Exploring the peel ash of musa acuminate as a heterogeneous green catalyst for producing biodiesel from Niger oil: A sustainable and circular bio economic approach

Currently, biodiesel stands as a sustainable and renewable alternative to depleting fossil fuels like petro-diesel. The widespread adoption of biodiesel production holds promise for enhancing environmental quality by reducing greenhouse gas emissions and promoting societal-economic development. In l...

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Published inSustainable chemistry and pharmacy Vol. 39; p. 101622
Main Authors Rajak, Amit Kumar, Madiga, Harikrishna, Mahato, Devi Lal, Pothu, Ramyakrishna, Periyasami, Govindasami, Sarangi, Prakash Kumar, Boddula, Rajender, Mallampalli S.L., Karuna
Format Journal Article
LanguageEnglish
Published Elsevier B.V 01.06.2024
Subjects
Banana peel ash
Biodiesel
Food waste
Green chemistry
Heterogeneous catalyst
Food waste
Heterogeneous catalyst
Green chemistry
Biodiesel
Banana peel ash
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Abstract Currently, biodiesel stands as a sustainable and renewable alternative to depleting fossil fuels like petro-diesel. The widespread adoption of biodiesel production holds promise for enhancing environmental quality by reducing greenhouse gas emissions and promoting societal-economic development. In line with this, our research has focused on synthesizing biodiesel from the novel and edible seed oil of Niger oil, utilizing a green catalyst derived from the calcination of banana peel ash at 600 °C for 4 h. Advanced characterization techniques, including X-Ray Diffraction (XRD), Scanning Electron Microscopy (SEM), Energy Diffraction X-Ray (EDX), Thermogravimetric Analysis (TGA), X-ray Photoelectron Spectroscopy (XPS), and Fourier-transform Infrared Spectroscopy (FT-IR), were employed to assess the catalytic activity of the catalyst. Under optimized reaction conditions a methanol-to-oil molar ratio of 15:1, catalyst loading of 1% (wt.%), reaction time of 4 h, and temperature of 70 °C we achieved a commendable biodiesel yield of 92.30%. Gas Chromatography (GC) analysis of the biodiesel revealed four distinctive peaks corresponding to methyl esters. Results from Fourier-transform Infrared Spectroscopy (FTIR) and Nuclear Magnetic Resonance (NMR) confirmed the presence of methyl esters in the biodiesel sample. Additionally, the fuel properties of the biodiesel, including density (0.904 kg/m3), kinematic viscosity (4.56 cst), cloud point (3 °C), pour point (2.8 °C), and flash point (149 °C), complied with international ASTM D standards. In conclusion, Niger biodiesel emerges as a highly promising, eco-friendly, reusable, and cost-effective feedstock for biodiesel production, thereby holding significant potential for advancing sustainable energy solutions. [Display omitted] •Environmentally friendly heterogeneous catalyst synthesis from biomass food waste.•The value-adding of leftover biogenic materials, such ash of banana peels.•Waste banana peel catalyst converts FAME at a rate of 92% with high efficiency.•The catalyst that was designed was stable and could be reused five times.•Green metrics shows that catalyst made of banana peel ash is low price and eco-safe.
