Electrically detected electron nuclear double resonance in amorphous hydrogenated boron thin films
We report on electrically detected electron nuclear double resonance (EDENDOR) observations via spin dependent trap assisted tunneling (SDTAT) in amorphous boron thin films at 250 K. We observe EDENDOR from both 10B and 11B nuclei, likely interacting with carbon impurities. In SDTAT, electron parama...
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| Published in | Solid state communications Vol. 353; p. 114846 |
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| Main Authors | , , |
| Format | Journal Article |
| Language | English |
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Elsevier Ltd
15.09.2022
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| Online Access | Get full text |
| ISSN | 0038-1098 1879-2766 |
| DOI | 10.1016/j.ssc.2022.114846 |
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| Abstract | We report on electrically detected electron nuclear double resonance (EDENDOR) observations via spin dependent trap assisted tunneling (SDTAT) in amorphous boron thin films at 250 K. We observe EDENDOR from both 10B and 11B nuclei, likely interacting with carbon impurities. In SDTAT, electron paramagnetic resonance (EPR) is detected through a change in the trap assisted tunneling current through the thin film. As in conventional electron nuclear double resonance (ENDOR) the ENDOR response is detected through a modest change in the EPR response. Since SDTAT detection sensitivity is about seven orders of magnitude greater than that of conventional EPR, it, in principle, can provide an enormous boost in ENDOR sensitivity. This enormous potential sensitivity improvement can be compromised by a coupling of the RF electromagnetic field driving the nuclear spin response and the electrical leads which are utilized to monitor the resonance induced changes in device current. We overcome this difficulty with the introduction of proportional-integral-derivative (PID) control of the RF circuitry which greatly suppresses fluctuations in the amplitude of the RF magnetic field at the thin film structure under investigation.
•Electrical detection of 10B and 11B nuclei via electron nuclear double resonance.•Electrically detected electron nuclear double resonance in a complex spin system.•Proportional-integral-derivative controller for nuclear frequency power smoothing. |
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| AbstractList | We report on electrically detected electron nuclear double resonance (EDENDOR) observations via spin dependent trap assisted tunneling (SDTAT) in amorphous boron thin films at 250 K. We observe EDENDOR from both 10B and 11B nuclei, likely interacting with carbon impurities. In SDTAT, electron paramagnetic resonance (EPR) is detected through a change in the trap assisted tunneling current through the thin film. As in conventional electron nuclear double resonance (ENDOR) the ENDOR response is detected through a modest change in the EPR response. Since SDTAT detection sensitivity is about seven orders of magnitude greater than that of conventional EPR, it, in principle, can provide an enormous boost in ENDOR sensitivity. This enormous potential sensitivity improvement can be compromised by a coupling of the RF electromagnetic field driving the nuclear spin response and the electrical leads which are utilized to monitor the resonance induced changes in device current. We overcome this difficulty with the introduction of proportional-integral-derivative (PID) control of the RF circuitry which greatly suppresses fluctuations in the amplitude of the RF magnetic field at the thin film structure under investigation.
•Electrical detection of 10B and 11B nuclei via electron nuclear double resonance.•Electrically detected electron nuclear double resonance in a complex spin system.•Proportional-integral-derivative controller for nuclear frequency power smoothing. |
| ArticleNumber | 114846 |
| Author | Myers, Kenneth J. Manning, Brian Lenahan, Patrick M. |
| Author_xml | – sequence: 1 givenname: Kenneth J. orcidid: 0000-0002-2015-0925 surname: Myers fullname: Myers, Kenneth J. email: k.j.myers5579@gmail.com organization: Intercollege Graduate Degree Program in Materials Science and Engineering, The Pennsylvania State University, 101 Earth and Engineering Sciences Building, University Park, PA, 16802, USA – sequence: 2 givenname: Brian surname: Manning fullname: Manning, Brian organization: High Frequency Technology Center, Keysight Technologies, 1400 Fountaingrove Pkwy, Santa Rosa, CA, 95403, USA – sequence: 3 givenname: Patrick M. surname: Lenahan fullname: Lenahan, Patrick M. organization: Department of Engineering Science and Mechanics, The Pennsylvania State University, 101 Earth and Engineering Sciences Building, University Park, PA, 16802, USA |
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| Cites_doi | 10.1063/1.115726 10.1103/PhysRevB.11.2370 10.4028/www.scientific.net/MSF.1004.306 10.4028/www.scientific.net/MSF.143-147.63 10.1063/1.5123619 10.1063/1.5108961 10.1016/S0022-3093(99)00871-6 10.1063/1.5123600 10.1103/PhysRevLett.106.187601 10.1103/PhysRevB.6.436 10.1143/JJAP.40.2840 10.1016/S0022-3093(99)00578-5 10.1103/PhysRevB.98.155203 10.1063/5.0041059 10.1016/0022-5088(79)90086-9 10.1063/1.3482071 10.1063/1.115900 10.1109/TNS.2019.2958351 10.1051/jphyslet:0197800390405100 10.1016/0022-5088(79)90099-7 10.1063/1.4942675 10.1103/PhysRevB.81.161203 10.1149/2.007206jss 10.1103/PhysRevB.54.7957 10.1016/S0022-3093(98)00073-8 |
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| Title | Electrically detected electron nuclear double resonance in amorphous hydrogenated boron thin films |
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