Structure stability driven large magnetocaloric response in Ni–Co–Mn–In–Si Heusler alloy
Ni–Mn–In Heusler alloys have received considerable attention in the field of magnetic refrigeration owing to their eco-friendliness and large magnetocaloric (MC) response. In this paper, samples of Ni45Co5Mn37In12Si1 thus heat-treated for 0 h and 15 h have prepared by means of arc-melting followed b...
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| Published in | Ceramics international Vol. 48; no. 19; pp. 29059 - 29066 |
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| Main Authors | , , |
| Format | Journal Article |
| Language | English |
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01.10.2022
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| Abstract | Ni–Mn–In Heusler alloys have received considerable attention in the field of magnetic refrigeration owing to their eco-friendliness and large magnetocaloric (MC) response. In this paper, samples of Ni45Co5Mn37In12Si1 thus heat-treated for 0 h and 15 h have prepared by means of arc-melting followed by quenching. X-ray diffraction analysis confirms L21-type crystal structure and stabilization of austenite phase at room temperature. FE-SEM equipped with EDS reveals the surface morphology and elemental composition of 15 h heat-treated Ni45Co5Mn37In12Si1 alloy with well-distinguished larger grains and a dendritic structure. Thermomagnetic measurements of 15 h heat-treated Ni45Co5Mn37In12Si1 shows the magnetostructural transition TCM at the temperature of ∼262 K and Curie temperature of austenite, TCA was found to be above ∼396 K with increase in the annealing time. Metamagnetic behavior and magnetic hysteresis are seen in isothermal magnetization curves. Interestingly, a large change in magnetic entropy ΔSM ∼9.3 J kg−1 K−1 was obtained with refrigeration capacity (RC) of ∼416.6 J kg−1 under an applied field change of 5T with a broad temperature window of ∼86 K for Ni45Co5Mn37In12Si1 alloy thus annealed for 15 h which makes it to be suitable for magnetic refrigeration applications. |
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| AbstractList | Ni–Mn–In Heusler alloys have received considerable attention in the field of magnetic refrigeration owing to their eco-friendliness and large magnetocaloric (MC) response. In this paper, samples of Ni45Co5Mn37In12Si1 thus heat-treated for 0 h and 15 h have prepared by means of arc-melting followed by quenching. X-ray diffraction analysis confirms L21-type crystal structure and stabilization of austenite phase at room temperature. FE-SEM equipped with EDS reveals the surface morphology and elemental composition of 15 h heat-treated Ni45Co5Mn37In12Si1 alloy with well-distinguished larger grains and a dendritic structure. Thermomagnetic measurements of 15 h heat-treated Ni45Co5Mn37In12Si1 shows the magnetostructural transition TCM at the temperature of ∼262 K and Curie temperature of austenite, TCA was found to be above ∼396 K with increase in the annealing time. Metamagnetic behavior and magnetic hysteresis are seen in isothermal magnetization curves. Interestingly, a large change in magnetic entropy ΔSM ∼9.3 J kg−1 K−1 was obtained with refrigeration capacity (RC) of ∼416.6 J kg−1 under an applied field change of 5T with a broad temperature window of ∼86 K for Ni45Co5Mn37In12Si1 alloy thus annealed for 15 h which makes it to be suitable for magnetic refrigeration applications. |
| Author | Venkatesan, Shaleni Kavita, S. Perumal, Suresh |
| Author_xml | – sequence: 1 givenname: Shaleni surname: Venkatesan fullname: Venkatesan, Shaleni organization: Laboratory for Energy and Advanced Devices (LEAD), Department of Physics and Nanotechnology, SRM Institute of Science and Technology, Kattankulathur, Chengalpattu, 603 203, Tamilnadu, India – sequence: 2 givenname: S. surname: Kavita fullname: Kavita, S. organization: International Advanced Research Centre for Powder Metallurgy and New Materials (ARCI), Chennai, 600113, Tamilnadu, India – sequence: 3 givenname: Suresh orcidid: 0000-0002-2310-545X surname: Perumal fullname: Perumal, Suresh email: sureshp4@srmist.edu.in, drsureshperumal@gmail.com organization: Laboratory for Energy and Advanced Devices (LEAD), Department of Physics and Nanotechnology, SRM Institute of Science and Technology, Kattankulathur, Chengalpattu, 603 203, Tamilnadu, India |
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| CitedBy_id | crossref_primary_10_1016_j_jallcom_2022_168590 crossref_primary_10_1016_j_mseb_2022_116067 crossref_primary_10_3390_met13121913 |
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| Keywords | NiMnIn based materials Large refrigeration capacity Austenite phase High change in magnetic entropy Structural transition |
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| SubjectTerms | Austenite phase High change in magnetic entropy Large refrigeration capacity NiMnIn based materials Structural transition |
| Title | Structure stability driven large magnetocaloric response in Ni–Co–Mn–In–Si Heusler alloy |
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