Urea-H2O2 defect engineering of δ-MnO2 for propane photothermal oxidation: Structure-activity relationship and synergetic mechanism determination
[Display omitted] •MnO2 treated by urea-H2O2 exhibits great photocatalytic propane oxidation activity.•H2O2 treatment increase active sites to thermal catalytic performance.•The photocatalytic performance improvement is related to photogenerated electrons.•A new photothermal synergetic catalysis mec...
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Published in | Journal of colloid and interface science Vol. 641; pp. 48 - 58 |
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Main Authors | , , , , , , , , , , , |
Format | Journal Article |
Language | English |
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Elsevier Inc
01.07.2023
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Abstract | [Display omitted]
•MnO2 treated by urea-H2O2 exhibits great photocatalytic propane oxidation activity.•H2O2 treatment increase active sites to thermal catalytic performance.•The photocatalytic performance improvement is related to photogenerated electrons.•A new photothermal synergetic catalysis mechanism was proposed.
Photothermal catalysis has an advantage in effective and economical elimination technology of volatile organic compounds (VOCs) in the ascendant. Herein, various surface defect engineering routes were adopted to enhance the low-temperature propane oxidation of δ-MnO2. Compared to reducing etchants urea and vitamin C, δ-MnO2 treated with urea - H2O2 exhibited an excellent thermal (T90 = 240 ℃) and photothermal (T90 = 196 ℃) activities of propane oxidation. Urea - H2O2 treatment provided high concentration of Mn4+ and surface-active oxygen (Mn4+-Osur) species as surface-active sites, and produced numerous oxygen vacancies to improve charge separation and superoxide species generation capacity. Thus, the photothermal conversion efficiency and low-temperature reducibility were remarkably enhanced. Furthermore, the photothermal synergistic catalytic mechanism was proposed based on in-situ diffuse reflectance infrared Fourier transform spectroscopy and control experiments. The strategy here offered insight into the rational design of efficient transition catalysts, and in-depth understanding of the photothermal catalytic VOCs removal mechanism. |
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AbstractList | [Display omitted]
•MnO2 treated by urea-H2O2 exhibits great photocatalytic propane oxidation activity.•H2O2 treatment increase active sites to thermal catalytic performance.•The photocatalytic performance improvement is related to photogenerated electrons.•A new photothermal synergetic catalysis mechanism was proposed.
Photothermal catalysis has an advantage in effective and economical elimination technology of volatile organic compounds (VOCs) in the ascendant. Herein, various surface defect engineering routes were adopted to enhance the low-temperature propane oxidation of δ-MnO2. Compared to reducing etchants urea and vitamin C, δ-MnO2 treated with urea - H2O2 exhibited an excellent thermal (T90 = 240 ℃) and photothermal (T90 = 196 ℃) activities of propane oxidation. Urea - H2O2 treatment provided high concentration of Mn4+ and surface-active oxygen (Mn4+-Osur) species as surface-active sites, and produced numerous oxygen vacancies to improve charge separation and superoxide species generation capacity. Thus, the photothermal conversion efficiency and low-temperature reducibility were remarkably enhanced. Furthermore, the photothermal synergistic catalytic mechanism was proposed based on in-situ diffuse reflectance infrared Fourier transform spectroscopy and control experiments. The strategy here offered insight into the rational design of efficient transition catalysts, and in-depth understanding of the photothermal catalytic VOCs removal mechanism. |
Author | Chen, Chong Li, Xuebing Li, Shuangju Zhang, Runduo Bi, Yuxi Wang, Zhong Liu, Yunqi Pan, Yuan Liu, Fang Feng, Chao Xin, Hongchuan Lu, Yukun |
Author_xml | – sequence: 1 givenname: Chao surname: Feng fullname: Feng, Chao organization: Key Laboratory of Biofuels, Qingdao Institute of Bioenergy and Bioprocess Technology, Chinese Academy of Sciences, Qingdao 266101, China – sequence: 2 givenname: Yuxi surname: Bi fullname: Bi, Yuxi organization: State Key Laboratory of Heavy Oil Processing, College of Chemical Engineering, China University of Petroleum, Qingdao 266580, China – sequence: 3 givenname: Chong surname: Chen fullname: Chen, Chong organization: State Key Laboratory of Heavy Oil Processing, College of Chemical Engineering, China University of Petroleum, Qingdao 266580, China – sequence: 4 givenname: Shuangju surname: Li fullname: Li, Shuangju organization: Key Laboratory of Biofuels, Qingdao Institute of Bioenergy and Bioprocess Technology, Chinese Academy of Sciences, Qingdao 266101, China – sequence: 5 givenname: Zhong surname: Wang fullname: Wang, Zhong organization: Key Laboratory of Biofuels, Qingdao Institute of Bioenergy and Bioprocess Technology, Chinese Academy of Sciences, Qingdao 266101, China – sequence: 6 givenname: Hongchuan surname: Xin fullname: Xin, Hongchuan organization: Key Laboratory of Biofuels, Qingdao Institute of Bioenergy and Bioprocess Technology, Chinese Academy of Sciences, Qingdao 266101, China – sequence: 7 givenname: Yuan surname: Pan fullname: Pan, Yuan organization: State Key Laboratory of Heavy Oil Processing, College of Chemical Engineering, China University of Petroleum, Qingdao 266580, China – sequence: 8 givenname: Fang surname: Liu fullname: Liu, Fang organization: State Key Laboratory of Heavy Oil Processing, College of Chemical Engineering, China University of Petroleum, Qingdao 266580, China – sequence: 9 givenname: Yukun surname: Lu fullname: Lu, Yukun organization: State Key Laboratory of Heavy Oil Processing, College of Chemical Engineering, China University of Petroleum, Qingdao 266580, China – sequence: 10 givenname: Yunqi surname: Liu fullname: Liu, Yunqi email: liuyq@upc.edu.cn organization: State Key Laboratory of Heavy Oil Processing, College of Chemical Engineering, China University of Petroleum, Qingdao 266580, China – sequence: 11 givenname: Runduo surname: Zhang fullname: Zhang, Runduo organization: State Key Laboratory of Chemical Resource Engineering, Beijing Key Laboratory of Energy Environmental Catalysis, Beijing University of Chemical Technology, Beijing 100029, China – sequence: 12 givenname: Xuebing surname: Li fullname: Li, Xuebing email: Lixb@qibebt.ac.cn organization: Key Laboratory of Biofuels, Qingdao Institute of Bioenergy and Bioprocess Technology, Chinese Academy of Sciences, Qingdao 266101, China |
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•MnO2 treated by urea-H2O2 exhibits great photocatalytic propane oxidation activity.•H2O2 treatment increase active sites to thermal... |
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SubjectTerms | Defect engineering Photothermal catalysis Propane oxidation Reaction mechanism δ-MnO2 |
Title | Urea-H2O2 defect engineering of δ-MnO2 for propane photothermal oxidation: Structure-activity relationship and synergetic mechanism determination |
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