Transition metal complexes of 13- and 14-membered N2O2 macrocycles: synthesis and characterization
Two novel series of 13- and 14-membered diazadioxamacrocyclic complexes [ML 1 Cl 2 ] and [ML 2 Cl 2 ] (M=Co 2+ , Ni 2+ , Cu 2+ , and Zn 2+ ) have been synthesized via the condensation reaction of o -aminophenol and 1,2-dibromoethane with a dialdehyde or a diketone in the presence of transition metal...
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| Published in | Transition metal chemistry (Weinheim) Vol. 33; no. 3; pp. 285 - 288 |
|---|---|
| Main Author | |
| Format | Journal Article |
| Language | English |
| Published |
Dordrecht
Springer Netherlands
01.04.2008
Springer Nature B.V |
| Subjects | |
| Online Access | Get full text |
| ISSN | 0340-4285 1572-901X |
| DOI | 10.1007/s11243-007-9040-0 |
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| Abstract | Two novel series of 13- and 14-membered diazadioxamacrocyclic complexes [ML
1
Cl
2
] and [ML
2
Cl
2
] (M=Co
2+
, Ni
2+
, Cu
2+
, and Zn
2+
) have been synthesized via the condensation reaction of
o
-aminophenol and 1,2-dibromoethane with a dialdehyde or a diketone in the presence of transition metal ions as templates in ethanol. The mode of bonding and overall geometry of the complexes have been inferred through IR,
1
H NMR, EPR, and electronic spectral studies, conductivity, and magnetic moment measurements. An octahedral geometry is proposed for all the complexes. |
|---|---|
| AbstractList | Two novel series of 13- and 14-membered diazadioxamacrocyclic complexes [ML^sup 1^Cl^sub 2^] and [ML^sup 2^Cl^sub 2^] (M=Co^sup 2+^, Ni^sup 2+^, Cu^sup 2+^, and Zn^sup 2+^) have been synthesized via the condensation reaction of o-aminophenol and 1,2-dibromoethane with a dialdehyde or a diketone in the presence of transition metal ions as templates in ethanol. The mode of bonding and overall geometry of the complexes have been inferred through IR, ^sup 1^H NMR, EPR, and electronic spectral studies, conductivity, and magnetic moment measurements. An octahedral geometry is proposed for all the complexes.[PUBLICATION ABSTRACT] Two novel series of 13- and 14-membered diazadioxamacrocyclic complexes [ML 1 Cl 2 ] and [ML 2 Cl 2 ] (M=Co 2+ , Ni 2+ , Cu 2+ , and Zn 2+ ) have been synthesized via the condensation reaction of o -aminophenol and 1,2-dibromoethane with a dialdehyde or a diketone in the presence of transition metal ions as templates in ethanol. The mode of bonding and overall geometry of the complexes have been inferred through IR, 1 H NMR, EPR, and electronic spectral studies, conductivity, and magnetic moment measurements. An octahedral geometry is proposed for all the complexes. |
| Author | Nasman, Omar S. M. |
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| Keywords | Electronic Spectral Study Macrocyclic Complex Octahedral Geometry Phthalaldehyde Charge Transfer Excitation |
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| References | Champness NR, Frampton CS, Reid G, Tocher DA (1994) J Chem Soc, Dalton Trans 3031 ShakirMVarkeySPPolyhedron19941379110.1016/S0277-5387(00)81686-11:CAS:528:DyaK2cXjtFCgt7c%3D Procter IM, Hathaway BJ, Nicholls P (1968) J Chem Soc, (A), 1678 LeverABPInorganic electronic spectroscopy1984AmsterdamElsevier Nasman OSM, Asian J Chem, (a)-(2), 19:1231 (2007); (b) –(1),16:471 (2004) NakamotoKInfrared spectra of inorganic and coordination compounds1970New YorkWiley Interscience SundarHGKRaoKJJ Non Cryst Solids19825013710.1016/0022-3093(82)90208-31:CAS:528:DyaL38XkvVeru7Y%3D ShakirMVarkeySPKumarDSynth React Inorg Met-Org Chem19942494110.1080/009457194080013131:CAS:528:DyaK2cXls1yqsb4%3D CurtisNFCoord Chem Rev19683310.1016/S0010-8545(00)80104-61:CAS:528:DyaF1cXktFGnsL4%3D