Hydrothermal synthesis and characterization of calcium phosphate-based coatings on AZ31 magnesium alloy

This study aims to analyze the influence of process parameters used for hydrothermal synthesis of CaP coatings on their properties and to improve their corrosion resistance and biocompatibility compared to the substrat AZ31. The parameters monitored were deposition time, pH of the reaction mixture,...

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Published inKorose a ochrana materiálu Vol. 67; no. 1; pp. 8 - 13
Main Authors Horáková, L., Doskočil, L., Wasserbauer, J., Buchtík, M.
Format Journal Article
LanguageEnglish
Published Prague Sciendo 01.05.2023
De Gruyter Poland
Subjects
Ammonium dihydrogen phosphate
Biocompatibility
Calcium phosphates
Coatings
Corrosion resistance
Deposition
Electrochemical corrosion
Electrode polarization
Electrodes
Magnesium alloys
Magnesium base alloys
Mixtures
Morphology
Precursors
Pressure vessels
Process parameters
Scanning electron microscopy
Synthesis
Transplants & implants
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Abstract This study aims to analyze the influence of process parameters used for hydrothermal synthesis of CaP coatings on their properties and to improve their corrosion resistance and biocompatibility compared to the substrat AZ31. The parameters monitored were deposition time, pH of the reaction mixture, and concentration of precursors in the reaction mixture. For the deposited CaP coatings on AZ31 magnesium alloy, the surface morphology and the number of structural defects were evaluated using scanning electron microscopy. Electrochemical corrosion properties were evaluated using polarization techniques in Hank’s solution. The results showed that the best properties were obtained for the sample prepared in a reaction mixture at 120 °C, pH 5 for a deposition time of 120 min, when the concentration of precursors in the reaction mixture was 0.30 mol/l Ca(NO ·4H O and 0.28 mol/l NH PO . Under these conditions, the best electrochemical corrosion properties were achieved.
AbstractList This study aims to analyze the influence of process parameters used for hydrothermal synthesis of CaP coatings on their properties and to improve their corrosion resistance and biocompatibility compared to the substrat AZ31. The parameters monitored were deposition time, pH of the reaction mixture, and concentration of precursors in the reaction mixture. For the deposited CaP coatings on AZ31 magnesium alloy, the surface morphology and the number of structural defects were evaluated using scanning electron microscopy. Electrochemical corrosion properties were evaluated using polarization techniques in Hank’s solution. The results showed that the best properties were obtained for the sample prepared in a reaction mixture at 120 °C, pH 5 for a deposition time of 120 min, when the concentration of precursors in the reaction mixture was 0.30 mol/l Ca(NO ·4H O and 0.28 mol/l NH PO . Under these conditions, the best electrochemical corrosion properties were achieved.
This study aims to analyze the influence of process parameters used for hydrothermal synthesis of CaP coatings on their properties and to improve their corrosion resistance and biocompatibility compared to the substrat AZ31. The parameters monitored were deposition time, pH of the reaction mixture, and concentration of precursors in the reaction mixture. For the deposited CaP coatings on AZ31 magnesium alloy, the surface morphology and the number of structural defects were evaluated using scanning electron microscopy. Electrochemical corrosion properties were evaluated using polarization techniques in Hank’s solution. The results showed that the best properties were obtained for the sample prepared in a reaction mixture at 120 °C, pH 5 for a deposition time of 120 min, when the concentration of precursors in the reaction mixture was 0.30 mol/l Ca(NO 3 ) 2 ·4H 2 O and 0.28 mol/l NH 4 H 2 PO 4 . Under these conditions, the best electrochemical corrosion properties were achieved.
This study aims to analyze the influence of process parameters used for hydrothermal synthesis of CaP coatings on their properties and to improve their corrosion resistance and biocompatibility compared to the substrat AZ31. The parameters monitored were deposition time, pH of the reaction mixture, and concentration of precursors in the reaction mixture. For the deposited CaP coatings on AZ31 magnesium alloy, the surface morphology and the number of structural defects were evaluated using scanning electron microscopy. Electrochemical corrosion properties were evaluated using polarization techniques in Hank’s solution. The results showed that the best properties were obtained for the sample prepared in a reaction mixture at 120 °C, pH 5 for a deposition time of 120 min, when the concentration of precursors in the reaction mixture was 0.30 mol/l Ca(NO3)2·4H2O and 0.28 mol/l NH4H2PO4. Under these conditions, the best electrochemical corrosion properties were achieved.
Author Wasserbauer, J.
Buchtík, M.
Doskočil, L.
Horáková, L.
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SubjectTerms Ammonium dihydrogen phosphate
Biocompatibility
Calcium phosphates
Coatings
Corrosion resistance
Deposition
Electrochemical corrosion
Electrode polarization
Electrodes
Magnesium alloys
Magnesium base alloys
Mixtures
Morphology
Precursors
Pressure vessels
Process parameters
Scanning electron microscopy
Synthesis
Transplants & implants
Title Hydrothermal synthesis and characterization of calcium phosphate-based coatings on AZ31 magnesium alloy
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Volume 67
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