Comparison on molecular transformation of dissolved organic matter during Fenton and activated carbon adsorption processes for chemical cleaning wastewater treatment

[Display omitted] •Dissolved organic matter (DOM) was removed from chemical cleaning wastewater (CCW).•Molecular insight into DOM transformation was elucidated in Fenton and PAC processes.•PAC adsorption was efficient in removing aromatic compounds compared to Fenton.•Carboxylic-rich alicyclic molec...

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Published inSeparation and purification technology Vol. 344; p. 127226
Main Authors Zhao, Xiaodan, Huang, Zhuojun, Sun, Haosen, Zhao, Qiqi, Huang, Zhanghe, Zhang, Chun, Wang, Yang, Yang, Chunyan, Zhou, Zhen
Format Journal Article
LanguageEnglish
Published Elsevier B.V 20.09.2024
Subjects
Activated carbon adsorption
Chemical cleaning wastewater
Dissolved organic matter
Fenton oxidation
FT-ICR MS
Chemical cleaning wastewater
Dissolved organic matter
FT-ICR MS
Activated carbon adsorption
Fenton oxidation
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Abstract [Display omitted] •Dissolved organic matter (DOM) was removed from chemical cleaning wastewater (CCW).•Molecular insight into DOM transformation was elucidated in Fenton and PAC processes.•PAC adsorption was efficient in removing aromatic compounds compared to Fenton.•Carboxylic-rich alicyclic molecules/lignin dominated by CHON were produced in Fenton.•Aliphatic compounds in CCW were resistant to PAC adsorption and Fenton oxidation. This study employed Fenton oxidation and powdered activated carbon (PAC) adsorption processes for the removal of recalcitrant dissolved organic matter (DOM) in chemical cleaning wastewater (CCW) to meet discharge standards. Fourier transform ion cyclotron resonance mass spectrometry (FT-ICR MS) was used to identify resistant compounds and investigate the transformation characteristics of DOM. CCW mainly contained surfactant exhibiting heteroatom-rich characteristics, and both processes exhibited effective DOM removal but distinct selectivity towards different subclasses of formulas. PAC adsorption significantly decreased the number of DOM compounds and more effective in aromatic compounds than Fenton oxidation. The aliphatic compounds (AImod ≤ 0.5, 1.5 ≤ H/C ≤ 2.0) predominantly with saturated and reduced states were resistant to PAC adsorption, and particularly a specific CHONSP formula was the predominant contributor to residual DOM in the effluent. In contrast, Fenton oxidation degraded most substances in the CCW except for a few saturated and reduced compounds primarily consisting of CHO, resulting in an increase in DOM number. Two unsaturated subclasses, carboxylic-rich alicyclic molecules/lignin-like structures (primarily CHON) and carbohydrates (primarily CHONP and CHONSP), were prominently produced after Fenton oxidation. The major mechanisms governing Fenton oxidation of surfactant in CCW primarily involved dealkylation (25.2 %), oxygen addition (21.2 %), and decarboxylation (19.8 %). Given the unique removal preferences and resistance observed in Fenton and PAC processes, a combination approach could be explored in the future to achieve advanced overall performance.
AbstractList [Display omitted] •Dissolved organic matter (DOM) was removed from chemical cleaning wastewater (CCW).•Molecular insight into DOM transformation was elucidated in Fenton and PAC processes.•PAC adsorption was efficient in removing aromatic compounds compared to Fenton.•Carboxylic-rich alicyclic molecules/lignin dominated by CHON were produced in Fenton.•Aliphatic compounds in CCW were resistant to PAC adsorption and Fenton oxidation. This study employed Fenton oxidation and powdered activated carbon (PAC) adsorption processes for the removal of recalcitrant dissolved organic matter (DOM) in chemical cleaning wastewater (CCW) to meet discharge standards. Fourier transform ion cyclotron resonance mass spectrometry (FT-ICR MS) was used to identify resistant compounds and investigate the transformation characteristics of DOM. CCW mainly contained surfactant exhibiting heteroatom-rich characteristics, and both processes exhibited effective DOM removal but distinct selectivity towards different subclasses of formulas. PAC adsorption significantly decreased the number of DOM compounds and more effective in aromatic compounds than Fenton oxidation. The aliphatic compounds (AImod ≤ 0.5, 1.5 ≤ H/C ≤ 2.0) predominantly with saturated and reduced states were resistant to PAC adsorption, and particularly a specific CHONSP formula was the predominant contributor to residual DOM in the effluent. In contrast, Fenton oxidation degraded most substances in the CCW except for a few saturated and reduced compounds primarily consisting of CHO, resulting in an increase in DOM number. Two unsaturated subclasses, carboxylic-rich alicyclic molecules/lignin-like structures (primarily CHON) and carbohydrates (primarily CHONP and CHONSP), were prominently produced after Fenton oxidation. The major mechanisms governing Fenton oxidation of surfactant in CCW primarily involved dealkylation (25.2 %), oxygen addition (21.2 %), and decarboxylation (19.8 %). Given the unique removal preferences and resistance observed in Fenton and PAC processes, a combination approach could be explored in the future to achieve advanced overall performance.
ArticleNumber 127226
Author Wang, Yang
Zhao, Xiaodan
Zhou, Zhen
Huang, Zhuojun
Zhao, Qiqi
Yang, Chunyan
Sun, Haosen
Huang, Zhanghe
Zhang, Chun
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  email: zhouzhen@shiep.edu.cn
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Dissolved organic matter
FT-ICR MS
Activated carbon adsorption
Fenton oxidation
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Snippet [Display omitted] •Dissolved organic matter (DOM) was removed from chemical cleaning wastewater (CCW).•Molecular insight into DOM transformation was elucidated...
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StartPage 127226
SubjectTerms Activated carbon adsorption
Chemical cleaning wastewater
Dissolved organic matter
Fenton oxidation
FT-ICR MS
Title Comparison on molecular transformation of dissolved organic matter during Fenton and activated carbon adsorption processes for chemical cleaning wastewater treatment
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