Effects of ultrasonic impregnation combined with calcination in N2 atmosphere on the property of Co3O4/CeO2 composites for catalytic methane combustion
Co3O4/CeO2 composites with high surface areas and ultrafine crystalline sizes for catalytic combustion of methane were firstly prepared by a new sol-gel method which combined ultrasonic impregnation treatment and calcination in N2 atmosphere. The samples were characterized by various means such as n...
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| Published in | Journal of energy chemistry Vol. 25; no. 3; pp. 387 - 392 |
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| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
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Elsevier B.V
01.05.2016
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| Subjects | |
| Online Access | Get full text |
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| Abstract | Co3O4/CeO2 composites with high surface areas and ultrafine crystalline sizes for catalytic combustion of methane were firstly prepared by a new sol-gel method which combined ultrasonic impregnation treatment and calcination in N2 atmosphere. The samples were characterized by various means such as nitrogen adsorption/desorption, X-ray diffraction（XRD）, H2 temperature-programmed reduction（H2-TPR）,X-ray photoelectron spectroscopy（XPS） and transmission electron microscopy（TEM）. Results showed that the modified catalyst had the mesoporous structure, comparatively higher amount of surface oxygen and larger oxygen vacancies than others. As a result of the structure and surface composition merits, a high methane combustion conversion（50%） could be obtained at a low temperature of 262 °C for the modified Co3O4/CeO2 composites catalysts. The experimental results demonstrated that ultrasonic impregnation treatment combined with the N2 thermal treatment prior to calcination in air had a promising application for preparation of Co3O4/CeO2 composites catalysts for low-temperature catalytic combustion of methane. |
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| AbstractList | Co3O4/CeO2 composites with high surface areas and ultrafine crystalline sizes for catalytic combustion of methane were firstly prepared by a new sol-gel method which combined ultrasonic impregnation treatment and calcination in N2 atmosphere. The samples were characterized by various means such as nitrogen adsorption/desorption, X-ray diffraction（XRD）, H2 temperature-programmed reduction（H2-TPR）,X-ray photoelectron spectroscopy（XPS） and transmission electron microscopy（TEM）. Results showed that the modified catalyst had the mesoporous structure, comparatively higher amount of surface oxygen and larger oxygen vacancies than others. As a result of the structure and surface composition merits, a high methane combustion conversion（50%） could be obtained at a low temperature of 262 °C for the modified Co3O4/CeO2 composites catalysts. The experimental results demonstrated that ultrasonic impregnation treatment combined with the N2 thermal treatment prior to calcination in air had a promising application for preparation of Co3O4/CeO2 composites catalysts for low-temperature catalytic combustion of methane. Co3O4/CeO2 composites with high surface areas and ultrafine crystalline sizes for catalytic combustion of methane were firstly prepared by a new sol-gel method which combined ultrasonic impregnation treatment and calcination in N2 atmosphere. The samples were characterized by various means such as nitrogen adsorption/desorption, X-ray diffraction (XRD), H2 temperature-programmed reduction (H2-TPR), X-ray photoelectron spectroscopy (XPS) and transmission electron microscopy (TEM). Results showed that the modified catalyst had the mesoporous structure, comparatively higher amount of surface oxygen and larger oxygen vacancies than others. As a result of the structure and surface composition merits, a high methane combustion conversion (50%) could be obtained at a low temperature of 262°C for the modified Co3O4/CeO2 composites catalysts. The experimental results demonstrated that ultrasonic impregnation treatment combined with the N2 thermal treatment prior to calcination in air had a promising application for preparation of Co3O4/CeO2 composites catalysts for low-temperature catalytic combustion of methane. Ultrasonic impregnation can promote the organic reactions and suppresses the formation of active substance soft agglomerates. The superior Co3O4/CeO2 composites can be obtained due to the synergistic effect in the course of processing. [Display omitted] |
