Persulfate coupled with Cu2+/LDH-MoS4: A novel process for the efficient atrazine abatement, mechanism and degradation pathway
[Display omitted] •The slow regeneration of Cu+ restricts the Cu-based catalysts from widespread application.•The electron-rich center of LDH-MoS4 fuel electrons to accelerate the regeneration of Cu+.•The continuous electrons feeding increases the stability of the Cu2+/LDH-MoS4/PS system.•The Cu+ re...
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| Published in | Chemical engineering journal (Lausanne, Switzerland : 1996) Vol. 436; p. 134933 |
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| Main Authors | , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
15.05.2022
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| Subjects | |
| Online Access | Get full text |
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| Abstract | [Display omitted]
•The slow regeneration of Cu+ restricts the Cu-based catalysts from widespread application.•The electron-rich center of LDH-MoS4 fuel electrons to accelerate the regeneration of Cu+.•The continuous electrons feeding increases the stability of the Cu2+/LDH-MoS4/PS system.•The Cu+ regeneration enhances both the catalyst activity and PS utilization efficiency.
The Cu-based catalytic activation of persulfate is considered very attractive to deal with the growing concern of water pollution. However, the difficulty in regenerating Cu+ from Cu2+ restricts it from widespread field applications. This work described the regeneration of Cu+ with the help of layered double hydroxide (LDH-MoS4), being used as a co-catalyst in the Cu2+/persulfate process. The results revealed that the Cu2+/LDH-MoS4/persulfate (PS) system offered better efficiency (30 times) than the normal Cu2+/PS process. Also, the Cu2+/LDH-MoS4/PS system demonstrated faster removal of atrazine (10–20 times) than the recently reported Cu2+/WS2/PS, Cu2+/MoS2/PS or Cu2+/Mo/PS co-catalytic systems or other tested systems, i.e., Cu2+/LDH-BH4/PS, Cu2+/LDH-EDTA/PS etc. This excellent performance of the Cu2+/LDH-MoS4/PS system was related to the constant regeneration of Cu+ from the reduction of Cu2+ ions, which minimizes the effect of the rate-limiting step during reactions. Furthermore, the Cu2+/LDH-MoS4/PS system exhibited good efficiency over a wide pH range (3.0–9.0), high oxidant utilization efficiency, excellent activities during recycling, less susceptibility in the presence of certain electrolytes or organic matters. This study provides the co-catalysts intrinsic role in reducing the Cu2+ ions by continuously feeding electrons from the unsaturated S2− and Mo4+ of LDH-MoS4. |
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| AbstractList | [Display omitted]
•The slow regeneration of Cu+ restricts the Cu-based catalysts from widespread application.•The electron-rich center of LDH-MoS4 fuel electrons to accelerate the regeneration of Cu+.•The continuous electrons feeding increases the stability of the Cu2+/LDH-MoS4/PS system.•The Cu+ regeneration enhances both the catalyst activity and PS utilization efficiency.
