Fabrication of novel noble-metal-free ZnIn2S4/WC Schottky junction heterojunction photocatalyst: Efficient charge separation, increased active sites and low hydrogen production overpotential for boosting visible-light H2 evolution

•A novel noble metal-free ZnIn2S4/WC heterojunction was synthesized based on the combination of semiconductor and metal-like.•The optimal ZnIn2S4/WC photocatalysts have a lower overpotential for hydrogen evolution than pristine ZnIn2S4.•The H2 production ability of the optimal ZnIn2S4/WC was about 9...

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Published inJournal of alloys and compounds Vol. 901; p. 163709
Main Authors Ma, Xiaohui, Li, Wenjun, Ren, Chaojun, Li, Hongda, Li, Xinyang, Dong, Mei, Gao, Ying, Wang, Tianyu, Zhou, Hualei, Li, Yanyan
Format Journal Article
LanguageEnglish
Published Lausanne Elsevier B.V 25.04.2022
Elsevier BV
Subjects
Catalytic activity
Heterojunctions
Hydrogen
Hydrogen evolution
Hydrogen production
Hydrogen production overpotential
Nanoparticles
Noble metal-free
Noble metals
Photocatalysis
Photocatalysts
Photocatalytic hydrogen production
Reaction mechanisms
Schottky junction heterojunction
Separation
ZnIn2S4/WC
ZnIn2S4/WC
Hydrogen production overpotential
Photocatalytic hydrogen production
Noble metal-free
Schottky junction heterojunction
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Abstract •A novel noble metal-free ZnIn2S4/WC heterojunction was synthesized based on the combination of semiconductor and metal-like.•The optimal ZnIn2S4/WC photocatalysts have a lower overpotential for hydrogen evolution than pristine ZnIn2S4.•The H2 production ability of the optimal ZnIn2S4/WC was about 9.2 times than that of ZnIn2S4-1% Pt.•A feasible Schottky junction reaction mechanism of intensive photocatalytic activity was discussed. [Display omitted] Herein, we report the synthesis of ZnIn2S4 nanoparticles on bulk WC by a facile hydrothermal process to construct novel and highly efficient noble metal-free Schottky junction heterojunction photocatalysts. Morphology characterization revealed that the ZnIn2S4 nanoparticles were deposited on the surface of the WC. Meanwhile, the combination of the ZnIn2S4 and the metal-like WC formed the Schottky energy barrier, which greatly promoted the migration and separation of photo-generated carriers. Especially, the optimal ZnIn2S4/WC photocatalysts have a lower overpotential for hydrogen evolution (−0.35 V) than pristine ZnIn2S4 (−0.49 V). The hydrogen production ability of the optimal ZnIn2S4/WC photocatalyst (2400.3 μmol·h−1·g−1) was approximately 9.2 times higher than that of ZnIn2S4-1% Pt (260.1 μmol·h−1·g−1). Photocatalytic experiments demonstrated that metal-like WC plays an important role in replacing precious metal to increase the active site of ZnIn2S4. Moreover, a feasible Schottky junction reaction mechanism of intensive photocatalytic activity was discussed. This study proves that it is a very fascinating strategy to combine the advantages of ZnIn2S4 and metal-like to construct Schottky heterojunction for photocatalytic hydrogen production.
AbstractList Herein, we report the synthesis of ZnIn2S4 nanoparticles on bulk WC by a facile hydrothermal process to construct novel and highly efficient noble metal-free Schottky junction heterojunction photocatalysts. Morphology characterization revealed that the ZnIn2S4 nanoparticles were deposited on the surface of the WC. Meanwhile, the combination of the ZnIn2S4 and the metal-like WC formed the Schottky energy barrier, which greatly promoted the migration and separation of photo-generated carriers. Especially, the optimal ZnIn2S4/WC photocatalysts have a lower overpotential for hydrogen evolution (−0.35 V) than pristine ZnIn2S4 (−0.49 V). The hydrogen production ability of the optimal ZnIn2S4/WC photocatalyst (2400.3 μmol·h−1·g−1) was approximately 9.2 times higher than that of ZnIn2S4-1% Pt (260.1 μmol·h−1·g−1). Photocatalytic experiments demonstrated that metal-like WC plays an important role in replacing precious metal to increase the active site of ZnIn2S4. Moreover, a feasible Schottky junction reaction mechanism of intensive photocatalytic activity was discussed. This study proves that it is a very fascinating strategy to combine the advantages of ZnIn2S4 and metal-like to construct Schottky heterojunction for photocatalytic hydrogen production.
