On the structural arrangement and optical band gap (PbO)x(ZnO)10(TeO2)90−x glasses
The glasses (PbO)x(ZnO)10(TeO2)90−x, where x=10, 20, 30, 35 and 40mol%, were prepared with a classic melting method from pure oxides. With an increase in x the density increases from 5.92 (x=10) to 6.8 (x=40) g/cm3, the glass-transition temperature decreases from 299 to 254°C and the optical band ga...
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Published in | Journal of non-crystalline solids Vol. 459; pp. 63 - 67 |
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Language | English |
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01.03.2017
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Abstract | The glasses (PbO)x(ZnO)10(TeO2)90−x, where x=10, 20, 30, 35 and 40mol%, were prepared with a classic melting method from pure oxides. With an increase in x the density increases from 5.92 (x=10) to 6.8 (x=40) g/cm3, the glass-transition temperature decreases from 299 to 254°C and the optical band gap decreases from 3.73 to 3.48eV. It is suggested from the Raman scattering spectra that the structural units inherent to [Te3O8]4− and [TeO3]2− anions form the Te-O based network, that is with an increase in x the conversion proceeds from TeO4 to TeO3 structural units. The values of the non-linear refractive index were estimated from the optical band gap values in the region: (6.5–8.4)×10−12esu.
•Conversion of TeO4 trigonal bipyramids to TeO3 trigonal pyramids•Optical band gap decreased from 3.73 to 3.48eV with an increase in PbO content.•Estimated values of the non-linear refractive index are around 7.5×10−12esu. |
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AbstractList | The glasses (PbO)x(ZnO)10(TeO2)90−x, where x=10, 20, 30, 35 and 40mol%, were prepared with a classic melting method from pure oxides. With an increase in x the density increases from 5.92 (x=10) to 6.8 (x=40) g/cm3, the glass-transition temperature decreases from 299 to 254°C and the optical band gap decreases from 3.73 to 3.48eV. It is suggested from the Raman scattering spectra that the structural units inherent to [Te3O8]4− and [TeO3]2− anions form the Te-O based network, that is with an increase in x the conversion proceeds from TeO4 to TeO3 structural units. The values of the non-linear refractive index were estimated from the optical band gap values in the region: (6.5–8.4)×10−12esu.
•Conversion of TeO4 trigonal bipyramids to TeO3 trigonal pyramids•Optical band gap decreased from 3.73 to 3.48eV with an increase in PbO content.•Estimated values of the non-linear refractive index are around 7.5×10−12esu. |
Author | Tichy, Ladislav Schwarz, Jiri Ticha, Helena |
Author_xml | – sequence: 1 givenname: Helena surname: Ticha fullname: Ticha, Helena email: helena.ticha@upce.cz – sequence: 2 givenname: Jiri surname: Schwarz fullname: Schwarz, Jiri – sequence: 3 givenname: Ladislav surname: Tichy fullname: Tichy, Ladislav |
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Snippet | The glasses (PbO)x(ZnO)10(TeO2)90−x, where x=10, 20, 30, 35 and 40mol%, were prepared with a classic melting method from pure oxides. With an increase in x the... |
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StartPage | 63 |
SubjectTerms | Non-linear refractive index Optical band gap Raman spectra Tellurite glass |
Title | On the structural arrangement and optical band gap (PbO)x(ZnO)10(TeO2)90−x glasses |
URI | https://dx.doi.org/10.1016/j.jnoncrysol.2017.01.012 |
Volume | 459 |
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