Surface Morphology and Hardness Analysis of TiCN Coated AA7075 Aluminium Alloy

Successful titanium carbonitride (TiCN) coating on AA7075 plates using the PVD technique depends upon many variables, including temperature, pressure, incident angle and energy of the reactive ions. Coated specimens have shown an increase in their surface hardness of 2.566 GPa. In this work, an atte...

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Published inJournal of the Institution of Engineers (India) Series C Vol. 100; no. 1; pp. 221 - 228
Main Authors Srinath, M. K., Ganesha Prasad, M. S.
Format Journal Article
LanguageEnglish
Published New Delhi Springer India 08.02.2019
Springer Nature B.V
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Abstract Successful titanium carbonitride (TiCN) coating on AA7075 plates using the PVD technique depends upon many variables, including temperature, pressure, incident angle and energy of the reactive ions. Coated specimens have shown an increase in their surface hardness of 2.566 GPa. In this work, an attempt to further augment the surface hardness and understand its effects on the surface morphology was performed through heat treatments at 500°C for different duration of times. Specimen’s heat treated at 500°C for 1 h exhibited a maximum surface hardness of 6.433 GPa, corresponding to an increase of 92.07%. The XRD results showed the presence of Al 2 Ti and AlTi 3 N and indicate the bond created between them. Unit cell lattice parameters in the XRD data are calculated using Bragg’s law. The SEM images exhibit increasing crack sizes as the heat treatment time is increased. From the studies, the heat treatment duration can be optimized to 1 h, which exhibited an augmented surface hardness, as further increases in durations caused a drop in the surface hardness. The heat treatment effectively modified the surface hardness. Equations providing the relationships that temperature and time have with the reaction parameters are presented.
AbstractList Successful titanium carbonitride (TiCN) coating on AA7075 plates using the PVD technique depends upon many variables, including temperature, pressure, incident angle and energy of the reactive ions. Coated specimens have shown an increase in their surface hardness of 2.566 GPa. In this work, an attempt to further augment the surface hardness and understand its effects on the surface morphology was performed through heat treatments at 500°C for different duration of times. Specimen’s heat treated at 500°C for 1 h exhibited a maximum surface hardness of 6.433 GPa, corresponding to an increase of 92.07%. The XRD results showed the presence of Al 2 Ti and AlTi 3 N and indicate the bond created between them. Unit cell lattice parameters in the XRD data are calculated using Bragg’s law. The SEM images exhibit increasing crack sizes as the heat treatment time is increased. From the studies, the heat treatment duration can be optimized to 1 h, which exhibited an augmented surface hardness, as further increases in durations caused a drop in the surface hardness. The heat treatment effectively modified the surface hardness. Equations providing the relationships that temperature and time have with the reaction parameters are presented.
Successful titanium carbonitride (TiCN) coating on AA7075 plates using the PVD technique depends upon many variables, including temperature, pressure, incident angle and energy of the reactive ions. Coated specimens have shown an increase in their surface hardness of 2.566 GPa. In this work, an attempt to further augment the surface hardness and understand its effects on the surface morphology was performed through heat treatments at 500°C for different duration of times. Specimen’s heat treated at 500°C for 1 h exhibited a maximum surface hardness of 6.433 GPa, corresponding to an increase of 92.07%. The XRD results showed the presence of Al2Ti and AlTi3N and indicate the bond created between them. Unit cell lattice parameters in the XRD data are calculated using Bragg’s law. The SEM images exhibit increasing crack sizes as the heat treatment time is increased. From the studies, the heat treatment duration can be optimized to 1 h, which exhibited an augmented surface hardness, as further increases in durations caused a drop in the surface hardness. The heat treatment effectively modified the surface hardness. Equations providing the relationships that temperature and time have with the reaction parameters are presented.
Author Ganesha Prasad, M. S.
Srinath, M. K.
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Issue 1
Keywords Surface hardness
SEM
XRD
PVD-coatings
TiCN
AA7075
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  contributor:
    fullname: R Figueroa
– volume: 31
  start-page: 329
  year: 2015
  ident: 427_CR18
  publication-title: Surf. Eng.
  doi: 10.1179/1743294414Y.0000000421
  contributor:
    fullname: YB Lin
SSID ssj0001764299
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Snippet Successful titanium carbonitride (TiCN) coating on AA7075 plates using the PVD technique depends upon many variables, including temperature, pressure, incident...
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SubjectTerms Aerospace Technology and Astronautics
Aluminum base alloys
Engineering
Hardness
Heat treating
Heat treatment
Industrial and Production Engineering
Lattice parameters
Mathematical analysis
Mechanical Engineering
Morphology
Original Contribution
Surface hardness
Titanium carbonitride
Unit cell
Title Surface Morphology and Hardness Analysis of TiCN Coated AA7075 Aluminium Alloy
URI https://link.springer.com/article/10.1007/s40032-017-0427-1
https://www.proquest.com/docview/2174786558/abstract/
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