Controlled synthesis and luminescence properties of doped NaLa(WO4)2 microstructures

In this work, well-defined NaLa(WO4)2 microstructures were prepared by a facile hydrothermal process in the presence of oleylamine and oleic acid as a mixed surfactant. The phase, morphology, size and luminescence properties were well characterized by means of X-ray diffraction (XRD), scanning elect...

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Published inJournal of industrial and engineering chemistry (Seoul, Korea) Vol. 34; pp. 269 - 277
Main Authors Han, Yunhua, Wang, Yan, Huang, Shaohua, Jin, Fan-Long, Gai, Shili, Niu, Na, Wang, Liuzhen, Yang, Piaoping
Format Journal Article
LanguageEnglish
Published Elsevier B.V 25.02.2016
한국공업화학회
Subjects
Down-conversion luminescence
Hydrothermal
NaLa(WO4)2
Up-conversion luminescence
화학공학
NaLa(WO4)2
Down-conversion luminescence
Up-conversion luminescence
Hydrothermal
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Abstract In this work, well-defined NaLa(WO4)2 microstructures were prepared by a facile hydrothermal process in the presence of oleylamine and oleic acid as a mixed surfactant. The phase, morphology, size and luminescence properties were well characterized by means of X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), photoluminescence (PL) spectra, and decay time, respectively. The results reveal that the morphology and size of the as-synthesized samples can be tuned by altering the reaction time and the amounts of oleic acid. A possible formation mechanism of tetragonal NaLa(WO4)2 is proposed on the basis of oleic acid amount-dependent experiments. Upon ultraviolet (UV) excitation, NaLa(WO4)2:Eu3+ and NaLa(WO4)2:Tb3+ exhibit the characteristic down-conversion emissions of Eu3+ and Tb3+. Yb3+/Er3+ and Yb3+/Tm3+ co-doped NaLa(WO4)2 samples show strong green (Er3+, 4S3/2, 2H11/2→4I15/2) and blue (Tm3+, 1G4→3H6) up-conversion emission under 980nm laser diode excitation. Upconversion emission mechanisms of NaLa(WO4)2:Ln (Ln=Yb/Er, Yb/Tm) are also presented based on the emission spectra and the plot of luminescence intensity to pump power. It should be noted that the intensity of the upconversion emissions can be dramatically enhanced compared with sodium free tungstates, which can be attributed to the charge compensation and means the introduction of Na+ ions in WO42− causes less distortion in the crystal structure.
AbstractList In this work, well-defined NaLa(WO4)2microstructures were prepared by a facile hydrothermal processin the presence of oleylamine and oleic acid as a mixed surfactant. The phase, morphology, size andluminescence properties were well characterized by means of X-ray diffraction (XRD), scanning electronmicroscopy (SEM), transmission electron microscopy (TEM), photoluminescence (PL) spectra, and decaytime, respectively. The results reveal that the morphology and size of the as-synthesized samples can betuned by altering the reaction time and the amounts of oleic acid. A possible formation mechanism oftetragonal NaLa(WO4)2 is proposed on the basis of oleic acid amount-dependent experiments. Uponultraviolet (UV) excitation, NaLa(WO4)2:Eu3+ and NaLa(WO4)2:Tb3+ exhibit the characteristic downconversionemissions of Eu3+ and Tb3+. Yb3+/Er3+ and Yb3+/Tm3+ co-doped NaLa(WO4)2 samples showstrong green (Er3+, 4S3/2, 2H11/2!4I15/2) and blue (Tm3+, 1G4!3H6) up-conversion emission under980 nm laser diode excitation. Upconversion emission mechanisms of NaLa(WO4)2:Ln (Ln = Yb/Er, Yb/Tm) are also presented based on the emission spectra and the plot of luminescence intensity to pumppower. It should be noted that the intensity of the upconversion emissions can be dramatically enhancedcompared with sodium free tungstates, which can be attributed to the charge compensation and meansthe introduction of Na+ ions in WO42 causes less distortion in the crystal structure. KCI Citation Count: 16
In this work, well-defined NaLa(WO4)2 microstructures were prepared by a facile hydrothermal process in the presence of oleylamine and oleic acid as a mixed surfactant. The phase, morphology, size and luminescence properties were well characterized by means of X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), photoluminescence (PL) spectra, and decay time, respectively. The results reveal that the morphology and size of the as-synthesized samples can be tuned by altering the reaction time and the amounts of oleic acid. A possible formation mechanism of tetragonal NaLa(WO4)2 is proposed on the basis of oleic acid amount-dependent experiments. Upon ultraviolet (UV) excitation, NaLa(WO4)2:Eu3+ and NaLa(WO4)2:Tb3+ exhibit the characteristic down-conversion emissions of Eu3+ and Tb3+. Yb3+/Er3+ and Yb3+/Tm3+ co-doped NaLa(WO4)2 samples show strong green (Er3+, 4S3/2, 2H11/2→4I15/2) and blue (Tm3+, 1G4→3H6) up-conversion emission under 980nm laser diode excitation. Upconversion emission mechanisms of NaLa(WO4)2:Ln (Ln=Yb/Er, Yb/Tm) are also presented based on the emission spectra and the plot of luminescence intensity to pump power. It should be noted that the intensity of the upconversion emissions can be dramatically enhanced compared with sodium free tungstates, which can be attributed to the charge compensation and means the introduction of Na+ ions in WO42− causes less distortion in the crystal structure.
Author Huang, Shaohua
Han, Yunhua
Yang, Piaoping
Jin, Fan-Long
Gai, Shili
Niu, Na
Wang, Liuzhen
Wang, Yan
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Keywords NaLa(WO4)2
Down-conversion luminescence
Up-conversion luminescence
Hydrothermal
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한국공업화학회
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SSID ssj0060386
ssib009049966
Score 2.2134702
Snippet In this work, well-defined NaLa(WO4)2 microstructures were prepared by a facile hydrothermal process in the presence of oleylamine and oleic acid as a mixed...
In this work, well-defined NaLa(WO4)2microstructures were prepared by a facile hydrothermal processin the presence of oleylamine and oleic acid as a mixed...
SourceID nrf
crossref
elsevier
SourceType Open Website
Aggregation Database
Publisher
StartPage 269
SubjectTerms Down-conversion luminescence
Hydrothermal
NaLa(WO4)2
Up-conversion luminescence
화학공학
Title Controlled synthesis and luminescence properties of doped NaLa(WO4)2 microstructures
URI https://dx.doi.org/10.1016/j.jiec.2015.11.021
https://www.kci.go.kr/kciportal/ci/sereArticleSearch/ciSereArtiView.kci?sereArticleSearchBean.artiId=ART002079737
Volume 34
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ispartofPNX Journal of Industrial and Engineering Chemistry, 2016, 34(0), , pp.269-277
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