Preparation of hybrid photoelectrode based on defect-poor Zn-CuInSe2 QDs sensitized nanoporous ZnO nanosheets with an application in azo dye removal
The glutathione (GSH) and mercaptopropionic acid (MPA) modified internal defect-rich, surface defects-poor near infrared (NIR) Zn–CuInSe 2 (ZCISe) QDs were synthesized. Nanoporous ZnO nanosheets (NS) were firstly loaded with those ZCISe QDs to improve photoelectrochemical response in the NIR light r...
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| Published in | Journal of materials science. Materials in electronics Vol. 30; no. 8; pp. 7928 - 7939 |
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| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
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Springer US
01.04.2019
Springer Nature B.V |
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| Abstract | The glutathione (GSH) and mercaptopropionic acid (MPA) modified internal defect-rich, surface defects-poor near infrared (NIR) Zn–CuInSe
2
(ZCISe) QDs were synthesized. Nanoporous ZnO nanosheets (NS) were firstly loaded with those ZCISe QDs to improve photoelectrochemical response in the NIR light region. Then loading Mn doping CdS thin film onto the ZCISe/ZnO NS was further used to reduce the interfacial recombination between different components of hybrid photoelectrode, in addition to enhance the light absorption and resist the photo-oxidation decomposition of the photocatalysts. Successively introducing ZCISe and Mn–CdS onto ZnO NS can increase the photocurrent intensities from 1 mA/cm
2
for naked ZnO NS, 2.2 mA/cm
2
for ZCISe/ZnO NS, to 9 mA/cm
2
for Mn–CdS/ZCISe/ZnO NS. Here, excellent performance of ZCISe based ZnO NS photoelectrode is mainly attributed to an intrinsic defect state-related donor–acceptor pair (DAP) in ZCISe QDs with long-lived photogenerated carriers. Photocatalytic properties of Mn–CdS/ZCISe/ZnO NS were evaluated by removing azo dyes with an efficiency of 83%, an enhancement of 97% compared to that of ZnO NS. |
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| AbstractList | The glutathione (GSH) and mercaptopropionic acid (MPA) modified internal defect-rich, surface defects-poor near infrared (NIR) Zn–CuInSe2 (ZCISe) QDs were synthesized. Nanoporous ZnO nanosheets (NS) were firstly loaded with those ZCISe QDs to improve photoelectrochemical response in the NIR light region. Then loading Mn doping CdS thin film onto the ZCISe/ZnO NS was further used to reduce the interfacial recombination between different components of hybrid photoelectrode, in addition to enhance the light absorption and resist the photo-oxidation decomposition of the photocatalysts. Successively introducing ZCISe and Mn–CdS onto ZnO NS can increase the photocurrent intensities from 1 mA/cm2 for naked ZnO NS, 2.2 mA/cm2 for ZCISe/ZnO NS, to 9 mA/cm2 for Mn–CdS/ZCISe/ZnO NS. Here, excellent performance of ZCISe based ZnO NS photoelectrode is mainly attributed to an intrinsic defect state-related donor–acceptor pair (DAP) in ZCISe QDs with long-lived photogenerated carriers. Photocatalytic properties of Mn–CdS/ZCISe/ZnO NS were evaluated by removing azo dyes with an efficiency of 83%, an enhancement of 97% compared to that of ZnO NS. The glutathione (GSH) and mercaptopropionic acid (MPA) modified internal defect-rich, surface defects-poor near infrared (NIR) Zn–CuInSe 2 (ZCISe) QDs were synthesized. Nanoporous ZnO nanosheets (NS) were firstly loaded with those ZCISe QDs to improve photoelectrochemical response in the NIR light region. Then loading Mn doping CdS thin film onto the ZCISe/ZnO NS was further used to reduce the interfacial recombination between different components of hybrid photoelectrode, in addition to enhance the light absorption and resist the photo-oxidation decomposition of the photocatalysts. Successively introducing ZCISe and Mn–CdS onto ZnO NS can increase the photocurrent intensities from 1 mA/cm 2 for naked ZnO NS, 2.2 mA/cm 2 for ZCISe/ZnO NS, to 9 mA/cm 2 for Mn–CdS/ZCISe/ZnO NS. Here, excellent performance of ZCISe based ZnO NS photoelectrode is mainly attributed to an intrinsic defect state-related donor–acceptor pair (DAP) in ZCISe QDs with long-lived photogenerated carriers. Photocatalytic properties of Mn–CdS/ZCISe/ZnO NS were evaluated by removing azo dyes with an efficiency of 83%, an enhancement of 97% compared to that of ZnO NS. |
| Author | Cao, Kesheng Li, Weili Yao, Lu Cheng, Runrun Sheng, Pengtao Li, Songtian Geng, Hongchao |
| Author_xml | – sequence: 1 givenname: Lu surname: Yao fullname: Yao, Lu organization: College of Chemistry and Molecular Engineering, Zhengzhou University, College of Chemistry and Environmental Engineering, Pingdingshan University – sequence: 2 givenname: Hongchao surname: Geng fullname: Geng, Hongchao organization: College of Chemistry and Molecular Engineering, Zhengzhou University, College of Chemistry and Environmental Engineering, Pingdingshan University – sequence: 3 givenname: Runrun surname: Cheng fullname: Cheng, Runrun organization: College of Chemistry and Environmental Engineering, Pingdingshan University – sequence: 4 givenname: Kesheng surname: Cao fullname: Cao, Kesheng organization: Analytical Instrumentation Center, Pingdingshan University – sequence: 5 givenname: Pengtao surname: Sheng fullname: Sheng, Pengtao organization: College of Chemistry and Environmental Engineering, Pingdingshan University – sequence: 6 givenname: Weili orcidid: 0000-0002-8387-6539 surname: Li fullname: Li, Weili email: liweiliziji11@126.com organization: College of Chemistry and Environmental Engineering, Pingdingshan University – sequence: 7 givenname: Songtian surname: Li fullname: Li, Songtian email: PDSUCHEM@sina.com organization: College of Chemistry and Environmental Engineering, Pingdingshan University |
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| CitedBy_id | crossref_primary_10_1016_j_mseb_2023_116556 crossref_primary_10_1016_j_jallcom_2020_153700 crossref_primary_10_1007_s00216_020_02974_1 |
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| SubjectTerms | Azo dyes Cadmium sulfide Characterization and Evaluation of Materials Chemistry and Materials Science Copper indium selenides Defects Electromagnetic absorption Glutathione Materials Science Nanosheets Optical and Electronic Materials Oxidation Photocatalysis Photoelectric effect Photoelectric emission Photovoltaic cells Surface defects Thin films Zinc oxide |
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| Title | Preparation of hybrid photoelectrode based on defect-poor Zn-CuInSe2 QDs sensitized nanoporous ZnO nanosheets with an application in azo dye removal |
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