Temperature dependence of polymer melt viscosity obtained based on DSC data and the consistency between thermodynamic and kinetic fragility

The viscosity of the polymer melt has an impact on both the processing and properties of the product. However, conventional viscosity measurement methods have limitations such as strict testing conditions, large sample sizes, and long response times. This paper proposes a simplified method that util...

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Published inJournal of applied polymer science Vol. 141; no. 23
Main Authors Fang, Chenghui, Chen, Huanhuan, Zhou, Juan, Chen, Liping, Guo, Zichao, Chen, Wanghua
Format Journal Article
LanguageEnglish
Published Hoboken, USA John Wiley & Sons, Inc 15.06.2024
Wiley Subscription Services, Inc
Subjects
Addition polymerization
differential scanning calorimetry
Fragility
Measurement methods
polymer melt
Polymers
Temperature dependence
thermodynamic fragility
Thermodynamics
viscosity
Viscosity measurement
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Abstract The viscosity of the polymer melt has an impact on both the processing and properties of the product. However, conventional viscosity measurement methods have limitations such as strict testing conditions, large sample sizes, and long response times. This paper proposes a simplified method that utilizes differential scanning calorimetry to determine the viscosity–temperature relationship of the polymer melt. The research subjects consist of four noncrystalline polymers and five crystalline polymers. A new thermodynamic fragility formula of crystalline polymer is obtained. Additionally, high‐temperature limiting viscosity shows a good linear relationship with fragility. Compared with the traditional viscosity measurement, this method is a simpler and more effective way to model the viscosity of polymer melt and has broad prospects in application. Temperature dependence of polymer melt viscosity obtained by DSC.
AbstractList The viscosity of the polymer melt has an impact on both the processing and properties of the product. However, conventional viscosity measurement methods have limitations such as strict testing conditions, large sample sizes, and long response times. This paper proposes a simplified method that utilizes differential scanning calorimetry to determine the viscosity–temperature relationship of the polymer melt. The research subjects consist of four noncrystalline polymers and five crystalline polymers. A new thermodynamic fragility formula of crystalline polymer is obtained. Additionally, high‐temperature limiting viscosity shows a good linear relationship with fragility. Compared with the traditional viscosity measurement, this method is a simpler and more effective way to model the viscosity of polymer melt and has broad prospects in application.
The viscosity of the polymer melt has an impact on both the processing and properties of the product. However, conventional viscosity measurement methods have limitations such as strict testing conditions, large sample sizes, and long response times. This paper proposes a simplified method that utilizes differential scanning calorimetry to determine the viscosity–temperature relationship of the polymer melt. The research subjects consist of four noncrystalline polymers and five crystalline polymers. A new thermodynamic fragility formula of crystalline polymer is obtained. Additionally, high‐temperature limiting viscosity shows a good linear relationship with fragility. Compared with the traditional viscosity measurement, this method is a simpler and more effective way to model the viscosity of polymer melt and has broad prospects in application. Temperature dependence of polymer melt viscosity obtained by DSC.
Author Guo, Zichao
Fang, Chenghui
Zhou, Juan
Chen, Wanghua
Chen, Liping
Chen, Huanhuan
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Snippet The viscosity of the polymer melt has an impact on both the processing and properties of the product. However, conventional viscosity measurement methods have...
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SubjectTerms Addition polymerization
differential scanning calorimetry
Fragility
Measurement methods
polymer melt
Polymers
Temperature dependence
thermodynamic fragility
Thermodynamics
viscosity
Viscosity measurement
Title Temperature dependence of polymer melt viscosity obtained based on DSC data and the consistency between thermodynamic and kinetic fragility
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