High specific surface area carbon aerogel derived from starch for methylene blue adsorption and supercapacitors
Starch based carbon aerogel has attracted significant attention due to the wide source, environmental friendliness and low price of raw materials. Here, starch based carbon aerogel was fabricated by graft reaction and cross-linking reaction of starch. The network structure of starch hydrogel was opt...
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| Published in | International journal of biological macromolecules Vol. 274; no. Pt 1; p. 133282 |
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| Main Authors | , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Netherlands
Elsevier B.V
01.08.2024
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| Subjects | |
| Online Access | Get full text |
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| Abstract | Starch based carbon aerogel has attracted significant attention due to the wide source, environmental friendliness and low price of raw materials. Here, starch based carbon aerogel was fabricated by graft reaction and cross-linking reaction of starch. The network structure of starch hydrogel was optimized through graft and cross-linking reaction. After freeze drying and high temperature carbonization, the obtained carbon aerogel that carbonized at 800 °C showed a specific surface area of 1508 m2·g−1 without activation which is far higher than that of other unactivated carbon aerogels. The starch based carbon aerogel carbonized at 800 °C exhibited superior methylene blue adsorption ability with a maximum adsorption capacity of 963.5 mg·g−1 as a result of its rich surface functional groups, high specific surface area, and reasonable pore size distribution. Furthermore, the carbon aerogel carbonized at 700 °C exhibited excellent electrochemical performance with a specific capacitance of 180.1 F·g−1 at a current density of 1 A·g−1as electrode materials for supercapacitors. Overall, this work provides a new method to prepare high performance starch based carbon aerogel.
•Preparation of carbon aerogel using grafted and cross-linked starch hydrogel for the first time.•The specific surface area of the prepared carbon aerogel can reached 1508 m2/g without activation.•The starch-based carbon aerogel exhibited a maximum methylene blue adsorption capacity of 963.5 mg/g.•The starch-based carbon aerogel showed a specific capacitance of 180.1 F/g as electrode materials for supercapacitors. |
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| AbstractList | Starch based carbon aerogel has attracted significant attention due to the wide source, environmental friendliness and low price of raw materials. Here, starch based carbon aerogel was fabricated by graft reaction and cross-linking reaction of starch. The network structure of starch hydrogel was optimized through graft and cross-linking reaction. After freeze drying and high temperature carbonization, the obtained carbon aerogel that carbonized at 800 °C showed a specific surface area of 1508 m2·g-1 without activation which is far higher than that of other unactivated carbon aerogels. The starch based carbon aerogel carbonized at 800 °C exhibited superior methylene blue adsorption ability with a maximum adsorption capacity of 963.5 mg·g-1 as a result of its rich surface functional groups, high specific surface area, and reasonable pore size distribution. Furthermore, the carbon aerogel carbonized at 700 °C exhibited excellent electrochemical performance with a specific capacitance of 180.1 F·g-1 at a current density of 1 A·g-1as electrode materials for supercapacitors. Overall, this work provides a new method to prepare high performance starch based carbon aerogel.Starch based carbon aerogel has attracted significant attention due to the wide source, environmental friendliness and low price of raw materials. Here, starch based carbon aerogel was fabricated by graft reaction and cross-linking reaction of starch. The network structure of starch hydrogel was optimized through graft and cross-linking reaction. After freeze drying and high temperature carbonization, the obtained carbon aerogel that carbonized at 800 °C showed a specific surface area of 1508 m2·g-1 without activation which is far higher than that of other unactivated carbon aerogels. The starch based carbon aerogel carbonized at 800 °C exhibited superior methylene blue adsorption ability with a maximum adsorption capacity of 963.5 mg·g-1 as a result of its rich surface functional groups, high specific surface area, and reasonable pore size distribution. Furthermore, the carbon aerogel carbonized at 700 °C exhibited excellent electrochemical performance with a specific capacitance of 180.1 F·g-1 at a current density of 1 A·g-1as electrode materials for supercapacitors. Overall, this work provides a new method to prepare high performance starch based carbon aerogel. Starch based carbon aerogel has attracted significant attention due to the wide source, environmental