Facile synthesis of ZnO nanoparticles for the effective photodegradation of malachite green dye in aqueous solution
Zinc oxide (ZnO) nanoparticles were synthesized using a simple co‐precipitation method and applied for effective photodegradation of malachite green (MG) dye in an aqueous solution. The synthesized ZnO nanoparticles were characterized by X‐ray diffraction (XRD), field emission scanning electron micr...
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| Published in | Water and environment journal : WEJ Vol. 36; no. 3; pp. 513 - 524 |
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| Main Authors | , , |
| Format | Journal Article |
| Language | English |
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London
Wiley Subscription Services, Inc
01.08.2022
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| Abstract | Zinc oxide (ZnO) nanoparticles were synthesized using a simple co‐precipitation method and applied for effective photodegradation of malachite green (MG) dye in an aqueous solution. The synthesized ZnO nanoparticles were characterized by X‐ray diffraction (XRD), field emission scanning electron microscopy (FESEM), energy dispersive spectroscopy (EDS), Fourier transform infrared (FTIR), and ultraviolet–visible (UV–vis) spectroscopic techniques. XRD pattern is confirmed the formation of crystalline ZnO nanoparticles with hexagonal wurtzite structure while the FESEM image validates the preparation of disc‐like spherical nanostructures agglomerated with the size of 30–50 nm. The nanostructures exhibited a strong UV absorption band at 370 nm, and the bandgap energy calculated from the Tauc plot is 3.12 eV. The prepared ZnO nanoparticles exhibited 92.07% photodegradation efficiency against the MG dye in 2 h of UV light irradiation at pH 8. The experimental data has followed the pseudo‐first‐order kinetic model, and the rate constant value obtained is 20.433 × 10−3 min−1. Thus, the synthesized ZnO nanoparticles degraded MG dye effectively and can be utilized for environmental remediation purposes. |
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| AbstractList | Zinc oxide (ZnO) nanoparticles were synthesized using a simple co‐precipitation method and applied for effective photodegradation of malachite green (MG) dye in an aqueous solution. The synthesized ZnO nanoparticles were characterized by X‐ray diffraction (XRD), field emission scanning electron microscopy (FESEM), energy dispersive spectroscopy (EDS), Fourier transform infrared (FTIR), and ultraviolet–visible (UV–vis) spectroscopic techniques. XRD pattern is confirmed the formation of crystalline ZnO nanoparticles with hexagonal wurtzite structure while the FESEM image validates the preparation of disc‐like spherical nanostructures agglomerated with the size of 30–50 nm. The nanostructures exhibited a strong UV absorption band at 370 nm, and the bandgap energy calculated from the Tauc plot is 3.12 eV. The prepared ZnO nanoparticles exhibited 92.07% photodegradation efficiency against the MG dye in 2 h of UV light irradiation at pH 8. The experimental data has followed the pseudo‐first‐order kinetic model, and the rate constant value obtained is 20.433 × 10−3 min−1. Thus, the synthesized ZnO nanoparticles degraded MG dye effectively and can be utilized for environmental remediation purposes. Zinc oxide (ZnO) nanoparticles were synthesized using a simple co‐precipitation method and applied for effective photodegradation of malachite green (MG) dye in an aqueous solution. The synthesized ZnO nanoparticles were characterized by X‐ray diffraction (XRD), field emission scanning electron microscopy (FESEM), energy dispersive spectroscopy (EDS), Fourier transform infrared (FTIR), and ultraviolet–visible (UV–vis) spectroscopic techniques. XRD pattern is confirmed the formation of crystalline ZnO nanoparticles with hexagonal wurtzite structure while the FESEM image validates the preparation of disc‐like spherical nanostructures agglomerated with the size of 30–50 nm. The nanostructures exhibited a strong UV absorption band at 370 nm, and the bandgap energy calculated from the Tauc plot is 3.12 eV. The prepared ZnO nanoparticles exhibited 92.07% photodegradation efficiency against the MG dye in 2 h of UV light irradiation at pH 8. The