Methyl orange adsorption studies on glutaraldehyde cross-linking chitosan/fluorapatite-based natural phosphate composite
In this work, chitosan, a biopolymer was cross-linked using glutaraldehyde (Gl) and modified by natural apatite. The Cs-Gl@Fap composite was used to adsorb methyl orange from an aqueous solution. The materials were characterised by SEM-EDX, FTIR, XRD and TGA-DTG analysis confirming the successful sy...
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Published in | International journal of environmental analytical chemistry Vol. ahead-of-print; no. ahead-of-print; pp. 1 - 17 |
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08.10.2022
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Abstract | In this work, chitosan, a biopolymer was cross-linked using glutaraldehyde (Gl) and modified by natural apatite. The Cs-Gl@Fap composite was used to adsorb methyl orange from an aqueous solution. The materials were characterised by SEM-EDX, FTIR, XRD and TGA-DTG analysis confirming the successful synthesis of Cs-Gl@Fap. The effects of experimental variables on adsorption efficiency were examined. Adsorption studies showed that the maximum adsorption capacity was 225.55 mg/g at an equilibration time of 120 min. The pseudo-second-order rate expression supported data best, while the Langmuir equation could satisfactorily describe isotherm data. The thermodynamic constants of the adsorption process were evaluated. The results showed that the stabilisation by contact of methyl orange on Cs-Gl@Fap was endothermic and spontaneous. Additionally, when reused, the hybrid adsorbent remains at approximately 83% of its original capacity after five adsorption cycles. |
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AbstractList | In this work, chitosan, a biopolymer was cross-linked using glutaraldehyde (Gl) and modified by natural apatite. The Cs-Gl@Fap composite was used to adsorb methyl orange from an aqueous solution. The materials were characterised by SEM-EDX, FTIR, XRD and TGA-DTG analysis confirming the successful synthesis of Cs-Gl@Fap. The effects of experimental variables on adsorption efficiency were examined. Adsorption studies showed that the maximum adsorption capacity was 225.55 mg/g at an equilibration time of 120 min. The pseudo-second-order rate expression supported data best, while the Langmuir equation could satisfactorily describe isotherm data. The thermodynamic constants of the adsorption process were evaluated. The results showed that the stabilisation by contact of methyl orange on Cs-Gl@Fap was endothermic and spontaneous. Additionally, when reused, the hybrid adsorbent remains at approximately 83% of its original capacity after five adsorption cycles. |
Author | EL Kaim Billah, Rachid Ahsaine, Hassan Ait El Messaoudi, Nourddine Zaghloul, Ahmed BaQais, Amal Jugade, Ravin Khadoudi, Idris Agunaou, Mahfoud Soufiane, Abdessadik |
Author_xml | – sequence: 1 givenname: Rachid surname: EL Kaim Billah fullname: EL Kaim Billah, Rachid email: rachidelkaimbillah@gmail.com organization: University of Chouaib Doukkali – sequence: 2 givenname: Ahmed surname: Zaghloul fullname: Zaghloul, Ahmed organization: Ibn Zohr University – sequence: 3 givenname: Hassan Ait orcidid: 0000-0002-8423-9689 surname: Ahsaine fullname: Ahsaine, Hassan Ait organization: Mohammed V University in Rabat – sequence: 4 givenname: Amal orcidid: 0000-0002-4896-8235 surname: BaQais fullname: BaQais, Amal organization: Princess Nourah bint Abdulrahman University – sequence: 5 givenname: Idris surname: Khadoudi fullname: Khadoudi, Idris organization: University of Chouaib Doukkali – sequence: 6 givenname: Nourddine surname: El Messaoudi fullname: El Messaoudi, Nourddine organization: Ibn Zohr University – sequence: 7 givenname: Mahfoud surname: Agunaou fullname: Agunaou, Mahfoud organization: University of Chouaib Doukkali – sequence: 8 givenname: Abdessadik surname: Soufiane fullname: Soufiane, Abdessadik organization: University of Chouaib Doukkali – sequence: 9 givenname: Ravin orcidid: 0000-0003-4504-3584 surname: Jugade fullname: Jugade, Ravin organization: R.T.M. Nagpur University |
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Title | Methyl orange adsorption studies on glutaraldehyde cross-linking chitosan/fluorapatite-based natural phosphate composite |
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