Microwave heating assisted synthesis of novel SnSe/g-C3N4 composites for effective photocatalytic H2 production
[Display omitted] •SnSe/g-C3N4 was prepared in 35min via a microwave heating method.•The spontaneous dispersion of SnSe on g-C3N4 during heating process was observed.•SnSe/g-C3N4 presented much better performance in H2 evolution than g-C3N4.•The enhanced charge separation was the key factor of the h...
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Published in | Journal of industrial and engineering chemistry (Seoul, Korea) Vol. 80; pp. 74 - 82 |
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Main Authors | , , , , , , , , |
Format | Journal Article |
Language | English |
Published |
Elsevier B.V
25.12.2019
한국공업화학회 |
Subjects | |
Online Access | Get full text |
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Abstract | [Display omitted]
•SnSe/g-C3N4 was prepared in 35min via a microwave heating method.•The spontaneous dispersion of SnSe on g-C3N4 during heating process was observed.•SnSe/g-C3N4 presented much better performance in H2 evolution than g-C3N4.•The enhanced charge separation was the key factor of the high photoactivity.
Novel SnSe/g-C3N4 photocatalysts were one-step synthesized via a microwave heating assisted process in 35min with SnSe and melamine as precursors. The as-synthesized SnSe/g-C3N4 worked very well in H2 evolution via photocatalysis. Under simulated sunlight, the best SnSe/g-C3N4 sample displayed a H2-production velocity of 1064μmolg−1h−1, which is 1.8 folds faster than that of neat g-C3N4. Similar promotion effect was also observed under visible light. To reveal the nature behind the high photoactivity, a thorough investigation was performed. XRD and XPS experiments proved the binary constitution of the composite. DRS experiment demonstrated that the addition of SnSe improved the photoabsorption performance. N2-adsorption analysis showed that the SnSe/g-C3N4 photocatalyst presented similar surface area as g-C3N4. TEM experiments showed that some bulk SnSe were spontaneously decomposed to nanoparticles and finely dispersed in g-C3N4 during the microwave heating process. These SnSe nanoparticles were believed to be the active phase and constructed a heterojunction structure with g-C3N4, resulting in the enhanced charge separation. This conclusion was considered as the key factor leading to the high H2-evolution performance and was further confirmed by the PL, EIS, and PC experiments. The present work provides a feasible and rapid method for the construction of g-C3N4 based photocatalysts. |
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AbstractList | Novel SnSe/g-C3N4 photocatalysts were one-step synthesized via a microwave heating assisted process in35 min with SnSe and melamine as precursors. The as-synthesized SnSe/g-C3N4 worked very well in H2evolution via photocatalysis. Under simulated sunlight, the best SnSe/g-C3N4 sample displayed a H2-production velocity of 1064 mmol g 1 h 1, which is 1.8 folds faster than that of neat g-C3N4. Similarpromotion effect was also observed under visible light. To reveal the nature behind the highphotoactivity, a thorough investigation was performed. XRD and XPS experiments proved the binaryconstitution of the composite. DRS experiment demonstrated that the addition of SnSe improved thephotoabsorption performance. N2-adsorption analysis showed that the SnSe/g-C3N4 photocatalystpresented similar surface area as g-C3N4. TEM experiments showed that some bulk SnSe werespontaneously decomposed to nanoparticles andfinely dispersed in g-C3N4 during the microwaveheating process. These SnSe nanoparticles were believed to be the active phase and constructed aheterojunction structure with g-C3N4, resulting in the enhanced charge separation. This conclusion wasconsidered as the key factor leading to the high H2-evolution performance and was further confirmed bythe PL, EIS, and PC experiments. The present work provides a feasible and rapid method for theconstruction of g-C3N4 based photocatalysts. KCI Citation Count: 1 [Display omitted] •SnSe/g-C3N4 was prepared in 35min via a microwave heating method.