NasmanOSMSynth React Inorg Met-org Chem2001318143310.1081/SIM-1001072081:CAS:528:DC%2BD3MXotVShtrs%3D MartellAEMotekaitisRJJ Am Chem Soc1988110805910.1021/ja00232a0171:CAS:528:DyaL1cXmtFKrtrY%3D MotekaitisRJMartellAEInorg Chem199231553410.1021/ic00052a0321:CAS:528:DyaK3sXmslyhtA%3D%3D AdamKRLeongAJLindoyLFLipHCSkeltonBWWhiteAHJ Am Chem Soc1983105464510.1021/ja00352a0211:CAS:528:DyaL3sXktlaitr4%3D Lazarides T, Miller TA, Jeffery JC, Ronson TK, Adams H, Ward MD (2005) J Chem Soc, Dalton Trans 528 Menif R, Martell AE (1989) J Chem Soc, Chem Commun 1521 GearyWJCoord Chem Rev197178110.1016/S0010-8545(00)80009-01:CAS:528:DyaE3MXlsVCgsrg%3D IsmaielAAABarakaRMNasmanOSMPolyhedron20012045510.1016/S0277-5387(00)00610-01:CAS:528:DC%2BD3MXhs1Sqsrc%3D Linday LF, Busch DH, Jolly W (Ed.) (1971) In: Preparative inorganic reactions, Interscience, New York, vol. 6 , p 1 FiggisBNIntroduction to ligand fields1966New YorkInterscience296 BiJHXieFXShingXSZhaoXDAsian J Chem2002148211:CAS:528:DC%2BD38XktFSrur8%3D LindoyLFSkeltonBWSmithSVWhiteAHAust J Chem1993463631:CAS:528:DyaK3sXkvFGnu7Y%3D10.1071/CH9930363 Garcia F, Goodman JM, Kowenicki RA, McPartlin M, Riera L, Silva MA, Wirsing A, Wright DS (2005) J Chem Soc, Dalton Trans, 1764 LIobetAReibenspiesJMartellAEInorg Chem199433594610.1021/ic00103a050 ShakirMVarkeySPNasmanOSMPolyhedron199514128310.1016/0277-5387(94)00395-U1:CAS:528:DyaK2MXlvFShsr4%3D Siegfried L, Kaden TA (2005) J Chem Soc, Dalton Trans 1136 Adam KR, Antolovich M, Baldwin DS, Duckworth PA, Leong AJ, Lindoy LF, McPartlin M, Tasker PA (1993) J Chem Soc, Dalton Trans 1013 ShakirMNasmanOSMMohamedAKVarkeySPPolyhedron199615128310.1016/0277-5387(95)00379-71:CAS:528:DyaK28XhtVymtb8%3D Gasperov V, Galbrith SG, Lindoy LF, Rumbel BR, Skelton BW, Tasker PA, White AH (2005) J Chem Soc, Dalton Trans 139 MelsonGACoordination chemistry of macrocyclic compounds1979New YorkPlenum Press BuschDHChristophGGZimmerLLJackelsSCGrzybowskiJJCallahanRCKojimaMHolterKAMocakJHeronNShavanMSchammelWPJ Am Chem Soc1981103510710.1021/ja00407a0271:CAS:528:DyaL3MXkvFSgs7w%3D Frausto da SilvaJJRWilliamsRJPThe biological chemistry of the elements1991OxfordClaredon Press ShakirMVarkeySPFirdausFHameedPSPolyhedron199415231910.1016/S0277-5387(00)88142-5 NasmanOSMBarakaRMKhaldiAAINahhalVarkeySPShakirMTransition Met Chem19972227310.1023/A:10184207258601:CAS:528:DyaK2sXktF2lsrs%3D VogelAIA text book of quantitative inorganic analysis1961LondonLongmans433 9040_CR15 9040_CR31 9040_CR10 A LIobet (9040_CR19) 1994; 33 GA Melson (9040_CR12) 1979 WJ Geary (9040_CR26) 1971; 7 ABP Lever (9040_CR34) 1984 M Shakir (9040_CR4) 1994; 13 AE Martell (9040_CR17) 1988; 110 M Shakir (9040_CR24) 1995; 14 K Nakamoto (9040_CR27) 1970 AAA Ismaiel (9040_CR8) 2001; 20 HGK Sundar (9040_CR30) 1982; 50 9040_CR5 9040_CR6 9040_CR3 JH Bi (9040_CR29) 2002; 14 NF Curtis (9040_CR14) 1968; 3 9040_CR20 9040_CR7 BN Figgis (9040_CR32) 1966 M Shakir (9040_CR23) 1996; 15 M Shakir (9040_CR28) 1994; 24 9040_CR1 JJR Frausto da Silva (9040_CR2) 1991 LF Lindoy (9040_CR9) 1993; 46 KR Adam (9040_CR11) 1983; 105 M Shakir (9040_CR33) 1994; 15 OSM Nasman (9040_CR22) 1997; 22 DH Busch (9040_CR13) 1981; 103 AI Vogel (9040_CR25) 1961 OSM Nasman (9040_CR21) 2001; 31 9040_CR18 RJ Motekaitis (9040_CR16) 1992; 31 |