•A novel noble metal-free ZnIn2S4/WC heterojunction was synthesized based on the combination of semiconductor and metal-like.•The optimal ZnIn2S4/WC photocatalysts have a lower overpotential for hydrogen evolution than pristine ZnIn2S4.•The H2 production ability of the optimal ZnIn2S4/WC was about 9.2 times than that of ZnIn2S4-1% Pt.•A feasible Schottky junction reaction mechanism of intensive photocatalytic activity was discussed. [Display omitted] Herein, we report the synthesis of ZnIn2S4 nanoparticles on bulk WC by a facile hydrothermal process to construct novel and highly efficient noble metal-free Schottky junction heterojunction photocatalysts. Morphology characterization revealed that the ZnIn2S4 nanoparticles were deposited on the surface of the WC. Meanwhile, the combination of the ZnIn2S4 and the metal-like WC formed the Schottky energy barrier, which greatly promoted the migration and separation of photo-generated carriers. Especially, the optimal ZnIn2S4/WC photocatalysts have a lower overpotential for hydrogen evolution (−0.35 V) than pristine ZnIn2S4 (−0.49 V). The hydrogen production ability of the optimal ZnIn2S4/WC photocatalyst (2400.3 μmol·h−1·g−1) was approximately 9.2 times higher than that of ZnIn2S4-1% Pt (260.1 μmol·h−1·g−1). Photocatalytic experiments demonstrated that metal-like WC plays an important role in replacing precious metal to increase the active site of ZnIn2S4. Moreover, a feasible Schottky junction reaction mechanism of intensive photocatalytic activity was discussed. This study proves that it is a very fascinating strategy to combine the advantages of ZnIn2S4 and metal-like to construct Schottky heterojunction for photocatalytic hydrogen production.
ArticleNumber 163709
Author Gao, Ying
Wang, Tianyu
Dong, Mei
Li, Yanyan
Li, Wenjun
Zhou, Hualei
Ma, Xiaohui
Li, Hongda
Li, Xinyang
Ren, Chaojun
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  fullname: Ma, Xiaohui
  organization: Beijing Key Laboratory for Science and Application of Functional Molecular and Crystalline Materials, University of Science and Technology Beijing, Beijing 100083, China
– sequence: 2
  givenname: Wenjun
  surname: Li
  fullname: Li, Wenjun
  email: wjli_ustb@163.com
  organization: Beijing Key Laboratory for Science and Application of Functional Molecular and Crystalline Materials, University of Science and Technology Beijing, Beijing 100083, China
– sequence: 3
  givenname: Chaojun
  surname: Ren
  fullname: Ren, Chaojun
  organization: Beijing Aerospace Propulsion Institute, No.1 South Dahongmen Road, Beijing 100076, China
– sequence: 4
  givenname: Hongda
  surname: Li
  fullname: Li, Hongda
  organization: Center for Materials Science and Engineering, Guangxi University of Science and Technology, Liuzhou 545006, China
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  givenname: Xinyang
  surname: Li
  fullname: Li, Xinyang
  organization: Beijing Key Laboratory for Science and Application of Functional Molecular and Crystalline Materials, University of Science and Technology Beijing, Beijing 100083, China
– sequence: 6
  givenname: Mei
  surname: Dong
  fullname: Dong, Mei
  organization: Beijing Key Laboratory for Science and Application of Functional Molecular and Crystalline Materials, University of Science and Technology Beijing, Beijing 100083, China
– sequence: 7
  givenname: Ying
  surname: Gao
  fullname: Gao, Ying
  organization: Beijing Key Laboratory for Science and Application of Functional Molecular and Crystalline Materials, University of Science and Technology Beijing, Beijing 100083, China
– sequence: 8
  givenname: Tianyu
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  fullname: Wang, Tianyu
  organization: Beijing Key Laboratory for Science and Application of Functional Molecular and Crystalline Materials, University of Science and Technology Beijing, Beijing 100083, China
– sequence: 9
  givenname: Hualei
  surname: Zhou
  fullname: Zhou, Hualei
  organization: Beijing Key Laboratory for Science and Application of Functional Molecular and Crystalline Materials, University of Science and Technology Beijing, Beijing 100083, China
– sequence: 10
  givenname: Yanyan
  surname: Li
  fullname: Li, Yanyan
  organization: Beijing Key Laboratory for Science and Application of Functional Molecular and Crystalline Materials, University of Science and Technology Beijing, Beijing 100083, China
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Keywords ZnIn2S4/WC
Hydrogen production overpotential
Photocatalytic hydrogen production
Noble metal-free
Schottky junction heterojunction
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SSID ssj0001931
Score 2.5859122
Snippet •A novel noble metal-free ZnIn2S4/WC heterojunction was synthesized based on the combination of semiconductor and metal-like.•The optimal ZnIn2S4/WC...
Herein, we report the synthesis of ZnIn2S4 nanoparticles on bulk WC by a facile hydrothermal process to construct novel and highly efficient noble metal-free...
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crossref
elsevier
SourceType Aggregation Database
Publisher
StartPage 163709
SubjectTerms Catalytic activity
Heterojunctions
Hydrogen
Hydrogen evolution
Hydrogen production
Hydrogen production overpotential
Nanoparticles
Noble metal-free
Noble metals
Photocatalysis
Photocatalysts
Photocatalytic hydrogen production
Reaction mechanisms
Schottky junction heterojunction
Separation
ZnIn2S4/WC
Title Fabrication of novel noble-metal-free ZnIn2S4/WC Schottky junction heterojunction photocatalyst: Efficient charge separation, increased active sites and low hydrogen production overpotential for boosting visible-light H2 evolution
URI https://dx.doi.org/10.1016/j.jallcom.2022.163709
https://www.proquest.com/docview/2640404827
Volume 901
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