Synthesis and structural studies (1H, 13C, 31P NMR and X-ray) of new C-bonded cyclotriphosphazenes with heterocyclic substituents from novel phosphinic acid derivatives
Three new C-bonded cyclotriphosphazenes, [N3P3(2-thienyl)(6)], 2, [N3P3(3-thienyl)(6)], 4, and [N3P3(3,3'-bithienyl-2,2'- ylene)(3)], 6, have been prepared by two new synthetic procedures and are the first examples of non-spiro and trispirocyclotriphosphazene derivatives composed of thioph...
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| Published in | New journal of chemistry Vol. 28; no. 3; pp. 418 - 424 |
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| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
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Royal Soc Chemistry
01.01.2004
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| Abstract | Three new C-bonded cyclotriphosphazenes, [N3P3(2-thienyl)(6)], 2, [N3P3(3-thienyl)(6)], 4, and [N3P3(3,3'-bithienyl-2,2'- ylene)(3)], 6, have been prepared by two new synthetic procedures and are the first examples of non-spiro and trispirocyclotriphosphazene derivatives composed of thiophene and 3,3'-dithiophene substituents, respectively. Their H-1, C-13 and P-31 NMR parameters are given. The solid state structures of 2, 4 and 6 have been determined by X-ray crystallography. |
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| AbstractList | Three new C-bonded cyclotriphosphazenes, [N3P3(2-thienyl)(6)], 2, [N3P3(3-thienyl)(6)], 4, and [N3P3(3,3'-bithienyl-2,2'- ylene)(3)], 6, have been prepared by two new synthetic procedures and are the first examples of non-spiro and trispirocyclotriphosphazene derivatives composed of thiophene and 3,3'-dithiophene substituents, respectively. Their H-1, C-13 and P-31 NMR parameters are given. The solid state structures of 2, 4 and 6 have been determined by X-ray crystallography. |
| Author | Plénat, F Cristau, HJ Fruchier, A Combes-Chamalet, C Taillefer, M Scowen, IJ Vicente |
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| CitedBy_id | crossref_primary_10_1246_cl_2010_448 crossref_primary_10_1021_cr040179m crossref_primary_10_1021_acs_joc_8b00030 crossref_primary_10_1007_s10904_006_9013_3 crossref_primary_10_3987_COM_21_14540 crossref_primary_10_1039_C6CS00257A crossref_primary_10_1246_cl_190879 crossref_primary_10_1039_b819255n crossref_primary_10_1016_j_inoche_2017_04_030 crossref_primary_10_1021_acs_inorgchem_1c00054 |
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| Snippet | Three new C-bonded cyclotriphosphazenes, [N3P3(2-thienyl)(6)], 2, [N3P3(3-thienyl)(6)], 4, and [N3P3(3,3'-bithienyl-2,2'- ylene)(3)], 6, have been prepared by... |
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| SubjectTerms | Chemistry Chemistry, Multidisciplinary Physical Sciences Science & Technology |
| Title | Synthesis and structural studies (1H, 13C, 31P NMR and X-ray) of new C-bonded cyclotriphosphazenes with heterocyclic substituents from novel phosphinic acid derivatives |
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