Surface reconstruction of NiFe layered double hydroxides by S2- corrosion for efficient oxygen evolution
[Display omitted] Nickel-iron layered double hydroxides (NiFe LDH) are subject to surface reconstruction by the applied anodic potential in alkaline media, and the reconstructed metal hydroxyl oxides are often considered to be the actual active material for oxygen evolution reaction (OER), so how to...
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| Published in | Journal of electroanalytical chemistry (Lausanne, Switzerland) Vol. 947; p. 117788 |
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| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
15.10.2023
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| Subjects | |
| Online Access | Get full text |
| ISSN | 1572-6657 1873-2569 |
| DOI | 10.1016/j.jelechem.2023.117788 |
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| Abstract | [Display omitted]
Nickel-iron layered double hydroxides (NiFe LDH) are subject to surface reconstruction by the applied anodic potential in alkaline media, and the reconstructed metal hydroxyl oxides are often considered to be the actual active material for oxygen evolution reaction (OER), so how to facilitate surface reconstruction is crucial for their performance. In this paper, the surface reconstruction of NiFe LDH nanosheets was successfully induced by S2- corrosion using rapid wet chemical engineering without affecting their crystal structure and nanomorphology; Notably, the NiOOH species formed on the corroded S-NiFe LDH/NF surface participate in the OER process as active species. The electrochemical measurements show that S-NiFe LDH/NF has a low overpotential of 250 mV and a Tafel slope of 26.3 mV dec -1 at 50 mA cm−2. This work provides a simple activation strategy for the surface reconstruction of NiFe LDH, which is an important reference for the design of advanced catalysts. |
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| AbstractList | [Display omitted]
Nickel-iron layered double hydroxides (NiFe LDH) are subject to surface reconstruction by the applied anodic potential in alkaline media, and the reconstructed metal hydroxyl oxides are often considered to be the actual active material for oxygen evolution reaction (OER), so how to facilitate surface reconstruction is crucial for their performance. In this paper, the surface reconstruction of NiFe LDH nanosheets was successfully induced by S2- corrosion using rapid wet chemical engineering without affecting their crystal structure and nanomorphology; Notably, the NiOOH species formed on the corroded S-NiFe LDH/NF surface participate in the OER process as active species. The electrochemical measurements show that S-NiFe LDH/NF has a low overpotential of 250 mV and a Tafel slope of 26.3 mV dec -1 at 50 mA cm−2. This work provides a simple activation strategy for the surface reconstruction of NiFe LDH, which is an important reference for the design of advanced catalysts. |
| ArticleNumber | 117788 |
| Author | Hao, Liping Wang, Peng Xuanwen, Liu Wang, Hongxin |
| Author_xml | – sequence: 1 givenname: Peng surname: Wang fullname: Wang, Peng organization: School of Materials Science and Engineering, Northeastern University, Shenyang 110819, PR China – sequence: 2 givenname: Liping surname: Hao fullname: Hao, Liping organization: School of Materials Science and Engineering, Northeastern University, Shenyang 110819, PR China – sequence: 3 givenname: Hongxin surname: Wang fullname: Wang, Hongxin organization: School of Materials Science and Engineering, Northeastern University, Shenyang 110819, PR China – sequence: 4 givenname: Liu surname: Xuanwen fullname: Xuanwen, Liu email: lxw@neuq.edu.cn organization: School of Materials Science and Engineering, Northeastern University, Shenyang 110819, PR China |
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