Synthesis, crystal structure, thermal, photoluminescent and magnetic properties of a new material: Na2[Ni(C2O4)2(H2O)2].6H2O

A new nickel oxalate complex, sodium diaquabis(oxalato)nickelate(II)hexahydrate {Na2 [Ni(C2O4)2(H2O)2]·6H2O} has been prepared by the method of slow evaporation and characterized by X-ray single crystal diffraction, FT-IR, UV–visible spectroscopy, photoluminescence, TG/DTA analysis and magnetic meas...

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Published inJournal of molecular structure Vol. 1178; pp. 155 - 161
Main Authors Narsimhulu, M., Anil Kumar, G., Bhargavi, G., Srinivas, B., Hussain, K.A.
Format Journal Article
LanguageEnglish
Published Elsevier B.V 15.02.2019
Subjects
Inorganic compound
Magnetic measurements
Photoluminescence
Thermal analysis
X-ray crystal structure
Magnetic measurements
X-ray crystal structure
Thermal analysis
Photoluminescence
Inorganic compound
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Abstract A new nickel oxalate complex, sodium diaquabis(oxalato)nickelate(II)hexahydrate {Na2 [Ni(C2O4)2(H2O)2]·6H2O} has been prepared by the method of slow evaporation and characterized by X-ray single crystal diffraction, FT-IR, UV–visible spectroscopy, photoluminescence, TG/DTA analysis and magnetic measurements. The X-ray single crystal analysis shows that the structure of the compound belongs to the triclinic system with P1¯space group and cell parameters of a = 6.7853 (5)Å, b = 6.8579 (5)Å, c = 8.8075 (7)Å, α = 87.252(4)°, β = 67.608(4)°, γ = 88.718(4)°, Z = 1. Within the crystal structure, the nickel atom acquires an octahedral environment with six oxygen atoms of which two are from coordinated water molecules and four are from two oxalate ligands. The UV–visible spectrum shows three absorption bands at 236, 376 and 650 nm in the ultraviolet and visible regions, respectively. The compound exhibits ultraviolet (UV) emission at 350 nm when excited at 320 nm at room temperature. The thermogravimetric studies confirm the existence of both hydrated and coordinated water molecules and thermal stability of the compound is 320 °C. Magnetic measurements reveal the occurrence of strong antiferromagnetic interactions between nickel ions in the structure. [Display omitted] •New compound, sodium diaquabis(oxalato)nickelate(II)hexahydrate has been synthesized and characterized.•X-ray single crystal structure was determined.•Photoluminescence property was investigated.•Exhibits antiferromagnetic ordering at low temperatures.
AbstractList A new nickel oxalate complex, sodium diaquabis(oxalato)nickelate(II)hexahydrate {Na2 [Ni(C2O4)2(H2O)2]·6H2O} has been prepared by the method of slow evaporation and characterized by X-ray single crystal diffraction, FT-IR, UV–visible spectroscopy, photoluminescence, TG/DTA analysis and magnetic measurements. The X-ray single crystal analysis shows that the structure of the compound belongs to the triclinic system with P1¯space group and cell parameters of a = 6.7853 (5)Å, b = 6.8579 (5)Å, c = 8.8075 (7)Å, α = 87.252(4)°, β = 67.608(4)°, γ = 88.718(4)°, Z = 1. Within the crystal structure, the nickel atom acquires an octahedral environment with six oxygen atoms of which two are from coordinated water molecules and four are from two oxalate ligands. The UV–visible spectrum shows three absorption bands at 236, 376 and 650 nm in the ultraviolet and visible regions, respectively. The compound exhibits ultraviolet (UV) emission at 350 nm when excited at 320 nm at room temperature. The thermogravimetric studies confirm the existence of both hydrated and coordinated water molecules and thermal stability of the compound is 320 °C. Magnetic measurements reveal the occurrence of strong antiferromagnetic interactions between nickel ions in the structure. [Display omitted] •New compound, sodium diaquabis(oxalato)nickelate(II)hexahydrate has been synthesized and characterized.•X-ray single crystal structure was determined.•Photoluminescence property was investigated.•Exhibits antiferromagnetic ordering at low temperatures.
Author Srinivas, B.
Hussain, K.A.
Narsimhulu, M.
Anil Kumar, G.
Bhargavi, G.
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CitedBy_id crossref_primary_10_1016_j_cdc_2022_100969
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Keywords Magnetic measurements
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Inorganic compound
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Snippet A new nickel oxalate complex, sodium diaquabis(oxalato)nickelate(II)hexahydrate {Na2 [Ni(C2O4)2(H2O)2]·6H2O} has been prepared by the method of slow...
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StartPage 155
SubjectTerms Inorganic compound
Magnetic measurements
Photoluminescence
Thermal analysis
X-ray crystal structure
Title Synthesis, crystal structure, thermal, photoluminescent and magnetic properties of a new material: Na2[Ni(C2O4)2(H2O)2].6H2O
URI https://dx.doi.org/10.1016/j.molstruc.2018.10.013
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