•The spontaneous dispersion of SnSe on g-C3N4 during heating process was observed.•SnSe/g-C3N4 presented much better performance in H2 evolution than g-C3N4.•The enhanced charge separation was the key factor of the high photoactivity. Novel SnSe/g-C3N4 photocatalysts were one-step synthesized via a microwave heating assisted process in 35min with SnSe and melamine as precursors. The as-synthesized SnSe/g-C3N4 worked very well in H2 evolution via photocatalysis. Under simulated sunlight, the best SnSe/g-C3N4 sample displayed a H2-production velocity of 1064μmolg−1h−1, which is 1.8 folds faster than that of neat g-C3N4. Similar promotion effect was also observed under visible light. To reveal the nature behind the high photoactivity, a thorough investigation was performed. XRD and XPS experiments proved the binary constitution of the composite. DRS experiment demonstrated that the addition of SnSe improved the photoabsorption performance. N2-adsorption analysis showed that the SnSe/g-C3N4 photocatalyst presented similar surface area as g-C3N4. TEM experiments showed that some bulk SnSe were spontaneously decomposed to nanoparticles and finely dispersed in g-C3N4 during the microwave heating process. These SnSe nanoparticles were believed to be the active phase and constructed a heterojunction structure with g-C3N4, resulting in the enhanced charge separation. This conclusion was considered as the key factor leading to the high H2-evolution performance and was further confirmed by the PL, EIS, and PC experiments. The present work provides a feasible and rapid method for the construction of g-C3N4 based photocatalysts. |
Author | Zhao, Xinyue Si, Jianxiao Zhang, Qingle Dai, Xiaoquan Chen, Pengfei He, Yiming Xing, Pingxing Ge, Shifeng Zhao, Leihong |
Author_xml | – sequence: 1 givenname: Pengfei surname: Chen fullname: Chen, Pengfei organization: Department of Materials Science and Engineering, Zhejiang Normal University, Jinhua 321004, China – sequence: 2 givenname: Xiaoquan surname: Dai fullname: Dai, Xiaoquan organization: Department of Materials Science and Engineering, Zhejiang Normal University, Jinhua 321004, China – sequence: 3 givenname: Pingxing surname: Xing fullname: Xing, Pingxing organization: Department of Materials Science and Engineering, Zhejiang Normal University, Jinhua 321004, China – sequence: 4 givenname: Xinyue surname: Zhao fullname: Zhao, Xinyue organization: Department of Materials Science and Engineering, Zhejiang Normal University, Jinhua 321004, China – sequence: 5 givenname: Qingle surname: Zhang fullname: Zhang, Qingle organization: Department of Materials Science and Engineering, Zhejiang Normal University, Jinhua 321004, China – sequence: 6 givenname: Shifeng surname: Ge fullname: Ge, Shifeng organization: Department of Materials Science and Engineering, Zhejiang Normal University, Jinhua 321004, China – sequence: 7 givenname: Jianxiao surname: Si fullname: Si, Jianxiao organization: Department of Materials Science and Engineering, Zhejiang Normal University, Jinhua 321004, China – sequence: 8 givenname: Leihong surname: Zhao fullname: Zhao, Leihong organization: Key Laboratory of the Ministry of Education for Advanced Catalysis Materials, Institute of Physical Chemistry, Zhejiang Normal University, Jinhua 321004, China – sequence: 9 givenname: Yiming orcidid: 0000-0002-1919-0719 surname: He fullname: He, Yiming email: hym@zjnu.cn organization: Department of Materials Science and Engineering, Zhejiang Normal University, Jinhua 321004, China |
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•SnSe/g-C3N4 was prepared in 35min via a microwave heating method.•The spontaneous dispersion of SnSe on g-C3N4 during heating process was... Novel SnSe/g-C3N4 photocatalysts were one-step synthesized via a microwave heating assisted process in35 min with SnSe and melamine as precursors. The... |
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SubjectTerms | g-C3N4 H2 production Microwave heating Photocatalysis SnSe 화학공학 |
Title | Microwave heating assisted synthesis of novel SnSe/g-C3N4 composites for effective photocatalytic H2 production |
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