AbstractList Currently, biodiesel stands as a sustainable and renewable alternative to depleting fossil fuels like petro-diesel. The widespread adoption of biodiesel production holds promise for enhancing environmental quality by reducing greenhouse gas emissions and promoting societal-economic development. In line with this, our research has focused on synthesizing biodiesel from the novel and edible seed oil of Niger oil, utilizing a green catalyst derived from the calcination of banana peel ash at 600 °C for 4 h. Advanced characterization techniques, including X-Ray Diffraction (XRD), Scanning Electron Microscopy (SEM), Energy Diffraction X-Ray (EDX), Thermogravimetric Analysis (TGA), X-ray Photoelectron Spectroscopy (XPS), and Fourier-transform Infrared Spectroscopy (FT-IR), were employed to assess the catalytic activity of the catalyst. Under optimized reaction conditions a methanol-to-oil molar ratio of 15:1, catalyst loading of 1% (wt.%), reaction time of 4 h, and temperature of 70 °C we achieved a commendable biodiesel yield of 92.30%. Gas Chromatography (GC) analysis of the biodiesel revealed four distinctive peaks corresponding to methyl esters. Results from Fourier-transform Infrared Spectroscopy (FTIR) and Nuclear Magnetic Resonance (NMR) confirmed the presence of methyl esters in the biodiesel sample. Additionally, the fuel properties of the biodiesel, including density (0.904 kg/m3), kinematic viscosity (4.56 cst), cloud point (3 °C), pour point (2.8 °C), and flash point (149 °C), complied with international ASTM D standards. In conclusion, Niger biodiesel emerges as a highly promising, eco-friendly, reusable, and cost-effective feedstock for biodiesel production, thereby holding significant potential for advancing sustainable energy solutions. [Display omitted] •Environmentally friendly heterogeneous catalyst synthesis from biomass food waste.•The value-adding of leftover biogenic materials, such ash of banana peels.•Waste banana peel catalyst converts FAME at a rate of 92% with high efficiency.•The catalyst that was designed was stable and could be reused five times.•Green metrics shows that catalyst made of banana peel ash is low price and eco-safe.
ArticleNumber 101622
Author Boddula, Rajender
Periyasami, Govindasami
Sarangi, Prakash Kumar
Mallampalli S.L., Karuna
Mahato, Devi Lal
Madiga, Harikrishna
Rajak, Amit Kumar
Pothu, Ramyakrishna
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  givenname: Amit Kumar
  surname: Rajak
  fullname: Rajak, Amit Kumar
  organization: Department of Energy & Environmental Engineering, CSIR−Indian Institute of Chemical Technology, Hyderabad, 500007, Telangana state, India
– sequence: 2
  givenname: Harikrishna
  surname: Madiga
  fullname: Madiga, Harikrishna
  organization: Department of Energy & Environmental Engineering, CSIR−Indian Institute of Chemical Technology, Hyderabad, 500007, Telangana state, India
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  givenname: Devi Lal
  surname: Mahato
  fullname: Mahato, Devi Lal
  organization: Department of Energy & Environmental Engineering, CSIR−Indian Institute of Chemical Technology, Hyderabad, 500007, Telangana state, India
– sequence: 4
  givenname: Ramyakrishna
  surname: Pothu
  fullname: Pothu, Ramyakrishna
  organization: School of Physics and Electronics, College of Chemistry and Chemical Engineering, Hunan University, Changsha, 410082, PR China
– sequence: 5
  givenname: Govindasami
  surname: Periyasami
  fullname: Periyasami, Govindasami
  organization: Department of Chemistry, College of Science, King Saud University, P.O. Box 2455, Riyadh 11451, Saudi Arabia
– sequence: 6
  givenname: Prakash Kumar
  surname: Sarangi
  fullname: Sarangi, Prakash Kumar
  organization: College of Agriculture, Central Agricultural University, Imphal, Manipur, 795004, India
– sequence: 7
  givenname: Rajender
  orcidid: 0000-0001-8533-3338
  surname: Boddula
  fullname: Boddula, Rajender
  email: research.raaj@gmail.com
  organization: Department of Energy & Environmental Engineering, CSIR−Indian Institute of Chemical Technology, Hyderabad, 500007, Telangana state, India
– sequence: 8
  givenname: Karuna
  surname: Mallampalli S.L.
  fullname: Mallampalli S.L., Karuna
  email: mslkaruna74@gmail.com
  organization: Department of Oils, Lipid Science & Technology, CSIR−Indian Institute of Chemical Technology, Hyderabad, 500007, Telangana state, India
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Heterogeneous catalyst
Green chemistry
Biodiesel
Banana peel ash
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Snippet Currently, biodiesel stands as a sustainable and renewable alternative to depleting fossil fuels like petro-diesel. The widespread adoption of biodiesel...
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SubjectTerms Banana peel ash
Biodiesel
Food waste
Green chemistry
Heterogeneous catalyst
Title Exploring the peel ash of musa acuminate as a heterogeneous green catalyst for producing biodiesel from Niger oil: A sustainable and circular bio economic approach
URI https://dx.doi.org/10.1016/j.scp.2024.101622
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