Relation between Viscosity and Film Thickness of Dental Luting Cements

Purpose: Film thickness of dental luting cement is an important property that influences in success of fixed prosthodontics. Conventionally, it has been considered that the film thickness depends on the maximum particle size of cement powder and the viscosity of cement mixtures. However, the detaile...

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Published inNihon Hotetsu Shika Gakkai Zasshi Vol. 45; no. 5; pp. 612 - 621
Main Authors Kimura, Kohei, Kasahara, Shin, Hosotani, Makoto, Ando, Masaaki, Saito, Hirota, Hatakeyama, Noriko
Format Journal Article
LanguageJapanese
Published Japan Prosthodontic Society 2001
Subjects
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ISSN0389-5386
1883-177X
DOI10.2186/jjps.45.612

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Abstract Purpose: Film thickness of dental luting cement is an important property that influences in success of fixed prosthodontics. Conventionally, it has been considered that the film thickness depends on the maximum particle size of cement powder and the viscosity of cement mixtures. However, the detailed mechanism remains uncertain. This study aimed to measure basic properties, consistency, film thickness, distribution of powder particles and viscosity change after mixing, and the factors given to the film thickness were investigated. Methods: Four commercial dental luting cements were used. Basic properties were measured following the standard of JIS T-6602 (Japanese Industrial Standard, corresponding to ISO 9917: Dental Water-based cements), and in addition, cement powder distributions were measured. Apparent viscosity changes after mixing were measured by a Cone-Plate-type Rotary Viscometer, and film thickness was measured at each viscosity of cements. Results: Consistency rose with the time course, and film thickness was not always increased. No relation could be recognized between the maximum particle size of cement powder and film thickness. As a result of the measurement, the viscosity increased, when it grew on doing the film thickness. Both relations were almost rectilinear. The tendency was different according to the type of cement. Conclusions: For film thickness of the cement, an effect of particle size could not be observed. It was indicated that the viscosity change after mixing, and the particle size distribution of cement powder, influenced film thickness.
AbstractList Purpose: Film thickness of dental luting cement is an important property that influences in success of fixed prosthodontics. Conventionally, it has been considered that the film thickness depends on the maximum particle size of cement powder and the viscosity of cement mixtures. However, the detailed mechanism remains uncertain. This study aimed to measure basic properties, consistency, film thickness, distribution of powder particles and viscosity change after mixing, and the factors given to the film thickness were investigated. Methods: Four commercial dental luting cements were used. Basic properties were measured following the standard of JIS T-6602 (Japanese Industrial Standard, corresponding to ISO 9917: Dental Water-based cements), and in addition, cement powder distributions were measured. Apparent viscosity changes after mixing were measured by a Cone-Plate-type Rotary Viscometer, and film thickness was measured at each viscosity of cements. Results: Consistency rose with the time course, and film thickness was not always increased. No relation could be recognized between the maximum particle size of cement powder and film thickness. As a result of the measurement, the viscosity increased, when it grew on doing the film thickness. Both relations were almost rectilinear. The tendency was different according to the type of cement. Conclusions: For film thickness of the cement, an effect of particle size could not be observed. It was indicated that the viscosity change after mixing, and the particle size distribution of cement powder, influenced film thickness.
Author Kasahara, Shin
Kimura, Kohei
Hosotani, Makoto
Ando, Masaaki
Hatakeyama, Noriko
Saito, Hirota
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  fullname: Kimura, Kohei
  organization: Division of Fixed Prosthodontics, Department of Oral Rehabilitation and Materials Science, Graduate School of Dentistry, Tohoku University
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  fullname: Kasahara, Shin
  organization: Division of Fixed Prosthodontics, Department of Oral Rehabilitation and Materials Science, Graduate School of Dentistry, Tohoku University
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  fullname: Hosotani, Makoto
  organization: Saito Dental Office
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  fullname: Ando, Masaaki
  organization: Division of Fixed Prosthodontics, Department of Oral Rehabilitation and Materials Science, Graduate School of Dentistry, Tohoku University
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  fullname: Saito, Hirota
  organization: Division of Fixed Prosthodontics, Department of Oral Rehabilitation and Materials Science, Graduate School of Dentistry, Tohoku University
– sequence: 1
  fullname: Hatakeyama, Noriko
  organization: Tohoku Welfare Pension Hospital
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References 4) 木村幸平, 志村俊晴, 小野寺勉ほか. グラスアイオノマーセメント合着による鋳造冠の浮き上がりについて. 補綴誌25: 304-310, 1981.
