Effect of carbon segregation at prior austenite grain boundary on hydrogen-related crack propagation behavior in 3Mn-0.2C martensitic steels

The present study aimed at strengthening prior austenite grain boundary (PAGB) cohesive energy using carbon segregation and investigated the effect of carbon segregation at PAGB on the microscopic crack propagation behavior of hydrogen-related intergranular fractures in high-strength martensitic ste...

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Published inActa materialia Vol. 280; p. 120288
Main Authors Okada, Kazuho, Shibata, Akinobu, Kimura, Yuuji, Yamaguchi, Masatake, Ebihara, Ken-ichi, Tsuji, Nobuhiro
Format Journal Article
LanguageEnglish
Published Elsevier Ltd 01.11.2024
Subjects
Crack propagation
Grain-boundary segregation
Hydrogen embrittlement
Intergranular failure
Martensitic steel
Intergranular failure
Martensitic steel
Hydrogen embrittlement
Crack propagation
Grain-boundary segregation
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Abstract The present study aimed at strengthening prior austenite grain boundary (PAGB) cohesive energy using carbon segregation and investigated the effect of carbon segregation at PAGB on the microscopic crack propagation behavior of hydrogen-related intergranular fractures in high-strength martensitic steels. At the low hydrogen content (below 0.2 wt. ppm), the fracture initiation toughness (JIC) and tearing modulus (TR), corresponding to crack growth resistance, were significantly improved by carbon segregation. In contrast, JIC and TR did not change by carbon segregation at the high hydrogen content (above 0.5 wt. ppm). Considering the non-linear relationship between the toughness properties and the PAGB cohesive energy, the experimentally evaluated toughness properties (JIC and TR) and the GB cohesive energy previously calculated by first-principles calculations were semi-quantitatively consistent even at the high hydrogen content. The microstructure observation confirmed that the plastic deformation associated with crack propagation, such as the local ductile fracture of uncracked ligaments and the formation of dislocation cell structures / nano-voids, played an important role in the non-linear relationship between the toughness properties and PAGB cohesive energy. [Display omitted]
AbstractList The present study aimed at strengthening prior austenite grain boundary (PAGB) cohesive energy using carbon segregation and investigated the effect of carbon segregation at PAGB on the microscopic crack propagation behavior of hydrogen-related intergranular fractures in high-strength martensitic steels. At the low hydrogen content (below 0.2 wt. ppm), the fracture initiation toughness (JIC) and tearing modulus (TR), corresponding to crack growth resistance, were significantly improved by carbon segregation. In contrast, JIC and TR did not change by carbon segregation at the high hydrogen content (above 0.5 wt. ppm). Considering the non-linear relationship between the toughness properties and the PAGB cohesive energy, the experimentally evaluated toughness properties (JIC and TR) and the GB cohesive energy previously calculated by first-principles calculations were semi-quantitatively consistent even at the high hydrogen content. The microstructure observation confirmed that the plastic deformation associated with crack propagation, such as the local ductile fracture of uncracked ligaments and the formation of dislocation cell structures / nano-voids, played an important role in the non-linear relationship between the toughness properties and PAGB cohesive energy. [Display omitted]
ArticleNumber 120288
Author Ebihara, Ken-ichi
Kimura, Yuuji
Tsuji, Nobuhiro
Okada, Kazuho
Yamaguchi, Masatake
Shibata, Akinobu
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  surname: Tsuji
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  organization: Department of Materials Science and Engineering, Kyoto University, Yoshida- honmachi, Sakyo-ku, Kyoto 606-8501, Japan
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Keywords Intergranular failure
Martensitic steel
Hydrogen embrittlement
Crack propagation
Grain-boundary segregation
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Snippet The present study aimed at strengthening prior austenite grain boundary (PAGB) cohesive energy using carbon segregation and investigated the effect of carbon...
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elsevier
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Publisher
StartPage 120288
SubjectTerms Crack propagation
Grain-boundary segregation
Hydrogen embrittlement
Intergranular failure
Martensitic steel
Title Effect of carbon segregation at prior austenite grain boundary on hydrogen-related crack propagation behavior in 3Mn-0.2C martensitic steels
URI https://dx.doi.org/10.1016/j.actamat.2024.120288
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