Enhanced NH3 sensing performance of polyaniline via a facile morphology modification strategy
The synthesis of polyaniline (PANI) composites is an effective method to improve the ammonia (NH3) gas sensing performance of PANI, and it is of great significance to develop a simple method to prepare PANI composites. Herein, the PANI/halloysite nanotubes (PANI/HNTs) composite was prepared via a si...
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| Published in | Sensors and actuators. B, Chemical Vol. 369; p. 132302 |
|---|---|
| Main Authors | , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Lausanne
Elsevier B.V
15.10.2022
Elsevier Science Ltd |
| Subjects | |
| Online Access | Get full text |
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| Abstract | The synthesis of polyaniline (PANI) composites is an effective method to improve the ammonia (NH3) gas sensing performance of PANI, and it is of great significance to develop a simple method to prepare PANI composites. Herein, the PANI/halloysite nanotubes (PANI/HNTs) composite was prepared via a simple in-situ polymerization method. Morphology characterization results show that the HNTs are covered by PANI to form a porous three-dimensional structure. Especially, the specific surface areas of the PANI and PANI/HNTs are 15.892 and 25.899 m2/g, respectively, and the specific surface area of PANI has been greatly improved (1.63 times). Gas sensing properties test results show that the PANI/HNTs sensor exhibits larger response (1.60 times) and shorter response/recovery times (0.93/0.6 times) than that of the PANI sensor to 10 ppm NH3 (25 °C, 50% relative humidity). In addition, the PANI/HNTs sensor exhibits low detection limit of 10 ppb NH3 and excellent selectivity. The enhanced NH3 sensing performance of PANI can be attributed to the unique hollow structure and large specific surface area of HNTs. In this work, a simple method is proposed to improve the NH3 sensing performance of PANI only by morphology modification. Meanwhile, it provides an idea for the application of HNTs in the field of gas sensors.
•The NH3 sensing performance of PANI is improved by a facile morphology modification strategy.•PANI/HNTs sensor was prepared by the in-situ polymerization method.•PANI/HNTs sensor exhibits higher NH3 sensing response than the PANI sensor.•PANI/HNTs sensor has an ultra-low detection limit of 10 ppb NH3. |
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| AbstractList | The synthesis of polyaniline (PANI) composites is an effective method to improve the ammonia (NH3) gas sensing performance of PANI, and it is of great significance to develop a simple method to prepare PANI composites. Herein, the PANI/halloysite nanotubes (PANI/HNTs) composite was prepared via a simple in-situ polymerization method. Morphology characterization results show that the HNTs are covered by PANI to form a porous three-dimensional structure. Especially, the specific surface areas of the PANI and PANI/HNTs are 15.892 and 25.899 m2/g, respectively, and the specific surface area of PANI has been greatly improved (1.63 times). Gas sensing properties test results show that the PANI/HNTs sensor exhibits larger response (1.60 times) and shorter response/recovery times (0.93/0.6 times) than that of the PANI sensor to 10 ppm NH3 (25 °C, 50% relative humidity). In addition, the PANI/HNTs sensor exhibits low detection limit of 10 ppb NH3 and excellent selectivity. The enhanced NH3 sensing performance of PANI can be attributed to the unique hollow structure and large specific surface area of HNTs. In this work, a simple method is proposed to improve the NH3 sensing performance of PANI only by morphology modification. Meanwhile, it provides an idea for the application of HNTs in the field of gas sensors. The synthesis of polyaniline (PANI) composites is an effective method to improve the ammonia (NH3) gas sensing performance of PANI, and it is of great significance to develop a simple method to prepare PANI composites. Herein, the PANI/halloysite nanotubes (PANI/HNTs) composite was prepared via a simple in-situ polymerization method. Morphology characterization results show that the HNTs are covered by PANI to form a porous three-dimensional structure. Especially, the specific surface areas of the PANI and PANI/HNTs are 15.892 and 