11) Wiskott HWA, Belser UC, Scherrer SS. The effect of film thickness and surface texture on the resistance of cemented extracoronal restorations to lateral fatigue loading. Int J Prosthodont 12: 255-262, 1999.
16) 中川鶴太郎. レオロジー第2版76-86, 東京: 岩波書店, 1978.
6) 本村和義, 大谷宏, 細田裕康. リン酸セメントの被膜厚さと軟度との相関関係. 歯材器誌9: 43-50, 1963.
5) Jørgensen KD. Factors affecting the film thickness of zinc phosphate cements. Acta Odontol Scand 18: 479-490, 1960.
7) Vermilyea S, Powers JM, Craig RG. Rotation viscometry of a zinc phosphate and a zinc polyacrylate cement. J Dent Res 56: 762-767, 1977.
12) 畠山憲子, 笠原紳, 安藤正明ほか. 接着性レジンセメントの諸性質第一報機械的強度について. 東北大歯誌18: 166-174, 1999.
26) 笠原紳, 木村幸平, 齋藤裕太ほか. 生体親和性セメントCPC (calcium phosphate cement) の硬化に与える各種添加物の影響. 東北大歯誌16: 54-61, 1997.
10) 畑村又好, 奥野忠一, 津村善郎訳. スネデカー, コクラン統計的方法原書第6版394-416, 東京: 岩波書店, 1979.
8) 竹内正巳. リン酸亜鉛セメントの硬化過程における粘性挙動. 歯理工誌19: 279-289, 1978.
21) Jørgensen KD, Petersen GF. The grain size of zinc phosphate cements. Acta Odontol Scand 21: 255-270, 1963.
1) 日本歯科材料工業協同組合. JDMA Guide Book 352-382, 東京: 日本規格協会, 1997.
13) 畠山憲子, 笠原紳, 安藤正明ほか. 接着性レジンセメントの諸性質第二報せん断強度, 疲労強度, 吸水量, 溶解量について. 東北大歯誌19: 64-75, 2000.
27) 笠原紳, 木村幸平, Takagi sほか. 生体親和性セメントCPCの硬化時粘度に与える各種添加物の影響. 歯産学誌11: 23-30, 1997.
22) 西村文夫, 宮治俊幸, 野本直. セメント膜厚への振動の影響. 歯材器誌23: 29-34, 1970.
15) 川上道夫. 第2版新歯科材料・器械98-105, 東京: 医歯薬出版, 1994.
2) 吉田恵夫, 佐藤弘, 鹿沼晶夫ほか. セメント合着による鋳造冠の浮き上りについて第1報金属原型使用の場合.補綴誌4: 157-161, 1960.
3) Fusayama T, Ide K, Hosoda H. Relief of resistance of cement of full cast crowns. J Prosth Dent 14: 95-106, 1964.
24) 笠原紳, 奥山弥生, 木村幸平ほか. 支台歯形成練習エキスパートシステムの開発QE19: 192-197, 2000.
9) Windeler AS. The use of film thickness to measure working time of zinc phosphate cements. J Dent Res 57: 697-701, 1978.
23) Kay GW, Jablonski DA, Dogon IL. Factors affecting the seating and fit of complete crowns: A computer simulation study. J Prosthet Dent 55: 13-18, 1986.
14) 長谷川二郎, 平沢忠, 高橋重雄編. 現代歯科理工学200-218, 東京: 医歯薬出版, 1996.
17) Jørgensen KD. Structure of the film of zinc phosphate cements. Acta Odontol Scand 18: 491-501, 1960.
20) 脇博泰. 仮着用ならびに合着用セメントの浮き上がりに関する実験的研究. 九州歯会誌42: 377-391, 1988.
19) 脇博泰. 村上繁樹, 内田康也ほか. 仮着用ならびに合着用セメントの被膜厚さに関する研究. 九州歯会誌40: 1143-1150, 1986.
25) 本永三千雄, 石橋実, 笠原紳ほか. 全部陶材冠の3次元有限要素法を用いた応力解析-境界の連続性を考慮した解析-.補綴誌43: 791-795, 1999.
18) 塩沢育己. セメント合着による全部鋳造冠の三次元的変位に関する研究. 補綴誌23: 86-102, 1979.
References_xml – reference: 3) Fusayama T, Ide K, Hosoda H. Relief of resistance of cement of full cast crowns. J Prosth Dent 14: 95-106, 1964.
– reference: 19) 脇博泰. 村上繁樹, 内田康也ほか. 仮着用ならびに合着用セメントの被膜厚さに関する研究. 九州歯会誌40: 1143-1150, 1986.
