Photocatalyst-, metal- and additive-free, direct C-H arylation of quinoxalin-2(1H)-ones with aryl acyl peroxides induced by visible light

A visible light-mediated direct C-H arylation of quinoxalin-2(1H)-ones with aryl acyl peroxides has been developed. The reaction proceeds smoothly through a radical process in the absence of photocatalyst, additive and metal catalyst, providing the corresponding products in moderate to good yields....

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Published inORGANIC CHEMISTRY FRONTIERS Vol. 7; no. 24; pp. 4031 - 4042
Main Authors Xu, Jun, Zhang, Hongdou, Zhao, Jianming, Ni, Zhigang, Zhang, Pengfei, Shi, Bing-Feng, Li, Wanmei
Format Journal Article
LanguageEnglish
Published CAMBRIDGE Royal Soc Chemistry 14.12.2020
Royal Society of Chemistry
Subjects
Aromatic compounds
Catalysts
Chemistry
Chemistry, Organic
Organic chemistry
Peroxides
Photocatalysts
Physical Sciences
Science & Technology
POTENT
QUINOXALINONES
DECARBOXYLATIVE ORTHO-ARYLATION
AGENTS
INHIBITORS
AROMATIC-SUBSTITUTION
BENZOYL PEROXIDE
BOND
ASYMMETRIC ALPHA-BENZOYLOXYLATION
PHOTOREDOX CATALYSIS
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Abstract A visible light-mediated direct C-H arylation of quinoxalin-2(1H)-ones with aryl acyl peroxides has been developed. The reaction proceeds smoothly through a radical process in the absence of photocatalyst, additive and metal catalyst, providing the corresponding products in moderate to good yields. This methodology opens a simple and green access to 3-arylquinoxalin-2(1H)-ones.
AbstractList A visible light-mediated direct C–H arylation of quinoxalin-2(1H)-ones with aryl acyl peroxides has been developed. The reaction proceeds smoothly through a radical process in the absence of photocatalyst, additive and metal catalyst, providing the corresponding products in moderate to good yields. This methodology opens a simple and green access to 3-arylquinoxalin-2(1H)-ones.
Author Li, Wanmei
Xu, Jun
Shi, Bing-Feng
Zhao, Jianming
Ni, Zhigang
Zhang, Pengfei
Zhang, Hongdou
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  givenname: Hongdou
  surname: Zhang
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  organization: Hangzhou Normal Univ, Coll Mat Chem & Chem Engn, Hangzhou 311121, Peoples R China
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  orcidid: 0000-0002-0109-3275
  surname: Ni
  fullname: Ni, Zhigang
  organization: Hangzhou Normal Univ, Coll Mat Chem & Chem Engn, Hangzhou 311121, Peoples R China
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  orcidid: 0000-0003-0519-1056
  surname: Zhang
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  organization: Hangzhou Normal Univ, Coll Mat Chem & Chem Engn, Hangzhou 311121, Peoples R China
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  givenname: Bing-Feng
  orcidid: 0000-0003-0375-955X
  surname: Shi
  fullname: Shi, Bing-Feng
  organization: Zhejiang Univ, Dept Chem, Hangzhou 310027, Peoples R China
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  givenname: Wanmei
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  surname: Li
  fullname: Li, Wanmei
  email: liwanmei@hznu.edu.cn
  organization: Hangzhou Normal Univ, Coll Mat Chem & Chem Engn, Hangzhou 311121, Peoples R China
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Keywords POTENT
QUINOXALINONES
DECARBOXYLATIVE ORTHO-ARYLATION
AGENTS
INHIBITORS
AROMATIC-SUBSTITUTION
BENZOYL PEROXIDE
BOND
ASYMMETRIC ALPHA-BENZOYLOXYLATION
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Snippet A visible light-mediated direct C-H arylation of quinoxalin-2(1H)-ones with aryl acyl peroxides has been developed. The reaction proceeds smoothly through a...
A visible light-mediated direct C–H arylation of quinoxalin-2(1H)-ones with aryl acyl peroxides has been developed. The reaction proceeds smoothly through a...
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SubjectTerms Aromatic compounds
Catalysts
Chemistry
Chemistry, Organic
Organic chemistry
Peroxides
Photocatalysts
Physical Sciences
Science & Technology
Title Photocatalyst-, metal- and additive-free, direct C-H arylation of quinoxalin-2(1H)-ones with aryl acyl peroxides induced by visible light
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Volume 7
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