Electrospun cellulose nanofibers membranes with photothermal/pH-induced switchable wettability for oil-water separation and elimination of bacteria
Considering the substantial annual global discharge of oily wastewater, there exists a crucial requirement to develop smart membranes that possess environmentally sustainable attributes, tunable wettability, and potent antibacterial properties, enabling efficient and controlled separation of oil/wat...
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| Published in | Chemical engineering journal (Lausanne, Switzerland : 1996) Vol. 518; p. 164394 |
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| Main Authors | , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
15.08.2025
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| Subjects | |
| Online Access | Get full text |
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| Abstract | Considering the substantial annual global discharge of oily wastewater, there exists a crucial requirement to develop smart membranes that possess environmentally sustainable attributes, tunable wettability, and potent antibacterial properties, enabling efficient and controlled separation of oil/water mixtures. Here, a photothermal/pH-responsive electrospun cellulose nanofibers (ECF-P-Fe3O4-N) membrane endowed with wettability modulation and bacterial elimination capabilities was successfully prepared. The advancement in the fabrication method stemmed from the ingenious integration of three key strategies: the interpenetrating network formation between cellulose and the thermosensitive polymer, the co-precipitation embedding of photothermal medium (Fe3O4 NPs), and the chemical grafting of aminosilane. The resultant ECF-P-Fe3O4-N membrane exhibited fast and reversible wettability transitions between high hydrophilicity (under acid or high-temperature stimulation) and hydrophobicity (under alkali or low-temperature stimulation), achieving on-demand separation of diverse immiscible oil-water mixtures and surfactant-stabilized emulsions. The maximum separation flux for oil-water emulsions attained a value of 225.6 L m−2 h−1, accompanied by a separation efficiency surpassing 98.53 %. It also possessed strong elimination of bacteria, satisfying for the long-lasting contact usage. This work holds significant implications in designing smart membranes for remotely controlling the oil-water separation.
The photothermal/pH-responsive electrospun cellulose nanofibers membranes, capable of wettability regulation and bacterial elimination, were successfully fabricated through the integration of three strategies: the formation of interpenetrating networks, the co-precipitation embedding of Fe3O4 NPs, and the chemical grafting of aminosilane. The resultant ECF-P-Fe3O4-N membrane exhibited rapid and reversible wettability transitions, thereby enabling high-efficiency separation of oil-water mixtures and emulsions. [Display omitted]
•A smart electrospun cellulose nanofibers membrane was successfully prepared.•Reversible transitions of hydro-phil/phobia facilitate on-demand oil-water separation.•The membrane achieves a maximum flux of 225.6 L m−2 h−1 with >98.53 % efficiency.•It is highly antibacterial and suitable for prolonged contact use. |
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| AbstractList | Considering the substantial annual global discharge of oily wastewater, there exists a crucial requirement to develop smart membranes that possess environmentally sustainable attributes, tunable wettability, and potent antibacterial properties, enabling efficient and controlled separation of oil/water mixtures. Here, a photothermal/pH-responsive electrospun cellulose nanofibers (ECF-P-Fe3O4-N) membrane endowed with wettability modulation and bacterial elimination capabilities was successfully prepared. The advancement in the fabrication method stemmed from the ingenious integration of three key strategies: the interpenetrating network formation between cellulose and the thermosensitive polymer, the co-precipitation embedding of photothermal medium (Fe3O4 NPs), and the chemical grafting of aminosilane. The resultant ECF-P-Fe3O4-N membrane exhibited fast and reversible wettability transitions between high hydrophilicity (under acid or high-temperature stimulation) and hydrophobicity (under alkali or low-temperature stimulation), achieving on-demand separation of diverse immiscible oil-water mixtures and surfactant-stabilized emulsions. The maximum separation flux for oil-water emulsions attained a value of 225.6 L m−2 h−1, accompanied by a separation efficiency surpassing 98.53 %. It also possessed strong elimination of bacteria, satisfying for the long-lasting contact usage. This work holds significant implications in designing smart membranes for remotely controlling the oil-water separation.
The photothermal/pH-responsive electrospun cellulose nanofibers membranes, capable of wettability regulation and bacterial elimination, were successfully fabricated through the integration of three strategies: the formation of interpenetrating networks, the co-precipitation embedding of Fe3O4 NPs, and the chemical grafting of aminosilane. The resultant ECF-P-Fe3O4-N membrane exhibited rapid and reversible wettability transitions, thereby enabling high-efficiency separation of oil-water mixtures and emulsions. [Display omitted]
•A smart electrospun cellulose nanofibers membrane was successfully prepared.•Reversible transitions of hydro-phil/phobia facilitate on-demand oil-water separation.•The membrane achieves a maximum flux of 225.6 L m−2 h−1 with >98.53 % efficiency.•It is highly antibacterial and suitable for prolonged contact use. |
| ArticleNumber | 164394 |
| Author | Zheng, Wenqiu Xu, Feng Du, Yuhan Nawaz, Haq Li, Deqiang Yan, Ning Fang, Xubo Li, Xin |
| Author_xml | – sequence: 1 givenname: Xubo surname: Fang fullname: Fang, Xubo organization: State Key Laboratory of Efficient Production of Forest Resources, Beijing Key Laboratory of Lignocellulosic Chemistry, Beijing Forestry University, Beijing, 100083, China – sequence: 2 givenname: Yuhan surname: Du fullname: Du, Yuhan organization: State Key Laboratory of Efficient Production of Forest Resources, Beijing Key Laboratory of Lignocellulosic Chemistry, Beijing Forestry University, Beijing, 100083, China – sequence: 3 givenname: Haq surname: Nawaz fullname: Nawaz, Haq organization: Jiangsu Key Laboratory for Biomass-Based Energy and Enzyme Technology, School of Chemistry and Chemical Engineering, Huaiyin Normal University, Huaian 223300, Jiangsu, China – sequence: 4 givenname: Xin surname: Li fullname: Li, Xin email: xinli@bjfu.edu.cn organization: State Key Laboratory of Efficient Production of Forest Resources, Beijing Key Laboratory of Lignocellulosic Chemistry, Beijing Forestry University, Beijing, 100083, China – sequence: 5 givenname: Ning surname: Yan fullname: Yan, Ning organization: Department of Chemical Engineering and Applied Chemistry, University of Toronto, Toronto, Ontario M5S 3B3, Canada – sequence: 6 givenname: Wenqiu surname: Zheng fullname: Zheng, Wenqiu organization: State Key Laboratory of Efficient Production of Forest Resources, Beijing Key Laboratory of Lignocellulosic Chemistry, Beijing Forestry University, Beijing, 100083, China – sequence: 7 givenname: Deqiang surname: Li fullname: Li, Deqiang organization: State Key Laboratory of Efficient Production of Forest Resources, Beijing Key Laboratory of Lignocellulosic Chemistry, Beijing Forestry University, Beijing, 100083, China – sequence: 8 givenname: Feng surname: Xu fullname: Xu, Feng email: xfx315@bjfu.edu.cn organization: State Key Laboratory of Efficient Production of Forest Resources, Beijing Key Laboratory of Lignocellulosic Chemistry, Beijing Forestry University, Beijing, 100083, China |
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| Keywords | Oil-water separation Electrospun cellulose nanofibers membranes Antibacterial Photothermal/pH-responsive Switchable wettability |
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| Title | Electrospun cellulose nanofibers membranes with photothermal/pH-induced switchable wettability for oil-water separation and elimination of bacteria |
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