Effects of ultrasonic impregnation combined with calcination in N2 atmosphere on the property of Co3O4/CeO2 composites for catalytic methane combustion
Co3O4/CeO2 composites with high surface areas and ultrafine crystalline sizes for catalytic combustion of methane were firstly prepared by a new sol-gel method which combined ultrasonic impregnation treatment and calcination in N2 atmosphere. The samples were characterized by various means such as n...
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Published in | Journal of energy chemistry Vol. 25; no. 3; pp. 387 - 392 |
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Main Authors | , , , , , |
Format | Journal Article |
Language | English |
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Elsevier B.V
01.05.2016
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Abstract | Co3O4/CeO2 composites with high surface areas and ultrafine crystalline sizes for catalytic combustion of methane were firstly prepared by a new sol-gel method which combined ultrasonic impregnation treatment and calcination in N2 atmosphere. The samples were characterized by various means such as nitrogen adsorption/desorption, X-ray diffraction(XRD), H2 temperature-programmed reduction(H2-TPR),X-ray photoelectron spectroscopy(XPS) and transmission electron microscopy(TEM). Results showed that the modified catalyst had the mesoporous structure, comparatively higher amount of surface oxygen and larger oxygen vacancies than others. As a result of the structure and surface composition merits, a high methane combustion conversion(50%) could be obtained at a low temperature of 262 °C for the modified Co3O4/CeO2 composites catalysts. The experimental results demonstrated that ultrasonic impregnation treatment combined with the N2 thermal treatment prior to calcination in air had a promising application for preparation of Co3O4/CeO2 composites catalysts for low-temperature catalytic combustion of methane. |
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AbstractList | Co3O4/CeO2 composites with high surface areas and ultrafine crystalline sizes for catalytic combustion of methane were firstly prepared by a new sol-gel method which combined ultrasonic impregnation treatment and calcination in N2 atmosphere. The samples were characterized by various means such as nitrogen adsorption/desorption, X-ray diffraction(XRD), H2 temperature-programmed reduction(H2-TPR),X-ray photoelectron spectroscopy(XPS) and transmission electron microscopy(TEM). Results showed that the modified catalyst had the mesoporous structure, comparatively higher amount of surface oxygen and larger oxygen vacancies than others. As a result of the structure and surface composition merits, a high methane combustion conversion(50%) could be obtained at a low temperature of 262 °C for the modified Co3O4/CeO2 composites catalysts. The experimental results demonstrated that ultrasonic impregnation treatment combined with the N2 thermal treatment prior to calcination in air had a promising application for preparation of Co3O4/CeO2 composites catalysts for low-temperature catalytic combustion of methane. Co3O4/CeO2 composites with high surface areas and ultrafine crystalline sizes for catalytic combustion of methane were firstly prepared by a new sol-gel method which combined ultrasonic impregnation treatment and calcination in N2 atmosphere. The samples were characterized by various means such as nitrogen adsorption/desorption, X-ray diffraction (XRD), H2 temperature-programmed reduction (H2-TPR), X-ray photoelectron spectroscopy (XPS) and transmission electron microscopy (TEM). Results showed that the modified catalyst had the mesoporous structure, comparatively higher amount of surface oxygen and larger oxygen vacancies than others. As a result of the structure and surface composition merits, a high methane combustion conversion (50%) could be obtained at a low temperature of 262°C for the modified Co3O4/CeO2 composites catalysts. The experimental results demonstrated that ultrasonic impregnation treatment combined with the N2 thermal treatment prior to calcination in air had a promising application for preparation of Co3O4/CeO2 composites catalysts for low-temperature catalytic combustion of methane. Ultrasonic impregnation can promote the organic reactions and suppresses the formation of active substance soft agglomerates. The superior Co3O4/CeO2 composites can be obtained due to the synergistic effect in the course of processing. [Display omitted] |
Author | Hong Lu Chengfa Jiang Zhenwu Ding Wei Wang Wei Chu Yanyan Feng |
AuthorAffiliation | Department of Chemical Engineering, Sichuan University;Sichuan Provincial Engineering Technology Center for Environmental Protection Catalytic Materials |
Author_xml | – sequence: 1 givenname: Hong surname: Lu fullname: Lu, Hong organization: Department of Chemical Engineering, Sichuan University, Chengdu 610065, Sichuan, China – sequence: 2 givenname: Chengfa surname: Jiang fullname: Jiang, Chengfa email: jiangcf@scu.edu.cn organization: Department of Chemical Engineering, Sichuan University, Chengdu 610065, Sichuan, China – sequence: 3 givenname: Zhenwu surname: Ding fullname: Ding, Zhenwu organization: Department of Chemical Engineering, Sichuan University, Chengdu 610065, Sichuan, China – sequence: 4 givenname: Wei surname: Wang fullname: Wang, Wei organization: Department of Chemical Engineering, Sichuan University, Chengdu 610065, Sichuan, China – sequence: 5 givenname: Wei surname: Chu fullname: Chu, Wei email: chuwei1965@foxmail.com organization: Department of Chemical Engineering, Sichuan University, Chengdu 610065, Sichuan, China – sequence: 6 givenname: Yanyan surname: Feng fullname: Feng, Yanyan organization: Department of Chemical Engineering, Sichuan University, Chengdu 610065, Sichuan, China |
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Keywords | Catalytic combustion Sol-gel method Ultrasonic N2 calcination Co3O4/CeO2 |
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Notes | Hong Lu;Chengfa Jiang;Zhenwu Ding;Wei Wang;Wei Chu;Yanyan Feng;Department of Chemical Engineering, Sichuan University;Sichuan Provincial Engineering Technology Center for Environmental Protection Catalytic Materials 21-1585/O4 |
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Snippet | Co3O4/CeO2 composites with high surface areas and ultrafine crystalline sizes for catalytic combustion of methane were firstly prepared by a new sol-gel method... |
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SubjectTerms | Catalytic combustion Co3O4/CeO2 N2 calcination Sol-gel method Ultrasonic |
Title | Effects of ultrasonic impregnation combined with calcination in N2 atmosphere on the property of Co3O4/CeO2 composites for catalytic methane combustion |
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