Build-up and consolidation of an attractive network of particles in cement-based pastes
The very early age flocculation of a cement based paste, in which cement is partially substituted by a calcined clay, metakaolin, is studied. We use rheological and ultrasonic reflection to monitor the evolution of the elastic properties of the paste with time, and light scattering to follow the cha...
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| Published in | Cement and concrete research Vol. 183; p. 107573 |
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| Main Authors | , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier Ltd
01.09.2024
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| Abstract | The very early age flocculation of a cement based paste, in which cement is partially substituted by a calcined clay, metakaolin, is studied. We use rheological and ultrasonic reflection to monitor the evolution of the elastic properties of the paste with time, and light scattering to follow the change of its relaxation modes at small scales. We show that, at very early ages, of the order of hundreds of seconds after the paste preparation, a network of flocculated particles establishes, which manifests by a slow down of the dynamics of the relaxation modes of the paste at small scale. Then, this network consolidates and the macroscopic elastic modulus of the paste progressively increases with time, leading eventually to the setting of the paste. These observations show that, whatever the degree of replacement of clinker by metakaolin, a connected network establishes at very early times after the paste preparation, although the kinetics of flocculation slows down with clinker replacement. |
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| AbstractList | The very early age flocculation of a cement based paste, in which cement is partially substituted by a calcined clay, metakaolin, is studied. We use rheological and ultrasonic reflection to monitor the evolution of the elastic properties of the paste with time, and light scattering to follow the change of its relaxation modes at small scales. We show that, at very early ages, of the order of hundreds of seconds after the paste preparation, a network of flocculated particles establishes, which manifests by a slow down of the dynamics of the relaxation modes of the paste at small scale. Then, this network consolidates and the macroscopic elastic modulus of the paste progressively increases with time, leading eventually to the setting of the paste. These observations show that, whatever the degree of replacement of clinker by metakaolin, a connected network establishes at very early times after the paste preparation, although the kinetics of flocculation slows down with clinker replacement. |
| ArticleNumber | 107573 |
| Author | Ojeda-Farías, Omar Lootens, Didier Hébraud, Pascal |
| Author_xml | – sequence: 1 givenname: Omar surname: Ojeda-Farías fullname: Ojeda-Farías, Omar organization: IPCMS/CNRS, UMR 7504, 23 rue du Loess 67200, Strasbourg, France – sequence: 2 givenname: Didier surname: Lootens fullname: Lootens, Didier organization: Sika Technology AG-Central Research, Tueffenwies 16 CH_8040, Zürich, Switzerland – sequence: 3 givenname: Pascal surname: Hébraud fullname: Hébraud, Pascal email: pascal.hebraud@ipcms.unistra.fr organization: IPCMS/CNRS, UMR 7504, 23 rue du Loess 67200, Strasbourg, France |
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| Keywords | Metakaolin Flocculation Diffusing wave spectroscopy Cement |
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