Thermoelectric Properties of Cu2Se Compound Fabricated at Low-Temperature Combustion Synthesis as a New Approach with Alternative Techniques
This article report the combustion synthesis of a Cu 2 Se thermoelectric intermetallic compound via spark plasma sintering (SPS). The elemental copper and selenium powder mixture makes a combustion reaction at ~ 130°C during spark plasma-assisted heating. The applied load and combustion reaction tog...
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| Published in | Journal of electronic materials Vol. 52; no. 3; pp. 2168 - 2176 |
|---|---|
| Main Authors | , |
| Format | Journal Article |
| Language | English |
| Published |
New York
Springer US
01.03.2023
Springer Nature B.V |
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| Abstract | This article report the combustion synthesis of a Cu
2
Se thermoelectric intermetallic compound via spark plasma sintering (SPS). The elemental copper and selenium powder mixture makes a combustion reaction at ~ 130°C during spark plasma-assisted heating. The applied load and combustion reaction together facilitate the densification of the reacted compound to a relative density of 88%. The x-ray diffractometer (XRD) data of the as-sintered bulk reacted compound confirms the formation of
α
-Cu
2
Se and
β
-Cu
2
Se compounds. On further short annealing at 350°C for 10 min, the
β
-Cu
2
Se transforms to
α
-Cu
2
Se and a complete monoclinic
α
-Cu
2
Se phase is obtained in the compound. The highest figure-of-merit (ZT) value of 0.61 at 650 K was achieved. This low-temperature sintering approach helps to overcome the issue of copper ion migration during SPS, and hence the chemical homogeneity is ascertained throughout the compound. The thermoelectric properties were compared with the Cu
2
Se material synthesized from other routes and found a superior ZT value than material prepared from solvothermal synthesis, mechanical alloying and hydrothermal-hot press techniques.
Graphical Abstract |
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| AbstractList | This article report the combustion synthesis of a Cu2Se thermoelectric intermetallic compound via spark plasma sintering (SPS). The elemental copper and selenium powder mixture makes a combustion reaction at ~ 130°C during spark plasma-assisted heating. The applied load and combustion reaction together facilitate the densification of the reacted compound to a relative density of 88%. The x-ray diffractometer (XRD) data of the as-sintered bulk reacted compound confirms the formation of α-Cu2Se and β-Cu2Se compounds. On further short annealing at 350°C for 10 min, the β-Cu2Se transforms to α-Cu2Se and a complete monoclinic α-Cu2Se phase is obtained in the compound. The highest figure-of-merit (ZT) value of 0.61 at 650 K was achieved. This low-temperature sintering approach helps to overcome the issue of copper ion migration during SPS, and hence the chemical homogeneity is ascertained throughout the compound. The thermoelectric properties were compared with the Cu2Se material synthesized from other routes and found a superior ZT value than material prepared from solvothermal synthesis, mechanical alloying and hydrothermal-hot press techniques. This article report the combustion synthesis of a Cu 2 Se thermoelectric intermetallic compound via spark plasma sintering (SPS). The elemental copper and selenium powder mixture makes a combustion reaction at ~ 130°C during spark plasma-assisted heating. The applied load and combustion reaction together facilitate the densification of the reacted compound to a relative density of 88%. The x-ray diffractometer (XRD) data of the as-sintered bulk reacted compound confirms the formation of α -Cu 2 Se and β -Cu 2 Se compounds. On further short annealing at 350°C for 10 min, the β -Cu 2 Se transforms to α -Cu 2 Se and a complete monoclinic α -Cu 2 Se phase is obtained in the compound. The highest figure-of-merit (ZT) value of 0.61 at 650 K was achieved. This low-temperature sintering approach helps to overcome the issue of copper ion migration during SPS, and hence the chemical homogeneity is ascertained throughout the compound. The thermoelectric properties were compared with the Cu 2 Se material synthesized from other routes and found a superior ZT value than material prepared from solvothermal synthesis, mechanical alloying and hydrothermal-hot press techniques. Graphical Abstract |
| Author | Kumaran, S. Thangavel, N. |
| Author_xml | – sequence: 1 givenname: N. surname: Thangavel fullname: Thangavel, N. organization: Green Energy Materials and Manufacturing Research Group, Department of Metallurgical and Materials Engineering, National Institute of Technology – sequence: 2 givenname: S. surname: Kumaran fullname: Kumaran, S. email: kumara@nitt.edu organization: Green Energy Materials and Manufacturing Research Group, Department of Metallurgical and Materials Engineering, National Institute of Technology |
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| Keywords | thermoelectric phase transition spark plasma sintering Combustion reaction |
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| Snippet | This article report the combustion synthesis of a Cu
2
Se thermoelectric intermetallic compound via spark plasma sintering (SPS). The elemental copper and... This article report the combustion synthesis of a Cu2Se thermoelectric intermetallic compound via spark plasma sintering (SPS). The elemental copper and... |
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| SubjectTerms | Characterization and Evaluation of Materials Chemistry and Materials Science Combustion synthesis Copper selenides Densification Electronics and Microelectronics Homogeneity Instrumentation Intermetallic compounds Ion migration Low temperature Materials Science Mechanical alloying Optical and Electronic Materials Original Research Article Plasma sintering Selenium Sintering (powder metallurgy) Solid State Physics Spark plasma sintering Specific gravity Thermoelectricity |
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| Title | Thermoelectric Properties of Cu2Se Compound Fabricated at Low-Temperature Combustion Synthesis as a New Approach with Alternative Techniques |
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