– reference: 11) Wiskott HWA, Belser UC, Scherrer SS. The effect of film thickness and surface texture on the resistance of cemented extracoronal restorations to lateral fatigue loading. Int J Prosthodont 12: 255-262, 1999.
– reference: 10) 畑村又好, 奥野忠一, 津村善郎訳. スネデカー, コクラン統計的方法原書第6版394-416, 東京: 岩波書店, 1979.
– reference: 23) Kay GW, Jablonski DA, Dogon IL. Factors affecting the seating and fit of complete crowns: A computer simulation study. J Prosthet Dent 55: 13-18, 1986.
– reference: 15) 川上道夫. 第2版新歯科材料・器械98-105, 東京: 医歯薬出版, 1994.
– reference: 27) 笠原紳, 木村幸平, Takagi sほか. 生体親和性セメントCPCの硬化時粘度に与える各種添加物の影響. 歯産学誌11: 23-30, 1997.
– reference: 6) 本村和義, 大谷宏, 細田裕康. リン酸セメントの被膜厚さと軟度との相関関係. 歯材器誌9: 43-50, 1963.
– reference: 13) 畠山憲子, 笠原紳, 安藤正明ほか. 接着性レジンセメントの諸性質第二報せん断強度, 疲労強度, 吸水量, 溶解量について. 東北大歯誌19: 64-75, 2000.
– reference: 12) 畠山憲子, 笠原紳, 安藤正明ほか. 接着性レジンセメントの諸性質第一報機械的強度について. 東北大歯誌18: 166-174, 1999.
– reference: 2) 吉田恵夫, 佐藤弘, 鹿沼晶夫ほか. セメント合着による鋳造冠の浮き上りについて第1報金属原型使用の場合.補綴誌4: 157-161, 1960.
– reference: 18) 塩沢育己. セメント合着による全部鋳造冠の三次元的変位に関する研究. 補綴誌23: 86-102, 1979.
– reference: 7) Vermilyea S, Powers JM, Craig RG. Rotation viscometry of a zinc phosphate and a zinc polyacrylate cement. J Dent Res 56: 762-767, 1977.
– reference: 9) Windeler AS. The use of film thickness to measure working time of zinc phosphate cements. J Dent Res 57: 697-701, 1978.
– reference: 14) 長谷川二郎, 平沢忠, 高橋重雄編. 現代歯科理工学200-218, 東京: 医歯薬出版, 1996.
– reference: 4) 木村幸平, 志村俊晴, 小野寺勉ほか. グラスアイオノマーセメント合着による鋳造冠の浮き上がりについて. 補綴誌25: 304-310, 1981.
– reference: 1) 日本歯科材料工業協同組合. JDMA Guide Book 352-382, 東京: 日本規格協会, 1997.
– reference: 8) 竹内正巳. リン酸亜鉛セメントの硬化過程における粘性挙動. 歯理工誌19: 279-289, 1978.
– reference: 20) 脇博泰. 仮着用ならびに合着用セメントの浮き上がりに関する実験的研究. 九州歯会誌42: 377-391, 1988.
– reference: 26) 笠原紳, 木村幸平, 齋藤裕太ほか. 生体親和性セメントCPC (calcium phosphate cement) の硬化に与える各種添加物の影響. 東北大歯誌16: 54-61, 1997.
– reference: 16) 中川鶴太郎. レオロジー第2版76-86, 東京: 岩波書店, 1978.
– reference: 25) 本永三千雄, 石橋実, 笠原紳ほか. 全部陶材冠の3次元有限要素法を用いた応力解析-境界の連続性を考慮した解析-.補綴誌43: 791-795, 1999.
– reference: 5) Jørgensen KD. Factors affecting the film thickness of zinc phosphate cements. Acta Odontol Scand 18: 479-490, 1960.
– reference: 22) 西村文夫, 宮治俊幸, 野本直. セメント膜厚への振動の影響. 歯材器誌23: 29-34, 1970.
– reference: 17) Jørgensen KD. Structure of the film of zinc phosphate cements. Acta Odontol Scand 18: 491-501, 1960.
– reference: 24) 笠原紳, 奥山弥生, 木村幸平ほか. 支台歯形成練習エキスパートシステムの開発QE19: 192-197, 2000.
– reference: 21) Jørgensen KD, Petersen GF. The grain size of zinc phosphate cements. Acta Odontol Scand 21: 255-270, 1963.
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Snippet Purpose: Film thickness of dental luting cement is an important property that influences in success of fixed prosthodontics. Conventionally, it has been...
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SubjectTerms cement
film thickness
particle size distribution
powder
viscosity
Title Relation between Viscosity and Film Thickness of Dental Luting Cements
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