Pallado-catalysed P-arylations and P-vinylation of 2-hydrogeno-2-oxo-1,4,2-oxazaphosphinanes
A simple and effective preparation of 2-aryl- (or 2-vinyl)-1,4,2-oxazaphosphinanes, phosphorus analogues of aryl-morpholinols has been developed, involving palladium catalysed coupling of aryl (or vinyl)-halides with 2- H-1,4,2-oxazaphosphinane in presence of triethylamine. A deprotection step was a...
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| Published in | Tetrahedron Vol. 61; no. 29; pp. 7029 - 7036 |
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| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
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| Abstract | A simple and effective preparation of 2-aryl- (or 2-vinyl)-1,4,2-oxazaphosphinanes, phosphorus analogues of aryl-morpholinols has been developed, involving palladium catalysed coupling of aryl (or vinyl)-halides with 2-
H-1,4,2-oxazaphosphinane in presence of triethylamine. A deprotection step was also proposed to afford the corresponding
P-aryl-α-aminobenzylphosphinic acid.
A simple and effective preparation of 2-aryl- (or 2-vinyl)-1,4,2-oxazaphosphinanes, phosphorus analogues of aryl-morpholinols has been developed, involving palladium catalysed coupling of aryl (or vinyl)-halides with 2-
H-1,4,2-oxazaphosphinane in presence of triethylamine. A deprotection step was also proposed to afford the corresponding
P-aryl-α-aminobenzylphosphinic acid. |
|---|---|
| AbstractList | A simple and effective preparation of 2-aryl- (or 2-vinyl)-1,4,2-oxazaphosphinanes, phosphorus analogues of aryl-morpholinols has been developed, involving palladium catalysed coupling of aryl (or vinyl)-halides with 2-
H-1,4,2-oxazaphosphinane in presence of triethylamine. A deprotection step was also proposed to afford the corresponding
P-aryl-α-aminobenzylphosphinic acid.
A simple and effective preparation of 2-aryl- (or 2-vinyl)-1,4,2-oxazaphosphinanes, phosphorus analogues of aryl-morpholinols has been developed, involving palladium catalysed coupling of aryl (or vinyl)-halides with 2-
H-1,4,2-oxazaphosphinane in presence of triethylamine. A deprotection step was also proposed to afford the corresponding
P-aryl-α-aminobenzylphosphinic acid. A simple and effective preparation of 2-aryl- (or 2-vinyl)-1,4,2-oxazaphosphinanes, phosphorus analogues of aryl-morpholinols has been developed, involving palladium catalysed coupling of aryl (or vinyl)-halides with 2-H-1,4,2-oxazaphosphinane in presence of triethylamine. A deprotection step was also proposed to afford the corresponding P-aryl-α-aminobenzylphosphinic acid |
| Author | Pirat, Jean-Luc Cristau, Henri-Jean Virieux, David Monbrun, Jérôme |
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| Keywords | Arylation Aminoalkylarylphosphinic acid Arylphosphinate Vinylation Pallado-catalyse |
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| Title | Pallado-catalysed P-arylations and P-vinylation of 2-hydrogeno-2-oxo-1,4,2-oxazaphosphinanes |
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