friendliness and low price of raw materials. Here, starch based carbon aerogel was fabricated by graft reaction and cross-linking reaction of starch. The network structure of starch hydrogel was optimized through graft and cross-linking reaction. After freeze drying and high temperature carbonization, the obtained carbon aerogel that carbonized at 800 °C showed a specific surface area of 1508 m2·g−1 without activation which is far higher than that of other unactivated carbon aerogels. The starch based carbon aerogel carbonized at 800 °C exhibited superior methylene blue adsorption ability with a maximum adsorption capacity of 963.5 mg·g−1 as a result of its rich surface functional groups, high specific surface area, and reasonable pore size distribution. Furthermore, the carbon aerogel carbonized at 700 °C exhibited excellent electrochemical performance with a specific capacitance of 180.1 F·g−1 at a current density of 1 A·g−1as electrode materials for supercapacitors. Overall, this work provides a new method to prepare high performance starch based carbon aerogel. •Preparation of carbon aerogel using grafted and cross-linked starch hydrogel for the first time.•The specific surface area of the prepared carbon aerogel can reached 1508 m2/g without activation.•The starch-based carbon aerogel exhibited a maximum methylene blue adsorption capacity of 963.5 mg/g.•The starch-based carbon aerogel showed a specific capacitance of 180.1 F/g as electrode materials for supercapacitors. Starch based carbon aerogel has attracted significant attention due to the wide source, environmental friendliness and low price of raw materials. Here, starch based carbon aerogel was fabricated by graft reaction and cross-linking reaction of starch. The network structure of starch hydrogel was optimized through graft and cross-linking reaction. After freeze drying and high temperature carbonization, the obtained carbon aerogel that carbonized at 800 °C showed a specific surface area of 1508 m ·g without activation which is far higher than that of other unactivated carbon aerogels. The starch based carbon aerogel carbonized at 800 °C exhibited superior methylene blue adsorption ability with a maximum adsorption capacity of 963.5 mg·g as a result of its rich surface functional groups, high specific surface area, and reasonable pore size distribution. Furthermore, the carbon aerogel carbonized at 700 °C exhibited excellent electrochemical performance with a specific capacitance of 180.1 F·g at a current density of 1 A·g as electrode materials for supercapacitors. Overall, this work provides a new method to prepare high performance starch based carbon aerogel. |
| ArticleNumber | 133282 |
| Author | Gao, Yuhua Peng, Hanqing Yan, Meifang Li, Haihua Zheng, Yuxuan Ji, Yangfan Yu, Haitao Zhai, Zuozhao |
| Author_xml | – sequence: 1 givenname: Zuozhao surname: Zhai fullname: Zhai, Zuozhao organization: Hebei Key Laboratory of Organic Functional Molecules, College of Chemistry and Materials Science, Hebei Normal University, Shijiazhuang, Hebei 050024, China – sequence: 2 givenname: Haihua surname: Li fullname: Li, Haihua organization: Institute of Energy Resources, Hebei Academy of Sciences, Shijiazhuang, Hebei 050081, China – sequence: 3 givenname: Yuxuan surname: Zheng fullname: Zheng, Yuxuan organization: Institute of Energy Resources, Hebei Academy of Sciences, Shijiazhuang, Hebei 050081, China – sequence: 4 givenname: Yangfan surname: Ji fullname: Ji, Yangfan organization: Institute of Energy Resources, Hebei Academy of Sciences, Shijiazhuang, Hebei 050081, China – sequence: 5 givenname: Hanqing surname: Peng fullname: Peng, Hanqing organization: Hebei Key Laboratory of Organic Functional Molecules, College of Chemistry and Materials Science, Hebei Normal University, Shijiazhuang, Hebei 050024, China – sequence: 6 givenname: Yuhua surname: Gao fullname: Gao, Yuhua organization: Institute of Energy Resources, Hebei Academy of Sciences, Shijiazhuang, Hebei 050081, China – sequence: 7 givenname: Meifang surname: Yan fullname: Yan, Meifang organization: Institute of Energy Resources, Hebei Academy of Sciences, Shijiazhuang, Hebei 050081, China – sequence: 8 givenname: Haitao surname: Yu fullname: Yu, Haitao email: haitaoyu@hebtu.edu.cn organization: Hebei Key Laboratory of Organic Functional Molecules, College of Chemistry and Materials Science, Hebei Normal University, Shijiazhuang, Hebei 050024, China |
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| Keywords | Supercapacitors Starch based carbon aerogel Methylene |
| Language | English |
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| SubjectTerms | Adsorption Carbon - chemistry Electric Capacitance Gels - chemistry Methylene Methylene Blue - chemistry Porosity Starch - chemistry Starch based carbon aerogel Supercapacitors Surface Properties |
| Title | High specific surface area carbon aerogel derived from starch for methylene blue adsorption and supercapacitors |
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