experimental data has followed the pseudo‐first‐order kinetic model, and the rate constant value obtained is 20.433 × 10⁻³ min⁻¹. Thus, the synthesized ZnO nanoparticles degraded MG dye effectively and can be utilized for environmental remediation purposes. Zinc oxide (ZnO) nanoparticles were synthesized using a simple co‐precipitation method and applied for effective photodegradation of malachite green (MG) dye in an aqueous solution. The synthesized ZnO nanoparticles were characterized by X‐ray diffraction (XRD), field emission scanning electron microscopy (FESEM), energy dispersive spectroscopy (EDS), Fourier transform infrared (FTIR), and ultraviolet–visible (UV–vis) spectroscopic techniques. XRD pattern is confirmed the formation of crystalline ZnO nanoparticles with hexagonal wurtzite structure while the FESEM image validates the preparation of disc‐like spherical nanostructures agglomerated with the size of 30–50 nm. The nanostructures exhibited a strong UV absorption band at 370 nm, and the bandgap energy calculated from the Tauc plot is 3.12 eV. The prepared ZnO nanoparticles exhibited 92.07% photodegradation efficiency against the MG dye in 2 h of UV light irradiation at pH 8. The experimental data has followed the pseudo‐first‐order kinetic model, and the rate constant value obtained is 20.433 × 10−3 min−1. Thus, the synthesized ZnO nanoparticles degraded MG dye effectively and can be utilized for environmental remediation purposes. Zinc oxide (ZnO) nanoparticles were synthesized using a simple co‐precipitation method and applied for effective photodegradation of malachite green (MG) dye in an aqueous solution. The synthesized ZnO nanoparticles were characterized by X‐ray diffraction (XRD), field emission scanning electron microscopy (FESEM), energy dispersive spectroscopy (EDS), Fourier transform infrared (FTIR), and ultraviolet–visible (UV–vis) spectroscopic techniques. XRD pattern is confirmed the formation of crystalline ZnO nanoparticles with hexagonal wurtzite structure while the FESEM image validates the preparation of disc‐like spherical nanostructures agglomerated with the size of 30–50 nm. The nanostructures exhibited a strong UV absorption band at 370 nm, and the bandgap energy calculated from the Tauc plot is 3.12 eV. The prepared ZnO nanoparticles exhibited 92.07% photodegradation efficiency against the MG dye in 2 h of UV light irradiation at pH 8. The experimental data has followed the pseudo‐first‐order kinetic model, and the rate constant value obtained is 20.433 × 10 −3 min −1 . Thus, the synthesized ZnO nanoparticles degraded MG dye effectively and can be utilized for environmental remediation purposes. |
| Author | Poswal, Krishna Meena, Parmeshwar Lal Surela, Ajay Kumar |
| Author_xml | – sequence: 1 givenname: Parmeshwar Lal orcidid: 0000-0003-4975-7250 surname: Meena fullname: Meena, Parmeshwar Lal email: parmeshwar1978@gmail.com organization: University of Rajasthan – sequence: 2 givenname: Krishna surname: Poswal fullname: Poswal, Krishna organization: University of Rajasthan – sequence: 3 givenname: Ajay Kumar surname: Surela fullname: Surela, Ajay Kumar organization: University of Rajasthan |
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| Snippet | Zinc oxide (ZnO) nanoparticles were synthesized using a simple co‐precipitation method and applied for effective photodegradation of malachite green (MG) dye... |
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| SubjectTerms | absorption Absorption spectra Analytical methods Aqueous solutions coprecipitation co‐precipitation method Dyes Electron microscopy energy energy-dispersive X-ray analysis environment Environmental cleanup Field emission microscopy Fourier transform infrared spectroscopy Fourier transforms Irradiation kinetics Light irradiation Malachite green malachite green dye Nanoparticles Nanostructure Photodegradation photodegradation efficiency photolysis remediation Scanning electron microscopy Spectroscopic techniques Synthesis Ultraviolet radiation water Wurtzite X-ray diffraction Zinc Zinc oxide Zinc oxides ZnO nanoparticles |
| Title | Facile synthesis of ZnO nanoparticles for the effective photodegradation of malachite green dye in aqueous solution |
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