The Cu-based catalytic activation of persulfate is considered very attractive to deal with the growing concern of water pollution. However, the difficulty in regenerating Cu+ from Cu2+ restricts it from widespread field applications. This work described the regeneration of Cu+ with the help of layered double hydroxide (LDH-MoS4), being used as a co-catalyst in the Cu2+/persulfate process. The results revealed that the Cu2+/LDH-MoS4/persulfate (PS) system offered better efficiency (30 times) than the normal Cu2+/PS process. Also, the Cu2+/LDH-MoS4/PS system demonstrated faster removal of atrazine (10–20 times) than the recently reported Cu2+/WS2/PS, Cu2+/MoS2/PS or Cu2+/Mo/PS co-catalytic systems or other tested systems, i.e., Cu2+/LDH-BH4/PS, Cu2+/LDH-EDTA/PS etc. This excellent performance of the Cu2+/LDH-MoS4/PS system was related to the constant regeneration of Cu+ from the reduction of Cu2+ ions, which minimizes the effect of the rate-limiting step during reactions. Furthermore, the Cu2+/LDH-MoS4/PS system exhibited good efficiency over a wide pH range (3.0–9.0), high oxidant utilization efficiency, excellent activities during recycling, less susceptibility in the presence of certain electrolytes or organic matters. This study provides the co-catalysts intrinsic role in reducing the Cu2+ ions by continuously feeding electrons from the unsaturated S2− and Mo4+ of LDH-MoS4. |
| ArticleNumber | 134933 |
| Author | Nie, Hui Li, Dan Xiao, Haoliang Chen, Zhuqi Shahzad, Ajmal Wang, Songlin Ali, Jawad Abdelnasser Gendy, Eman Jiang, Wang |
| Author_xml | – sequence: 1 givenname: Dan surname: Li fullname: Li, Dan organization: School of Environmental Science and Engineering, Hubei Provincial Engineering Research Center for Water Quality Safety and Pollution Control, Key Laboratory of Water & Wastewater Treatment (MOHURD), Huazhong University of Science and Technology, Wuhan 430074, China – sequence: 2 givenname: Jawad surname: Ali fullname: Ali, Jawad organization: School of Environmental Science and Engineering, Hubei Provincial Engineering Research Center for Water Quality Safety and Pollution Control, Key Laboratory of Water & Wastewater Treatment (MOHURD), Huazhong University of Science and Technology, Wuhan 430074, China – sequence: 3 givenname: Ajmal surname: Shahzad fullname: Shahzad, Ajmal organization: School of Environmental Science and Engineering, Hubei Provincial Engineering Research Center for Water Quality Safety and Pollution Control, Key Laboratory of Water & Wastewater Treatment (MOHURD), Huazhong University of Science and Technology, Wuhan 430074, China – sequence: 4 givenname: Eman surname: Abdelnasser Gendy fullname: Abdelnasser Gendy, Eman organization: Key Laboratory of Material Chemistry for Energy Conversion and Storage, Ministry of Education, Hubei Key Laboratory of Material Chemistry and Service Failure, School of Chemistry and Chemical Engineering, Huazhong University of Science and Technology, Wuhan 430074, China – sequence: 5 givenname: Hui surname: Nie fullname: Nie, Hui organization: School of Environmental Science and Engineering, Hubei Provincial Engineering Research Center for Water Quality Safety and Pollution Control, Key Laboratory of Water & Wastewater Treatment (MOHURD), Huazhong University of Science and Technology, Wuhan 430074, China – sequence: 6 givenname: Wang surname: Jiang fullname: Jiang, Wang organization: Key Laboratory of Material Chemistry for Energy Conversion and Storage, Ministry of Education, Hubei Key Laboratory of Material Chemistry and Service Failure, School of Chemistry and Chemical Engineering, Huazhong University of Science and Technology, Wuhan 430074, China – sequence: 7 givenname: Haoliang surname: Xiao fullname: Xiao, Haoliang organization: School of Environmental Science and Engineering, Hubei Provincial Engineering Research Center for Water Quality Safety and Pollution Control, Key Laboratory of Water & Wastewater Treatment (MOHURD), Huazhong University of Science and Technology, Wuhan 430074, China – sequence: 8 givenname: Zhuqi surname: Chen fullname: Chen, Zhuqi email: zqchen@hust.edu.cn organization: Key Laboratory of Material Chemistry for Energy Conversion and Storage, Ministry of Education, Hubei Key Laboratory of Material Chemistry and Service Failure, School of Chemistry and Chemical Engineering, Huazhong University of Science and Technology, Wuhan 430074, China – sequence: 9 givenname: Songlin surname: Wang fullname: Wang, Songlin email: wangsonglin99@hust.edu.cn organization: School of Environmental Science and Engineering, Hubei Provincial Engineering Research Center for Water Quality Safety and Pollution Control, Key Laboratory of Water & Wastewater Treatment (MOHURD), Huazhong University of Science and Technology, Wuhan 430074, China |
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