Essential Oil Analysis of Illicium anistum L. Extracts
Fresh japanese anise (Illicium anisatum L.) tree leaves were collected and ground after drying. The essential oils of the leaves were analyzed by gas chromatography-mass spectrometry (GC-MS) using headspace (HS) and solid phase-microextra (SPME) methods. Volatile components of the leaves were identi...
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Published in | Journal of the Korean Wood Science and Technology Vol. 45; no. 6; pp. 682 - 688 |
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Main Authors | , , , |
Format | Journal Article |
Language | English |
Published |
한국목재공학회
01.11.2017
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Subjects | |
Online Access | Get full text |
ISSN | 1017-0715 2233-7180 |
DOI | 10.5658/WOOD.2017.45.6.682 |
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Abstract | Fresh japanese anise (Illicium anisatum L.) tree leaves were collected and ground after drying. The essential oils of the leaves were analyzed by gas chromatography-mass spectrometry (GC-MS) using headspace (HS) and solid phase-microextra (SPME) methods.
Volatile components of the leaves were identified 21 and 65 components in HS and SPME, respectively. The main components of the essential oils obtained by HS method were eucalyptol (36.7%), (+)-sabinene (15.61%), δ-3-carene (6.87%), α-pinene (6.07%), γ-terpinen (5.72%), α-limonene (5.26%), β-myrcene (4.13%), α-terpinene (4.04%) and β-pinene (3.73%). The other components were less than 3.5%. SPME method also showed that eucalyptol (17.88%) was main. The other were 5-allyl-1-methoxy-2 (13.29%), caryophyllene (6.09%), (+)-sabinene (5.60%), α-ocimene (4.89%) and β-myrcene (3.73%), and the rest were less amounts than 3.5%. This work indicated that many more volatile components were isolated, comparing to the previous literature data and that SPME method was much more effective than HS method in the analysis of the volatile components. KCI Citation Count: 4 |
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AbstractList | Fresh japanese anise (Illicium anisatum L.) tree leaves were collected and ground after drying. The essential oils of the leaves were analyzed by gas chromatography-mass spectrometry (GC-MS) using headspace (HS) and solid phase-microextra (SPME) methods.
Volatile components of the leaves were identified 21 and 65 components in HS and SPME, respectively. The main components of the essential oils obtained by HS method were eucalyptol (36.7%), (+)-sabinene (15.61%), δ-3-carene (6.87%), α-pinene (6.07%), γ-terpinen (5.72%), α-limonene (5.26%), β-myrcene (4.13%), α-terpinene (4.04%) and β-pinene (3.73%). The other components were less than 3.5%. SPME method also showed that eucalyptol (17.88%) was main. The other were 5-allyl-1-methoxy-2 (13.29%), caryophyllene (6.09%), (+)-sabinene (5.60%), α-ocimene (4.89%) and β-myrcene (3.73%), and the rest were less amounts than 3.5%. This work indicated that many more volatile components were isolated, comparing to the previous literature data and that SPME method was much more effective than HS method in the analysis of the volatile components. KCI Citation Count: 4 |
Author | Hyun, Hwa-Ja Kim, Chan-Soo Bae, Young-Soo Min, Hee-Jeong |
Author_xml | – sequence: 1 givenname: Hee-Jeong surname: Min fullname: Min, Hee-Jeong – sequence: 2 givenname: Chan-Soo surname: Kim fullname: Kim, Chan-Soo – sequence: 3 givenname: Hwa-Ja surname: Hyun fullname: Hyun, Hwa-Ja – sequence: 4 givenname: Young-Soo orcidid: 0000-0003-1108-9269 surname: Bae fullname: Bae, Young-Soo |
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Cites_doi | 10.2478/v10007-009-0022-y 10.1271/bbb.63.184 10.1002/recl.18850040202 10.1016/0040-4020(68)89022-2 10.1016/j.chroma.2005.09.067 10.1139/v66-371 10.1002/ptr.1592 10.1021/ac00218a019 10.1021/jf020850t |
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References | Arthur (key2.02201271014e+13_R1) 1990; 62 Cook (key2.02201271014e+13_R2) 1966; 44 Kim (key2.02201271014e+13_R3) 2005; 19 Yamada (key2.02201271014e+13_R10) 1968; 24 Eijkman (key2.02201271014e+13_R7) 1885; 4 Kim (key2.02201271014e+13_R4) 2003; 51 Zhao (key2.02201271014e+13_R11) 2005; 1096 Kim (key2.02201271014e+13_R5) 2009; 59 Lim (key2.02201271014e+13_R9) 2008; 21 Kim (key2.02201271014e+13_R6) 1999; 63 |
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