High p-xylene selectivity in aluminum-based metal–organic framework with 1-D channels
[Display omitted] •MIL-120(Al) showed high pX selectivity superior to reported values in MOFs and zeolites.•MIL-120(Al) exhibited good cyclic adsorption properties and excellent stabilities.•A dynamic simulation showed a potential of pX separation using a SMB with MIL-120(Al).•High pX selectivity ca...
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| Published in | Journal of industrial and engineering chemistry (Seoul, Korea) Vol. 117; pp. 333 - 341 |
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| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
25.01.2023
한국공업화학회 |
| Subjects | |
| Online Access | Get full text |
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| Abstract | [Display omitted]
•MIL-120(Al) showed high pX selectivity superior to reported values in MOFs and zeolites.•MIL-120(Al) exhibited good cyclic adsorption properties and excellent stabilities.•A dynamic simulation showed a potential of pX separation using a SMB with MIL-120(Al).•High pX selectivity can be attained within 1-D channels of approximately 7 Å.
The separation of highly pure p-xylene (pX) from xylene isomers is an industrially important and challenging issue. Although simulated moving bed (SMB) processes using faujasite zeolites are currently used for pX separation, developing novel adsorbents with improved pX separation performances is strongly needed. In this study, an aluminum-based metal–organic framework (MOF), MIL-120(Al) with 1-D channels of approximately 7 Å, exhibited considerably high pX selectivities compared to xylene isomers (αpX/oX: ∼31; αpX/mX: ∼17; αpX/EB: ∼7.5; αpX/OME: ∼11), which are superior to reported values for other MOFs and zeolites under similar conditions. Such high selectivities may originate from the proper pore shape and size of MIL-120(Al). MIL-120(Al) also showed good cyclic adsorption properties as well as superior hydrothermal and chemical stabilities. Finally, a dynamic simulation showed that MIL-120(Al) could achieve approximately complete separation of pX from a xylene isomer mixture using an SMB process. |
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| AbstractList | [Display omitted]
•MIL-120(Al) showed high pX selectivity superior to reported values in MOFs and zeolites.•MIL-120(Al) exhibited good cyclic adsorption properties and excellent stabilities.•A dynamic simulation showed a potential of pX separation using a SMB with MIL-120(Al).•High pX selectivity can be attained within 1-D channels of approximately 7 Å.
The separation of highly pure p-xylene (pX) from xylene isomers is an industrially important and challenging issue. Although simulated moving bed (SMB) processes using faujasite zeolites are currently used for pX separation, developing novel adsorbents with improved pX separation performances is strongly needed. In this study, an aluminum-based metal–organic framework (MOF), MIL-120(Al) with 1-D channels of approximately 7 Å, exhibited considerably high pX selectivities compared to xylene isomers (αpX/oX: ∼31; αpX/mX: ∼17; αpX/EB: ∼7.5; αpX/OME: ∼11), which are superior to reported values for other MOFs and zeolites under similar conditions. Such high selectivities may originate from the proper pore shape and size of MIL-120(Al). MIL-120(Al) also showed good cyclic adsorption properties as well as superior hydrothermal and chemical stabilities. Finally, a dynamic simulation showed that MIL-120(Al) could achieve approximately complete separation of pX from a xylene isomer mixture using an SMB process. The separation of highly pure p-xylene (pX) from xylene isomers is an industrially important and challengingissue. Although simulated moving bed (SMB) processes using faujasite zeolites are currently usedfor pX separation, developing novel adsorbents with improved pX separation performances is stronglyneeded. In this study, an aluminum-based metal–organic framework (MOF), MIL-120(Al) with 1-D channelsof approximately 7 Å, exhibited considerably high pX selectivities compared to xylene isomers(apX/oX: 31; apX/mX: 17; apX/EB: 7.5; apX/OME: 11), which are superior to reported values for otherMOFs and zeolites under similar conditions. Such high selectivities may originate from the proper poreshape and size of MIL-120(Al). MIL-120(Al) also showed good cyclic adsorption properties as well assuperior hydrothermal and chemical stabilities. Finally, a dynamic simulation showed that MIL-120(Al)could achieve approximately complete separation of pX from a xylene isomer mixture using an SMBprocess. KCI Citation Count: 0 |
| Author | Bae, Youn-Sang Bae, Hyun Jin Choi, Yujin Kim, Kyung-Min Kim, Seung-Ik |
| Author_xml | – sequence: 1 givenname: Hyun Jin surname: Bae fullname: Bae, Hyun Jin organization: Department of Chemical and Biomolecular Engineering, Yonsei University, Seoul 03722, South Korea – sequence: 2 givenname: Seung-Ik surname: Kim fullname: Kim, Seung-Ik organization: Environmental and Sustainable Resources Research Center, Korea Research Institute of Chemical Technology (KRICT), Daejeon 34114, South Korea – sequence: 3 givenname: Yujin surname: Choi fullname: Choi, Yujin organization: Department of Chemical and Biomolecular Engineering, Yonsei University, Seoul 03722, South Korea – sequence: 4 givenname: Kyung-Min surname: Kim fullname: Kim, Kyung-Min email: kmkim@gwnu.ac.kr organization: Department of Biochemical Engineering, Gangneung-Wonju National University, Gangneung-si, Gangwon-do, South Korea – sequence: 5 givenname: Youn-Sang surname: Bae fullname: Bae, Youn-Sang email: mowbae@yonsei.ac.kr organization: Department of Chemical and Biomolecular Engineering, Yonsei University, Seoul 03722, South Korea |
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| Keywords | Xylene isomer separation Adsorption Simulated moving bed (SMB) Metal-organic framework (MOF) p-Xylene (pX) |
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•MIL-120(Al) showed high pX selectivity superior to reported values in MOFs and zeolites.•MIL-120(Al) exhibited good cyclic adsorption... The separation of highly pure p-xylene (pX) from xylene isomers is an industrially important and challengingissue. Although simulated moving bed (SMB)... |
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| SubjectTerms | Adsorption Metal-organic framework (MOF) p-Xylene (pX) Simulated moving bed (SMB) Xylene isomer separation 화학공학 |
| Title | High p-xylene selectivity in aluminum-based metal–organic framework with 1-D channels |
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