| References_xml | – reference: LeverABPInorganic electronic spectroscopy1984AmsterdamElsevier – reference: AdamKRLeongAJLindoyLFLipHCSkeltonBWWhiteAHJ Am Chem Soc1983105464510.1021/ja00352a0211:CAS:528:DyaL3sXktlaitr4%3D – reference: NasmanOSMBarakaRMKhaldiAAINahhalVarkeySPShakirMTransition Met Chem19972227310.1023/A:10184207258601:CAS:528:DyaK2sXktF2lsrs%3D – reference: LIobetAReibenspiesJMartellAEInorg Chem199433594610.1021/ic00103a050 – reference: Frausto da SilvaJJRWilliamsRJPThe biological chemistry of the elements1991OxfordClaredon Press – reference: NakamotoKInfrared spectra of inorganic and coordination compounds1970New YorkWiley Interscience – reference: LindoyLFSkeltonBWSmithSVWhiteAHAust J Chem1993463631:CAS:528:DyaK3sXkvFGnu7Y%3D10.1071/CH9930363 – reference: ShakirMVarkeySPPolyhedron19941379110.1016/S0277-5387(00)81686-11:CAS:528:DyaK2cXjtFCgt7c%3D – reference: MotekaitisRJMartellAEInorg Chem199231553410.1021/ic00052a0321:CAS:528:DyaK3sXmslyhtA%3D%3D – reference: Lazarides T, Miller TA, Jeffery JC, Ronson TK, Adams H, Ward MD (2005) J Chem Soc, Dalton Trans 528 – reference: CurtisNFCoord Chem Rev19683310.1016/S0010-8545(00)80104-61:CAS:528:DyaF1cXktFGnsL4%3D – reference: ShakirMNasmanOSMMohamedAKVarkeySPPolyhedron199615128310.1016/0277-5387(95)00379-71:CAS:528:DyaK28XhtVymtb8%3D – reference: GearyWJCoord Chem Rev197178110.1016/S0010-8545(00)80009-01:CAS:528:DyaE3MXlsVCgsrg%3D – reference: FiggisBNIntroduction to ligand fields1966New YorkInterscience296 – reference: Garcia F, Goodman JM, Kowenicki RA, McPartlin M, Riera L, Silva MA, Wirsing A, Wright DS (2005) J Chem Soc, Dalton Trans, 1764 – reference: Nasman OSM, Asian J Chem, (a)-(2), 19:1231 (2007); (b) –(1),16:471 (2004) – reference: Adam KR, Antolovich M, Baldwin DS, Duckworth PA, Leong AJ, Lindoy LF, McPartlin M, Tasker PA (1993) J Chem Soc, Dalton Trans 1013 – reference: BuschDHChristophGGZimmerLLJackelsSCGrzybowskiJJCallahanRCKojimaMHolterKAMocakJHeronNShavanMSchammelWPJ Am Chem Soc1981103510710.1021/ja00407a0271:CAS:528:DyaL3MXkvFSgs7w%3D – reference: MartellAEMotekaitisRJJ Am Chem Soc1988110805910.1021/ja00232a0171:CAS:528:DyaL1cXmtFKrtrY%3D – reference: BiJHXieFXShingXSZhaoXDAsian J Chem2002148211:CAS:528:DC%2BD38XktFSrur8%3D – reference: VogelAIA text book of quantitative inorganic analysis1961LondonLongmans433 – reference: Gasperov V, Galbrith SG, Lindoy LF, Rumbel BR, Skelton BW, Tasker PA, White AH (2005) J Chem Soc, Dalton Trans 139 – reference: ShakirMVarkeySPNasmanOSMPolyhedron199514128310.1016/0277-5387(94)00395-U1:CAS:528:DyaK2MXlvFShsr4%3D – reference: ShakirMVarkeySPFirdausFHameedPSPolyhedron199415231910.1016/S0277-5387(00)88142-5 – reference: Siegfried L, Kaden TA (2005) J Chem Soc, Dalton Trans 1136 – reference: NasmanOSMSynth React Inorg Met-org Chem2001318143310.1081/SIM-1001072081:CAS:528:DC%2BD3MXotVShtrs%3D – reference: Menif R, Martell AE (1989) J Chem Soc, Chem Commun 1521 – reference: Procter IM, Hathaway BJ, Nicholls P (1968) J Chem Soc, (A), 1678 – reference: ShakirMVarkeySPKumarDSynth React Inorg Met-Org Chem19942494110.1080/009457194080013131:CAS:528:DyaK2cXls1yqsb4%3D – reference: SundarHGKRaoKJJ Non Cryst Solids19825013710.1016/0022-3093(82)90208-31:CAS:528:DyaL38XkvVeru7Y%3D – reference: Champness NR, Frampton CS, Reid G, Tocher DA (1994) J Chem Soc, Dalton Trans 3031 – reference: Linday LF, Busch DH, Jolly W (Ed.) 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| Snippet | Two novel series of 13- and 14-membered diazadioxamacrocyclic complexes [ML
1
Cl
2
] and [ML
2
Cl
2
] (M=Co
2+
, Ni
2+
, Cu
2+
, and Zn
2+
) have been... Two novel series of 13- and 14-membered diazadioxamacrocyclic complexes [ML^sup 1^Cl^sub 2^] and [ML^sup 2^Cl^sub 2^] (M=Co^sup 2+^, Ni^sup 2+^, Cu^sup 2+^,... |
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| SubjectTerms | Catalysis Chemistry Chemistry and Materials Science Inorganic Chemistry Organometallic Chemistry Physical Chemistry |
| Title | Transition metal complexes of 13- and 14-membered N2O2 macrocycles: synthesis and characterization |
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