Recovering levulinic acid by adsorption using efficient basic anion exchangers
Levulinic acid (LA) is a versatile compound used in biofuels, resins, etc., and its efficient recovery is required for its high value-added use. This study investigates the use of four anion exchange resins -Lewatit M-500 (a strong basic anion exchanger) and three weak basic anion exchangers (WBAEs)...
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| Published in | Separation science and technology Vol. 60; no. 11; pp. 1300 - 1315 |
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| Main Authors | , , |
| Format | Journal Article |
| Language | English |
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Taylor & Francis
24.07.2025
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| Abstract | Levulinic acid (LA) is a versatile compound used in biofuels, resins, etc., and its efficient recovery is required for its high value-added use. This study investigates the use of four anion exchange resins -Lewatit M-500 (a strong basic anion exchanger) and three weak basic anion exchangers (WBAEs), namely Amberlite IRA-67, Lewatit MP-62, and Lewatit MP-64- for LA recovery. The effects of pH, agitation time, LA concentration, resin dosage, and temperature on the adsorption efficiency were studied via batch experiments. Solution pH significantly influenced the yield. The highest efficiency was obtained at pH 2.1 for the WBAEs and pH 5 for Lewatit M-500. The kinetic data followed the pseudo-second-order model with R
2
>0.99. Increasing temperature slightly decreased the efficiency, with negative values for enthalpy (ΔH°) and Gibbs free energy (ΔG°), suggesting that the process was spontaneous and exothermic. The yield increased with resin dosage but decreased with higher initial LA concentrations. The highest adsorption capacity obtained from the four resins followed the order: Lewatit MP-62 (487.7 mg/g) > Amberlite IRA-67 (418.0 mg/g) > Lewatit MP-64 (371.6 mg/g) > Lewatit M-500 (278.7 mg/g). The successive adsorption-desorption trials using Lewatit MP-62 showed a slight decline (90% to 85%) in recovery efficiency over five cycles. |
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| AbstractList | Levulinic acid (LA) is a versatile compound used in biofuels, resins, etc., and its efficient recovery is required for its high value-added use. This study investigates the use of four anion exchange resins -Lewatit M-500 (a strong basic anion exchanger) and three weak basic anion exchangers (WBAEs), namely Amberlite IRA-67, Lewatit MP-62, and Lewatit MP-64- for LA recovery. The effects of pH, agitation time, LA concentration, resin dosage, and temperature on the adsorption efficiency were studied via batch experiments. Solution pH significantly influenced the yield. The highest efficiency was obtained at pH 2.1 for the WBAEs and pH 5 for Lewatit M-500. The kinetic data followed the pseudo-second-order model with R
2
>0.99. Increasing temperature slightly decreased the efficiency, with negative values for enthalpy (ΔH°) and Gibbs free energy (ΔG°), suggesting that the process was spontaneous and exothermic. The yield increased with resin dosage but decreased with higher initial LA concentrations. The highest adsorption capacity obtained from the four resins followed the order: Lewatit MP-62 (487.7 mg/g) > Amberlite IRA-67 (418.0 mg/g) > Lewatit MP-64 (371.6 mg/g) > Lewatit M-500 (278.7 mg/g). The successive adsorption-desorption trials using Lewatit MP-62 showed a slight decline (90% to 85%) in recovery efficiency over five cycles. |
| Author | Zeidan, Hani Altinsu, Yasemin Cemile Marti, Mustafa Esen |
| Author_xml | – sequence: 1 givenname: Yasemin Cemile surname: Altinsu fullname: Altinsu, Yasemin Cemile organization: Konya Technical University – sequence: 2 givenname: Hani surname: Zeidan fullname: Zeidan, Hani organization: Konya Technical University – sequence: 3 givenname: Mustafa Esen surname: Marti fullname: Marti, Mustafa Esen email: memarti@ktun.edu.tr, mustafaesenmarti@gmail.com organization: Konya Technical University |
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| SubjectTerms | adsorption Anion exchanger carboxylic acid ion exchange levulinic acid separation |
| Title | Recovering levulinic acid by adsorption using efficient basic anion exchangers |
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