Differential detection of strong acids in weak acids: a combination of a benzimidazole-carbazole backbone with AIE luminophores as highly sensitive and selective turn-on fluorescent probes

o -BzcDPE and p -BzcDPE have been synthesized and used as probes for strong acid detection. The probes contain aggregation-induced emission luminogens (AIEgens) that are incorporated with a benzimidazole-carbazole backbone. Both probes show turn-on green fluorescence with a good contrast in the pres...

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Published inNew journal of chemistry Vol. 46; no. 21; pp. 1317 - 1327
Main Authors Lin, Pei-Chi, Lin, Yu-Ting, Liu, Kuan-Ting, Chen, Meng-Sin, Zhang, Yong-Yun, Li, Jie-Cheng, Leung, Man-kit
Format Journal Article
LanguageEnglish
Published CAMBRIDGE Royal Soc Chemistry 30.05.2022
Royal Society of Chemistry
Subjects
Acetic acid
Acids
Backbone
Carbazoles
Chemistry
Chemistry, Multidisciplinary
Crystallography
Fluorescent indicators
NMR spectroscopy
Physical Sciences
Protonation
Response time
Science & Technology
Selectivity
Sulfuric acid
BODIPY
ELECTRON-TRANSFER
FLUOROPHORES
AGGREGATION-INDUCED EMISSION
DONOR
PH
ENHANCED EMISSION
TETRAPHENYLETHYLENE
DERIVATIVES
INTRAMOLECULAR CHARGE-TRANSFER
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Abstract o -BzcDPE and p -BzcDPE have been synthesized and used as probes for strong acid detection. The probes contain aggregation-induced emission luminogens (AIEgens) that are incorporated with a benzimidazole-carbazole backbone. Both probes show turn-on green fluorescence with a good contrast in the presence of trace amounts of strong acids in a weak acid environment. These probes are not only suitable for visual detection of strong acids, but also exhibit high selectivity, excellent sensitivity, and short response time and are capable of quantitative detection of strong acids with a good linear relationship. A concentration of H 2 SO 4 as low as 1 mol% in acetic acid can be differentiated. The fluorescence-turn-on mechanisms are due to protonation on the benzimidazole moiety that have been proved by X-ray crystallographic analysis and NMR spectroscopy. With the combination of a benzimidazole-carbazole backbone and AIE luminophores, highly sensitive and selective turn-on fluorescent probes are achieved and applicable for differential detection of strong acids in weak acids.
AbstractList o-BzcDPE and p-BzcDPE have been synthesized and used as probes for strong acid detection. The probes contain aggregation-induced emission luminogens (AIEgens) that are incorporated with a benzimidazole-carbazole backbone. Both probes show turn-on green fluorescence with a good contrast in the presence of trace amounts of strong acids in a weak acid environment. These probes are not only suitable for visual detection of strong acids, but also exhibit high selectivity, excellent sensitivity, and short response time and are capable of quantitative detection of strong acids with a good linear relationship. A concentration of H 2 SO 4 as low as 1 mol% in acetic acid can be differentiated. The fluorescence-turn-on mechanisms are due to protonation on the benzimidazole moiety that have been proved by X-ray crystallographic analysis and NMR spectroscopy.
o -BzcDPE and p -BzcDPE have been synthesized and used as probes for strong acid detection. The probes contain aggregation-induced emission luminogens (AIEgens) that are incorporated with a benzimidazole-carbazole backbone. Both probes show turn-on green fluorescence with a good contrast in the presence of trace amounts of strong acids in a weak acid environment. These probes are not only suitable for visual detection of strong acids, but also exhibit high selectivity, excellent sensitivity, and short response time and are capable of quantitative detection of strong acids with a good linear relationship. A concentration of H 2 SO 4 as low as 1 mol% in acetic acid can be differentiated. The fluorescence-turn-on mechanisms are due to protonation on the benzimidazole moiety that have been proved by X-ray crystallographic analysis and NMR spectroscopy. With the combination of a benzimidazole-carbazole backbone and AIE luminophores, highly sensitive and selective turn-on fluorescent probes are achieved and applicable for differential detection of strong acids in weak acids.
o-BzcDPE and p-BzcDPE have been synthesized and used as probes for strong acid detection. The probes contain aggregation-induced emission luminogens (AIEgens) that are incorporated with a benzimidazole-carbazole backbone. Both probes show turn-on green fluorescence with a good contrast in the presence of trace amounts of strong acids in a weak acid environment. These probes are not only suitable for visual detection of strong acids, but also exhibit high selectivity, excellent sensitivity, and short response time and are capable of quantitative detection of strong acids with a good linear relationship. A concentration of H2SO4 as low as 1 mol% in acetic acid can be differentiated. The fluorescence-turn-on mechanisms are due to protonation on the benzimidazole moiety that have been proved by X-ray crystallographic analysis and NMR spectroscopy.
o-BzcDPE and p-BzcDPE have been synthesized and used as probes for strong acid detection. The probes contain aggregation-induced emission luminogens (AlEgens) that are incorporated with a benzimidazole-carbazole backbone. Both probes show turn-on green fluorescence with a good contrast in the presence of trace amounts of strong acids in a weak acid environment. These probes are not only suitable for visual detection of strong acids, but also exhibit high selectivity, excellent sensitivity, and short response time and are capable of quantitative detection of strong acids with a good linear relationship. A concentration of H2SO4 as low as 1 mol% in acetic acid can be differentiated. The fluorescence-turn-on mechanisms are due to protonation on the benzimidazole moiety that have been proved by X-ray crystallographic analysis and NMR spectroscopy.
Author Li, Jie-Cheng
Liu, Kuan-Ting
Leung, Man-kit
Chen, Meng-Sin
Lin, Pei-Chi
Lin, Yu-Ting
Zhang, Yong-Yun
AuthorAffiliation Chang Chun Plastics Co., Ltd. Kaohsiung Factory
National Taiwan University
Department of Chemistry and Advanced Research Center for Green Materials Science and Technology
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Issue 21
Keywords BODIPY
ELECTRON-TRANSFER
FLUOROPHORES
AGGREGATION-INDUCED EMISSION
DONOR
PH
ENHANCED EMISSION
TETRAPHENYLETHYLENE
DERIVATIVES
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Snippet o -BzcDPE and p -BzcDPE have been synthesized and used as probes for strong acid detection. The probes contain aggregation-induced emission luminogens...
o-BzcDPE and p-BzcDPE have been synthesized and used as probes for strong acid detection. The probes contain aggregation-induced emission luminogens (AlEgens)...
o-BzcDPE and p-BzcDPE have been synthesized and used as probes for strong acid detection. The probes contain aggregation-induced emission luminogens (AIEgens)...
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SubjectTerms Acetic acid
Acids
Backbone
Carbazoles
Chemistry
Chemistry, Multidisciplinary
Crystallography
Fluorescent indicators
NMR spectroscopy
Physical Sciences
Protonation
Response time
Science & Technology
Selectivity
Sulfuric acid
Title Differential detection of strong acids in weak acids: a combination of a benzimidazole-carbazole backbone with AIE luminophores as highly sensitive and selective turn-on fluorescent probes
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