,S‐Fe3O4‐FeOOH/IF), in which the S leaching promotes the Fe dissolution and the Zn co‐deposition regulates the activity of the obtained FeOOH. Moreover, the presence of Fe3O4 provides a stable site for FeOOH deposition, and thus causes more FeOOH active components to be formed. Directionally reconstructed Zn,S‐Fe3O4‐FeOOH/IF outperformes many state‐of‐the‐art OER catalysts and demonstrates a remarkable stability. The experimental and density functional theory (DFT) calculation results show that the introduction of Zn‐doped FeOOH with abundant oxygen vacancies through directional reconstruction has activated lattice O atoms, facilitating the OER process on the heterojunction surface following the lattice oxygen mechanism (LOM) pathway. This work makes a stride in co‐induced strategy modulating directional reconstruction. |
| Author | Liu, Hai‐Jun Zhang, Shuo Dong, Bin Yang, Wen‐Yu Yu, Ning Chai, Yong‐Ming Liu, Chun‐Ying |
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| SubjectTerms | Catalysts Density functional theory Deposition Dissolution Electrolysis Ferric hydroxide Ferric oxide Heterojunctions In situ leaching Iron oxides Lattice vacancies Leaching Materials science Metal foams Oxidation Oxygen evolution reactions Reconstruction Zinc |
| Title | Directional Reconstruction of Iron Oxides to Active Sites for Superior Water Oxidation |
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