Transmission and photoacoustic spectroscopy of organosulphur and aromatic hydrocarbons using coherent synchrotron radiation

•Transmission and photoacoustic spectra of hydrocarbons were acquired using coherent synchrotron radiation.•Effects of ring energy, current, and synchrotron frequency were determined.•Absorption bands were observed near 20 cm−1. This article describes transmission and photoacoustic spectroscopy expe...

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Published inInfrared physics & technology Vol. 94; pp. 91 - 95
Main Authors Michaelian, Kirk H., Billinghurst, Brant E., May, Tim E., Wurtz, Ward A., Baribeau, Cameron
Format Journal Article
LanguageEnglish
Published Elsevier B.V 01.11.2018
Subjects
Coherent synchrotron radiation
Hydrocarbons
THz spectroscopy
Coherent synchrotron radiation
Hydrocarbons
THz spectroscopy
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Abstract •Transmission and photoacoustic spectra of hydrocarbons were acquired using coherent synchrotron radiation.•Effects of ring energy, current, and synchrotron frequency were determined.•Absorption bands were observed near 20 cm−1. This article describes transmission and photoacoustic spectroscopy experiments performed using coherent synchrotron radiation (CSR) at the Canadian Light Source. The storage ring was operated at energies of 1.0 and 1.5 GeV, with currents between 0.8 and 8.6 mA and synchrotron frequencies from 4.0 to 7.7 kHz. Relationships among these parameters and the associated energy curves were characterized in detail. Spectra of organosulphur and aromatic hydrocarbon compounds acquired using CSR exhibited absorption bands near 20 cm−1, likely due to translational and rotational motion in dimers. The location and extent of usable CSR can be modified through adjustment of the ring energy, synchrotron frequency, and ring current, making this radiation suitable for acquisition of spectra at very low wavenumbers.
AbstractList •Transmission and photoacoustic spectra of hydrocarbons were acquired using coherent synchrotron radiation.•Effects of ring energy, current, and synchrotron frequency were determined.•Absorption bands were observed near 20 cm−1. This article describes transmission and photoacoustic spectroscopy experiments performed using coherent synchrotron radiation (CSR) at the Canadian Light Source. The storage ring was operated at energies of 1.0 and 1.5 GeV, with currents between 0.8 and 8.6 mA and synchrotron frequencies from 4.0 to 7.7 kHz. Relationships among these parameters and the associated energy curves were characterized in detail. Spectra of organosulphur and aromatic hydrocarbon compounds acquired using CSR exhibited absorption bands near 20 cm−1, likely due to translational and rotational motion in dimers. The location and extent of usable CSR can be modified through adjustment of the ring energy, synchrotron frequency, and ring current, making this radiation suitable for acquisition of spectra at very low wavenumbers.
Author Michaelian, Kirk H.
May, Tim E.
Wurtz, Ward A.
Billinghurst, Brant E.
Baribeau, Cameron
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  fullname: Baribeau, Cameron
  organization: Canadian Light Source Inc., 44 Innovation Boulevard, Saskatoon, Saskatchewan S7N 2V3, Canada
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Keywords Coherent synchrotron radiation
Hydrocarbons
THz spectroscopy
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SubjectTerms Coherent synchrotron radiation
Hydrocarbons
THz spectroscopy
Title Transmission and photoacoustic spectroscopy of organosulphur and aromatic hydrocarbons using coherent synchrotron radiation
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