Dissolution Behavior of Silver Anode in Cyanide Free Bath
The cyanide-free silver plating bath that we developed produced good silver film, but the cell voltage of the bath increased over time if electrodeposition was conducted continuously. Green film also formed on the silver anode with increasing voltage. To clarify these phenomena, we studied the anodi...
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| Published in | Hyōmen gijutsu Vol. 49; no. 3; pp. 320 - 322 |
|---|---|
| Main Authors | , , , |
| Format | Journal Article |
| Language | English Japanese |
| Published |
Tokyo
The Surface Finishing Society of Japan
01.03.1998
Japan Science and Technology Agency |
| Subjects | |
| Online Access | Get full text |
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| Abstract | The cyanide-free silver plating bath that we developed produced good silver film, but the cell voltage of the bath increased over time if electrodeposition was conducted continuously. Green film also formed on the silver anode with increasing voltage. To clarify these phenomena, we studied the anodic polarization behavior of the silver electrode in the cyanide-free bath. The X-ray diffraction pattern for the green film agreed with that of AgI. Anodic polarization curves for the silver electrode indicated that less-conductive film formed on the electrode when the potential exceeded-0.3V. The polarization curve limiting current was increased by agitating the bath or increasing KI concentration. These results iudicate that Ag was dissolved into the solution via AgI rather than dissolving directly into the bath. |
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| AbstractList | The cyanide-free silver plating bath that we developed produced good silver film, but the cell voltage of the bath increased over time if electrodeposition was conducted continuously. Green film also formed on the Ag anode with increasing voltage. To clarify these phenomena, we studied the anodic polarization behavior of the Ag electrode in the cyanide-free bath. The x-ray diffraction pattern for the green film agreed with that of AgI. Anodic polarization curves for the Ag electrode indicated that less-conductive film formed on the electrode when the potential exceeded -0.3 V. The polarization curve limiting current was increased by agitating the bath or increasing KI concentration. These results indicate that Ag was dissolved into the solution via AgI rather than dissolving directly into the bath. The cyanide-free silver plating bath that we developed produced good silver film, but the cell voltage of the bath increased over time if electrodeposition was conducted continuously. Green film also formed on the silver anode with increasing voltage. To clarify these phenomena, we studied the anodic polarization behavior of the silver electrode in the cyanide-free bath. The X-ray diffraction pattern for the green film agreed with that of AgI. Anodic polarization curves for the silver electrode indicated that less-conductive film formed on the electrode when the potential exceeded-0.3V. The polarization curve limiting current was increased by agitating the bath or increasing KI concentration. These results iudicate that Ag was dissolved into the solution via AgI rather than dissolving directly into the bath. |
| Author | MASAKI, Seishi KONDO, Tetsuya INOUE, Hiroyuki HONMA, Hideo |
| Author_xml | – sequence: 1 fullname: MASAKI, Seishi organization: Daiwa Fine Chemicals Co., Ltd – sequence: 2 fullname: KONDO, Tetsuya organization: Daiwa Fine Chemicals Co., Ltd – sequence: 3 fullname: INOUE, Hiroyuki organization: College of Eng. Osaka Pref. Univ – sequence: 4 fullname: HONMA, Hideo organization: Fac. of Eng., Kanto Gakuin Univ |
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| References | 2) 井上博之, 山川宏二, 正木征史; 表面技術, 43, 478 (1992 3) 井上博之, 山川宏二, 正木征史; 表面技術, 44, 55 (1993 4) 正木征史, 吉本雅一, 井上博之, 本間英夫; 表面技術, 49, 84 (1998 1) 近藤哲也, 正木征史, 井上博之, 山川宏二; 表面技術, 42, 241 (1991 5) 正木征史, 吉本雅一, 田中恵美子, 井上博之, 本間英夫; 表面技術, 49, 201 (1998 |
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| SubjectTerms | Anodic Dissolution Cyanide Free Silver Electroplating |
| Title | Dissolution Behavior of Silver Anode in Cyanide Free Bath |
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