Insight into the early hydration characteristics of Portland cement with hydroxyethyl methyl cellulose highlighted by 1H low-field NMR
1H low-field nuclear magnetic resonance (1H NMR) as a non-destructive test method can effectively capture the water state changes in cement pastes. The water changes can in turn reflect the early hydration characteristics of cement pastes. Hydroxyethyl methyl cellulose (HEMC) with different viscosit...
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| Published in | Construction & building materials Vol. 424; p. 135904 |
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| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
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Elsevier Ltd
19.04.2024
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| Subjects | |
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| Abstract | 1H low-field nuclear magnetic resonance (1H NMR) as a non-destructive test method can effectively capture the water state changes in cement pastes. The water changes can in turn reflect the early hydration characteristics of cement pastes. Hydroxyethyl methyl cellulose (HEMC) with different viscosities affects the hydration characteristics of cement by acting on the water in different states. The following experimental results are obtained by testing hydration of cement pastes with HEMC by using 1H NMR test. Incorporating 0.1–3% HEMC with different viscosities all can effectively control the bleeding water phenomenon. HEMC can absorb a part of the water in the cement pastes. Incorporating 2–3% HEMC significantly delays the enrichment of the gel pores water and interlayer water. When the content of HEMC increases from 0% to 3%, the hydration degree of cement pastes tends to decrease. Besides, HEMC with higher viscosity of 15000–40000 mPa·s obviously delays the hydration process of cement pastes compared to HEMC with lower viscosity of 400 mPa·s.
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•1H low-field NMR can efficiently detect the hydration process of Portland cement with hydroxyethyl methyl cellulose (HEMC).•Incorporating HEMC effectively controls the bleeding water phenomenon.•The early cement hydration is obviously delayed by incorporating HEMC.•HEMC with higher viscosity more significantly affects the early hydration. |
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| AbstractList | 1H low-field nuclear magnetic resonance (1H NMR) as a non-destructive test method can effectively capture the water state changes in cement pastes. The water changes can in turn reflect the early hydration characteristics of cement pastes. Hydroxyethyl methyl cellulose (HEMC) with different viscosities affects the hydration characteristics of cement by acting on the water in different states. The following experimental results are obtained by testing hydration of cement pastes with HEMC by using 1H NMR test. Incorporating 0.1–3% HEMC with different viscosities all can effectively control the bleeding water phenomenon. HEMC can absorb a part of the water in the cement pastes. Incorporating 2–3% HEMC significantly delays the enrichment of the gel pores water and interlayer water. When the content of HEMC increases from 0% to 3%, the hydration degree of cement pastes tends to decrease. Besides, HEMC with higher viscosity of 15000–40000 mPa·s obviously delays the hydration process of cement pastes compared to HEMC with lower viscosity of 400 mPa·s.
[Display omitted]
•1H low-field NMR can efficiently detect the hydration process of Portland cement with hydroxyethyl methyl cellulose (HEMC).•Incorporating HEMC effectively controls the bleeding water phenomenon.•The early cement hydration is obviously delayed by incorporating HEMC.•HEMC with higher viscosity more significantly affects the early hydration. |
| ArticleNumber | 135904 |
| Author | Zhang, Peng Liang, Chaofeng Wang, Shunxiang Huang, Tianyong Zhang, Guofang |
| Author_xml | – sequence: 1 givenname: Shunxiang surname: Wang fullname: Wang, Shunxiang organization: School of Civil Engineering, Shaoxing University, Shaoxing 31200, China – sequence: 2 givenname: Guofang surname: Zhang fullname: Zhang, Guofang email: zgftj@sina.com organization: Key Laboratory of Advanced Civil Engineering Materials of Ministry of Education, School of Materials Science and Engineering, Tongji University, Shanghai 201804, China – sequence: 3 givenname: Chaofeng surname: Liang fullname: Liang, Chaofeng email: liangcf@tongji.edu.cn organization: School of Civil Engineering, Shaoxing University, Shaoxing 31200, China – sequence: 4 givenname: Tianyong surname: Huang fullname: Huang, Tianyong organization: State Key Laboratory of Solid Waste Reuse for Building Materials, Beijing Building Materials Academy of Sciences Research, Beijing 100041, China – sequence: 5 givenname: Peng surname: Zhang fullname: Zhang, Peng organization: School of Civil Engineering, Qingdao University of Technology, Qingdao 266033, China |
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| Keywords | Hydroxyethyl methyl cellulose (HEMC) Viscosities 1H low-field nuclear magnetic resonance Early hydration |
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| SubjectTerms | 1H low-field nuclear magnetic resonance Early hydration Hydroxyethyl methyl cellulose (HEMC) Viscosities |
| Title | Insight into the early hydration characteristics of Portland cement with hydroxyethyl methyl cellulose highlighted by 1H low-field NMR |
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