Cu(II)–Fe(II)–H2O2 oxidative removal of 3-nitroaniline in water under microwave irradiation
•Coexistence of Cu(II) and Fe(II) in MW-Fenton-like process was studied in detail.•3-Nitroaniline was removed effectively by MW-Cu(II)-Fenton process.•Experimental parameters were optimized by kinetics study.•Relationship between reaction rate constant and reactant concentration was determined.•Prob...
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| Published in | Chemical engineering journal (Lausanne, Switzerland : 1996) Vol. 260; pp. 386 - 392 |
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| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
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Elsevier B.V
15.01.2015
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| Abstract | •Coexistence of Cu(II) and Fe(II) in MW-Fenton-like process was studied in detail.•3-Nitroaniline was removed effectively by MW-Cu(II)-Fenton process.•Experimental parameters were optimized by kinetics study.•Relationship between reaction rate constant and reactant concentration was determined.•Probable Cu(II) effect in MW-Cu(II)-Fenton process was examined preliminarily.
Cu(II)–Fe(II)–H2O2 process was studied through degrading 3-nitroaniline (3-NA) in water under microwave (MW) irradiation. The experimental conditions were studied by investigating the removal rates and reaction rate constants of 3-NA at different levels of influence factors. The removal rates and reaction rate constants both increased with the increase of Cu(II), Fe(II) and H2O2 dosages when they were at reasonable concentration ranges ([Cu(II)] 0.0016–0.0094mmolL−1, [Fe(II)] 0.051–0.205mmolL−1 and [H2O2] 4.34–17.34mmolL−1). Under the examined conditions (initial pH=5.3, [Cu(II)], [Fe(II)] and [H2O2] were 0.0078, 0.205 and 17.37mmolL−1, respectively, PMW=100W, V3-NA=400mL), more than 92% of 3-NA was removed at 8.5min and the reaction rate constant reached 0.310min−1. Furthermore, the mathematical relationship between reaction rate constants and reactants concentrations was obtained via kinetic study, the result was k=43.9·e-2905.2T·[H2O2]1.675·[Fe(II)]0.908·[Cu(II)]0.080. Finally, the probable effect of Cu(II) in Cu(II)-Fenton process under MW irradiation was speculated according to the comparison result of 2-hydroxyterephtalic acid (generated by the reaction between hydroxyl radicals and terephthalic acid) intensity, the study of synergetic effects of Cu(II) and Fe(II) in Cu(II)-Fenton process and the comparative analysis of reaction mechanisms in Fenton process and Cu(II)–H2O2 process. |
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| AbstractList | •Coexistence of Cu(II) and Fe(II) in MW-Fenton-like process was studied in detail.•3-Nitroaniline was removed effectively by MW-Cu(II)-Fenton process.•Experimental parameters were optimized by kinetics study.•Relationship between reaction rate constant and reactant concentration was determined.•Probable Cu(II) effect in MW-Cu(II)-Fenton process was examined preliminarily.
Cu(II)–Fe(II)–H2O2 process was studied through degrading 3-nitroaniline (3-NA) in water under microwave (MW) irradiation. The experimental conditions were studied by investigating the removal rates and reaction rate constants of 3-NA at different levels of influence factors. The removal rates and reaction rate constants both increased with the increase of Cu(II), Fe(II) and H2O2 dosages when they were at reasonable concentration ranges ([Cu(II)] 0.0016–0.0094mmolL−1, [Fe(II)] 0.051–0.205mmolL−1 and [H2O2] 4.34–17.34mmolL−1). Under the examined conditions (initial pH=5.3, [Cu(II)], [Fe(II)] and [H2O2] were 0.0078, 0.205 and 17.37mmolL−1, respectively, PMW=100W, V3-NA=400mL), more than 92% of 3-NA was removed at 8.5min and the reaction rate constant reached 0.310min−1. Furthermore, the mathematical relationship between reaction rate constants and reactants concentrations was obtained via kinetic study, the result was k=43.9·e-2905.2T·[H2O2]1.675·[Fe(II)]0.908·[Cu(II)]0.080. Finally, the probable effect of Cu(II) in Cu(II)-Fenton process under MW irradiation was speculated according to the comparison result of 2-hydroxyterephtalic acid (generated by the reaction between hydroxyl radicals and terephthalic acid) intensity, the study of synergetic effects of Cu(II) and Fe(II) in Cu(II)-Fenton process and the comparative analysis of reaction mechanisms in Fenton process and Cu(II)–H2O2 process. |
| Author | Wang, Peng Jiang, Jiping Wang, Nannan Zheng, Tong |
| Author_xml | – sequence: 1 givenname: Nannan surname: Wang fullname: Wang, Nannan organization: School of Municipal and Environmental Engineering, Harbin Institute of Technology, Harbin 150090, PR China – sequence: 2 givenname: Tong surname: Zheng fullname: Zheng, Tong organization: School of Municipal and Environmental Engineering, Harbin Institute of Technology, Harbin 150090, PR China – sequence: 3 givenname: Jiping surname: Jiang fullname: Jiang, Jiping organization: School of Municipal and Environmental Engineering, Harbin Institute of Technology, Harbin 150090, PR China – sequence: 4 givenname: Peng surname: Wang fullname: Wang, Peng email: pwang73@hit.edu.cn organization: School of Municipal and Environmental Engineering, Harbin Institute of Technology, Harbin 150090, PR China |
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| Snippet | •Coexistence of Cu(II) and Fe(II) in MW-Fenton-like process was studied in detail.•3-Nitroaniline was removed effectively by MW-Cu(II)-Fenton... |
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| SubjectTerms | 3-Nitroaniline Combined-catalyst Fenton-like process Kinetics Microwave assistance |
| Title | Cu(II)–Fe(II)–H2O2 oxidative removal of 3-nitroaniline in water under microwave irradiation |
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