| Author | Hong Lu Chengfa Jiang Zhenwu Ding Wei Wang Wei Chu Yanyan Feng |
| AuthorAffiliation | Department of Chemical Engineering, Sichuan University;Sichuan Provincial Engineering Technology Center for Environmental Protection Catalytic Materials |
| Author_xml | – sequence: 1 givenname: Hong surname: Lu fullname: Lu, Hong organization: Department of Chemical Engineering, Sichuan University, Chengdu 610065, Sichuan, China – sequence: 2 givenname: Chengfa surname: Jiang fullname: Jiang, Chengfa email: jiangcf@scu.edu.cn organization: Department of Chemical Engineering, Sichuan University, Chengdu 610065, Sichuan, China – sequence: 3 givenname: Zhenwu surname: Ding fullname: Ding, Zhenwu organization: Department of Chemical Engineering, Sichuan University, Chengdu 610065, Sichuan, China – sequence: 4 givenname: Wei surname: Wang fullname: Wang, Wei organization: Department of Chemical Engineering, Sichuan University, Chengdu 610065, Sichuan, China – sequence: 5 givenname: Wei surname: Chu fullname: Chu, Wei email: chuwei1965@foxmail.com organization: Department of Chemical Engineering, Sichuan University, Chengdu 610065, Sichuan, China – sequence: 6 givenname: Yanyan surname: Feng fullname: Feng, Yanyan organization: Department of Chemical Engineering, Sichuan University, Chengdu 610065, Sichuan, China |
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| CitedBy_id | crossref_primary_10_1016_j_cattod_2018_09_007 crossref_primary_10_1016_j_jechem_2022_08_001 crossref_primary_10_1039_C7RA10892C crossref_primary_10_1039_D0NJ06110G crossref_primary_10_1021_acs_energyfuels_2c02719 crossref_primary_10_1007_s11164_022_04713_w crossref_primary_10_1016_j_apsusc_2017_02_186 crossref_primary_10_1016_j_ijhydene_2018_06_086 crossref_primary_10_1007_s10563_017_9234_1 crossref_primary_10_1021_acsami_0c21999 crossref_primary_10_1002_cctc_201801539 crossref_primary_10_1016_j_cattod_2017_04_053 crossref_primary_10_1002_advs_202204566 crossref_primary_10_1016_j_mcat_2022_112229 crossref_primary_10_1039_D2CY01880B crossref_primary_10_1016_j_jechem_2016_11_011 crossref_primary_10_1016_j_combustflame_2023_112739 crossref_primary_10_1016_j_jallcom_2017_11_008 crossref_primary_10_3390_nano13131917 crossref_primary_10_1039_C8CY00897C crossref_primary_10_1007_s10562_019_02731_9 crossref_primary_10_1016_j_jcis_2020_10_050 crossref_primary_10_1002_aoc_5100 crossref_primary_10_1007_s41810_020_00065_3 crossref_primary_10_1007_s10563_018_9240_y crossref_primary_10_1007_s11164_023_05164_7 crossref_primary_10_1016_j_joei_2023_101341 |
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| Keywords | Catalytic combustion Sol-gel method Ultrasonic N2 calcination Co3O4/CeO2 |
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| Notes | Hong Lu;Chengfa Jiang;Zhenwu Ding;Wei Wang;Wei Chu;Yanyan Feng;Department of Chemical Engineering, Sichuan University;Sichuan Provincial Engineering Technology Center for Environmental Protection Catalytic Materials 21-1585/O4 |
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| Snippet | Co3O4/CeO2 composites with high surface areas and ultrafine crystalline sizes for catalytic combustion of methane were firstly prepared by a new sol-gel method... |
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| SubjectTerms | Catalytic combustion Co3O4/CeO2 N2 calcination Sol-gel method Ultrasonic |
| Title | Effects of ultrasonic impregnation combined with calcination in N2 atmosphere on the property of Co3O4/CeO2 composites for catalytic methane combustion |
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