High-performance thin film composite nanofiltration membranes with HOF-21 interlayer
Hydrogen-bonded organic frameworks (HOF) possess desirable properties such as intrinsic, modifiable, and uniform pore structures, making them highly promising materials for molecular separation. However, their application in membrane technology remains underexplored. This study successfully fabricat...
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| Published in | Desalination Vol. 601; p. 118528 |
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| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
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Elsevier B.V
15.04.2025
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| Online Access | Get full text |
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| Abstract | Hydrogen-bonded organic frameworks (HOF) possess desirable properties such as intrinsic, modifiable, and uniform pore structures, making them highly promising materials for molecular separation. However, their application in membrane technology remains underexplored. This study successfully fabricated a novel interlayered thin-film nanocomposite (ITFN) membrane, using HOF material as the intermediate layer. The HOF-21 interlayer facilitated hydrogen bonding with piperazine, retarding amine monomer diffusion and resulting in a thinner, denser polyamide (PA) selective layer. The interconnected, uniformly sized pores of the HOF-21 nanoparticles yielded ultra-thin ITFN membranes with a highly ordered three-dimensional porous architecture. The study demonstrates that the new ITFN membranes are successfully prepared, and the PA layer of the membrane presents a wrinkled structure, and the cross-linking enhancement results in the improvement of the membrane performance. Consequently, the ITFN membrane demonstrates a high water flux (36.44 L m−2 h−1 bar−1), coupled with a large Na2SO4 rejection rate (97.06 %). The study establishes a foundation for advancing HOF membranes in liquid-phase molecular separation, thereby broadening the potential applicability of HOF materials across diverse domains.
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•HOF-21 was used to prepare ITFN membrane.•The special mechanism of the HOF-21 interlayer was discussed.•The TFNi membrane exhibit high water flux and unchanged high salt rejection.•The simple preparation conditions of HOF-21 facilitated the practical application of ITFN. |
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| AbstractList | Hydrogen-bonded organic frameworks (HOF) possess desirable properties such as intrinsic, modifiable, and uniform pore structures, making them highly promising materials for molecular separation. However, their application in membrane technology remains underexplored. This study successfully fabricated a novel interlayered thin-film nanocomposite (ITFN) membrane, using HOF material as the intermediate layer. The HOF-21 interlayer facilitated hydrogen bonding with piperazine, retarding amine monomer diffusion and resulting in a thinner, denser polyamide (PA) selective layer. The interconnected, uniformly sized pores of the HOF-21 nanoparticles yielded ultra-thin ITFN membranes with a highly ordered three-dimensional porous architecture. The study demonstrates that the new ITFN membranes are successfully prepared, and the PA layer of the membrane presents a wrinkled structure, and the cross-linking enhancement results in the improvement of the membrane performance. Consequently, the ITFN membrane demonstrates a high water flux (36.44 L m−2 h−1 bar−1), coupled with a large Na2SO4 rejection rate (97.06 %). The study establishes a foundation for advancing HOF membranes in liquid-phase molecular separation, thereby broadening the potential applicability of HOF materials across diverse domains.
[Display omitted]
•HOF-21 was used to prepare ITFN membrane.•The special mechanism of the HOF-21 interlayer was discussed.•The TFNi membrane exhibit high water flux and unchanged high salt rejection.•The simple preparation conditions of HOF-21 facilitated the practical application of ITFN. |
| ArticleNumber | 118528 |
| Author | Wang, Jian Wang, Ao Ding, Mingmei Pan, Yang Xu, Hang Wang, Jingjun Hu, Tianlong |
| Author_xml | – sequence: 1 givenname: Jian surname: Wang fullname: Wang, Jian organization: School of Environmental Science and Engineering, Suzhou University of Science and Technology, Suzhou, China – sequence: 2 givenname: Hang surname: Xu fullname: Xu, Hang email: xuhang810826@hhu.edu.com organization: Key Laboratory of Integrated Regulation and Resource Development on Shallow Lakes, Ministry of Education, College of Environment, Hohai University, No.1 Xikang Road, Nanjing 210098, China – sequence: 3 givenname: Ao surname: Wang fullname: Wang, Ao organization: Key Laboratory of Integrated Regulation and Resource Development on Shallow Lakes, Ministry of Education, College of Environment, Hohai University, No.1 Xikang Road, Nanjing 210098, China – sequence: 4 givenname: Mingmei surname: Ding fullname: Ding, Mingmei organization: Key Laboratory of Integrated Regulation and Resource Development on Shallow Lakes, Ministry of Education, College of Environment, Hohai University, No.1 Xikang Road, Nanjing 210098, China – sequence: 5 givenname: Tianlong surname: Hu fullname: Hu, Tianlong organization: Key Laboratory of Integrated Regulation and Resource Development on Shallow Lakes, Ministry of Education, College of Environment, Hohai University, No.1 Xikang Road, Nanjing 210098, China – sequence: 6 givenname: Jingjun surname: Wang fullname: Wang, Jingjun organization: Key Laboratory of Integrated Regulation and Resource Development on Shallow Lakes, Ministry of Education, College of Environment, Hohai University, No.1 Xikang Road, Nanjing 210098, China – sequence: 7 givenname: Yang surname: Pan fullname: Pan, Yang email: panyang@mail.usts.edu.cn organization: School of Environmental Science and Engineering, Suzhou University of Science and Technology, Suzhou, China |
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