25.899 m2/g, respectively, and the specific surface area of PANI has been greatly improved (1.63 times). Gas sensing properties test results show that the PANI/HNTs sensor exhibits larger response (1.60 times) and shorter response/recovery times (0.93/0.6 times) than that of the PANI sensor to 10 ppm NH3 (25 °C, 50% relative humidity). In addition, the PANI/HNTs sensor exhibits low detection limit of 10 ppb NH3 and excellent selectivity. The enhanced NH3 sensing performance of PANI can be attributed to the unique hollow structure and large specific surface area of HNTs. In this work, a simple method is proposed to improve the NH3 sensing performance of PANI only by morphology modification. Meanwhile, it provides an idea for the application of HNTs in the field of gas sensors. •The NH3 sensing performance of PANI is improved by a facile morphology modification strategy.•PANI/HNTs sensor was prepared by the in-situ polymerization method.•PANI/HNTs sensor exhibits higher NH3 sensing response than the PANI sensor.•PANI/HNTs sensor has an ultra-low detection limit of 10 ppb NH3. |
| ArticleNumber | 132302 |
| Author | Duan, Xiaohui Yuan, Zhen Liu, Bohao Li, Xian Jiang, Yadong Zhao, Qiuni Duan, Zaihua Zhang, Yajie Tai, Huiling |
| Author_xml | – sequence: 1 givenname: Xiaohui surname: Duan fullname: Duan, Xiaohui organization: State Key Laboratory of Electronic Thin Films and Integrated Devices, School of Optoelectronic Science and Engineering, University of Electronic Science and Technology of China (UESTC), Chengdu 610054, PR China – sequence: 2 givenname: Zaihua surname: Duan fullname: Duan, Zaihua organization: State Key Laboratory of Electronic Thin Films and Integrated Devices, School of Optoelectronic Science and Engineering, University of Electronic Science and Technology of China (UESTC), Chengdu 610054, PR China – sequence: 3 givenname: Yajie surname: Zhang fullname: Zhang, Yajie organization: State Key Laboratory of Electronic Thin Films and Integrated Devices, School of Optoelectronic Science and Engineering, University of Electronic Science and Technology of China (UESTC), Chengdu 610054, PR China – sequence: 4 givenname: Bohao surname: Liu fullname: Liu, Bohao organization: State Key Laboratory of Electronic Thin Films and Integrated Devices, School of Optoelectronic Science and Engineering, University of Electronic Science and Technology of China (UESTC), Chengdu 610054, PR China – sequence: 5 givenname: Xian surname: Li fullname: Li, Xian organization: Agricultural Information Institute, Chinese Academy of Agricultural Sciences, Key Laboratory of Agricultural Information Service Technology of Ministry of Agriculture, Beijing 100081, PR China – sequence: 6 givenname: Qiuni surname: Zhao fullname: Zhao, Qiuni organization: State Key Laboratory of Electronic Thin Films and Integrated Devices, School of Optoelectronic Science and Engineering, University of Electronic Science and Technology of China (UESTC), Chengdu 610054, PR China – sequence: 7 givenname: Zhen surname: Yuan fullname: Yuan, Zhen organization: State Key Laboratory of Electronic Thin Films and Integrated Devices, School of Optoelectronic Science and Engineering, University of Electronic Science and Technology of China (UESTC), Chengdu 610054, PR China – sequence: 8 givenname: Yadong surname: Jiang fullname: Jiang, Yadong organization: State Key Laboratory of Electronic Thin Films and Integrated Devices, School of Optoelectronic Science and Engineering, University of Electronic Science and Technology of China (UESTC), Chengdu 610054, PR China – sequence: 9 givenname: Huiling surname: Tai fullname: Tai, Huiling email: taitai1980@uestc.edu.cn organization: State Key Laboratory of Electronic Thin Films and Integrated Devices, School of Optoelectronic Science and Engineering, University of Electronic Science and Technology of China (UESTC), Chengdu 610054, PR China |
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| SubjectTerms | Ammonia Composite materials Gas sensors Halloysite nanotubes Morphology Morphology modification NH3 sensor Polyaniline Polyanilines Relative humidity Selectivity Sensors Specific surface Surface area |
| Title | Enhanced NH3 sensing performance of polyaniline via a facile morphology modification strategy |
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