The Functionalized UiO-66 Engineering for the Synergistic Enhancement of Mechanical Properties of Polydicyclopentadiene Nanocomposites

In this paper, zirconium-based MOF (Zr-MOFs) materials, namely UIO-66, UIO-66-NH 2 , GMA-UIO-66 and NB-UIO-66, were selected as fillers to enhance the mechanical properties of polydicyclopentadiene (PDCPD) nanocomposites, and Zr-MOFs/PDCPD nanocomposites were prepared by in situ polymerization. The...

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Published in	Journal of inorganic and organometallic polymers and materials Vol. 33; no. 2; pp. 328 - 336
Main Authors	Gao, Feifei, Wu, Feiyang, Zhang, Xianyang, Jiang, Bowen, Li, Qizhong
Format	Journal Article
Language	English
Published	New York Springer US 01.02.2023 Springer Nature B.V
Subjects	Bend strength Chemistry Chemistry and Materials Science Field emission microscopy Flexural strength Fourier transforms Functional groups Impact strength Inorganic Chemistry Mechanical properties Modulus of rupture in bending Nanocomposites Organic Chemistry Polymer Sciences Toughness Zirconium Mechanical properties Thermal deformation temperature Composite materials UIO-66 Polydicyclopentadiene
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Abstract	In this paper, zirconium-based MOF (Zr-MOFs) materials, namely UIO-66, UIO-66-NH 2 , GMA-UIO-66 and NB-UIO-66, were selected as fillers to enhance the mechanical properties of polydicyclopentadiene (PDCPD) nanocomposites, and Zr-MOFs/PDCPD nanocomposites were prepared by in situ polymerization. The functional groups and morphology of Zr-MOFs were characterized by Fourier transform infrared (FT-IR), X-ray diffraction (XRD) and field emission scanning electron microscopy (SEM). The mechanical properties of Zr-MOFs/PDCPD composites were studied by tensile toughness, notched impact strength and bending strength test. Furthermore, the optimum Zr-MOFs loading was determined. The results show that when the mass fraction of NB-UIO-66 is 0.4%, the composites’ tensile toughness, flexural strength, impact strength and heat distortion temperature (HDT) are simultaneously increased by 47.3%, 37.5%, 119.4%, and 59.2% respectively, compared with the pure PDCPD, which synergistically enhances the mechanical properties. Graphical Abstract
AbstractList	In this paper, zirconium-based MOF (Zr-MOFs) materials, namely UIO-66, UIO-66-NH 2 , GMA-UIO-66 and NB-UIO-66, were selected as fillers to enhance the mechanical properties of polydicyclopentadiene (PDCPD) nanocomposites, and Zr-MOFs/PDCPD nanocomposites were prepared by in situ polymerization. The functional groups and morphology of Zr-MOFs were characterized by Fourier transform infrared (FT-IR), X-ray diffraction (XRD) and field emission scanning electron microscopy (SEM). The mechanical properties of Zr-MOFs/PDCPD composites were studied by tensile toughness, notched impact strength and bending strength test. Furthermore, the optimum Zr-MOFs loading was determined. The results show that when the mass fraction of NB-UIO-66 is 0.4%, the composites’ tensile toughness, flexural strength, impact strength and heat distortion temperature (HDT) are simultaneously increased by 47.3%, 37.5%, 119.4%, and 59.2% respectively, compared with the pure PDCPD, which synergistically enhances the mechanical properties. Graphical Abstract In this paper, zirconium-based MOF (Zr-MOFs) materials, namely UIO-66, UIO-66-NH2, GMA-UIO-66 and NB-UIO-66, were selected as fillers to enhance the mechanical properties of polydicyclopentadiene (PDCPD) nanocomposites, and Zr-MOFs/PDCPD nanocomposites were prepared by in situ polymerization. The functional groups and morphology of Zr-MOFs were characterized by Fourier transform infrared (FT-IR), X-ray diffraction (XRD) and field emission scanning electron microscopy (SEM). The mechanical properties of Zr-MOFs/PDCPD composites were studied by tensile toughness, notched impact strength and bending strength test. Furthermore, the optimum Zr-MOFs loading was determined. The results show that when the mass fraction of NB-UIO-66 is 0.4%, the composites’ tensile toughness, flexural strength, impact strength and heat distortion temperature (HDT) are simultaneously increased by 47.3%, 37.5%, 119.4%, and 59.2% respectively, compared with the pure PDCPD, which synergistically enhances the mechanical properties.
Author	Jiang, Bowen Li, Qizhong Zhang, Xianyang Gao, Feifei Wu, Feiyang
Author_xml	– sequence: 1 givenname: Feifei surname: Gao fullname: Gao, Feifei organization: State Key Laboratory of Advanced Technology for Materials Synthesis and Processing, Wuhan University of Technology – sequence: 2 givenname: Feiyang surname: Wu fullname: Wu, Feiyang organization: State Key Laboratory of Advanced Technology for Materials Synthesis and Processing, Wuhan University of Technology – sequence: 3 givenname: Xianyang surname: Zhang fullname: Zhang, Xianyang organization: State Key Laboratory of Advanced Technology for Materials Synthesis and Processing, Wuhan University of Technology – sequence: 4 givenname: Bowen surname: Jiang fullname: Jiang, Bowen email: swedenjiang@whut.edu.cn organization: State Key Laboratory of Advanced Technology for Materials Synthesis and Processing, Wuhan University of Technology – sequence: 5 givenname: Qizhong surname: Li fullname: Li, Qizhong email: lqzho@ncist.edu.cn organization: North China Institute of Science and Technology
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Snippet	In this paper, zirconium-based MOF (Zr-MOFs) materials, namely UIO-66, UIO-66-NH 2 , GMA-UIO-66 and NB-UIO-66, were selected as fillers to enhance the... In this paper, zirconium-based MOF (Zr-MOFs) materials, namely UIO-66, UIO-66-NH2, GMA-UIO-66 and NB-UIO-66, were selected as fillers to enhance the mechanical...
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SubjectTerms	Bend strength Chemistry Chemistry and Materials Science Field emission microscopy Flexural strength Fourier transforms Functional groups Impact strength Inorganic Chemistry Mechanical properties Modulus of rupture in bending Nanocomposites Organic Chemistry Polymer Sciences Toughness Zirconium
Title	The Functionalized UiO-66 Engineering for the Synergistic Enhancement of Mechanical Properties of Polydicyclopentadiene Nanocomposites
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