Negative result: Chemical forensic attribution of ricin preparations using fatty acids analysed with gas chromatography-mass spectrometry

Here, samples of castor oil were extracted from Australian Ricinus communis seeds. The extracted oils were esterified and the derivatives characterised by gas chromatography-mass spectrometry (GC–MS). The fatty acid composition of the oils was profiled, enabling the trace fatty acid components of ca...

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Published inForensic Science International. Reports Vol. 2; p. 100127
Main Authors Webster, Renée L., Ovenden, Simon P.B., Yousef, Jumana
Format Journal Article
LanguageEnglish
Published Elsevier B.V 01.12.2020
Elsevier
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Abstract Here, samples of castor oil were extracted from Australian Ricinus communis seeds. The extracted oils were esterified and the derivatives characterised by gas chromatography-mass spectrometry (GC–MS). The fatty acid composition of the oils was profiled, enabling the trace fatty acid components of castor oil to be reported for the first time. The resulting data were also subjected to statistical analysis to test the applicability for provenance and geographic attribution purposes, but no discrimination was found.
AbstractList Here, samples of castor oil were extracted from Australian Ricinus communis seeds. The extracted oils were esterified and the derivatives characterised by gas chromatography-mass spectrometry (GC–MS). The fatty acid composition of the oils was profiled, enabling the trace fatty acid components of castor oil to be reported for the first time. The resulting data were also subjected to statistical analysis to test the applicability for provenance and geographic attribution purposes, but no discrimination was found.
ArticleNumber 100127
Author Yousef, Jumana
Webster, Renée L.
Ovenden, Simon P.B.
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Cites_doi 10.1016/S1044-0305(01)00251-3
10.1021/ac1006206
10.1039/an9871200391
10.1016/j.talanta.2018.03.070
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10.1021/ac051006f
10.1002/pca.2519
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10.1007/BF00000015
10.3390/toxins3101332
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Keywords castor oil
Multivariate analysis
Ricin
Fatty acid methyl esters
Chemical attribution
Language English
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  ident: 10.1016/j.fsir.2020.100127_bib0120
  article-title: Production, chemistry, and commercial applications of various chemicals from castor oil
  publication-title: J. Am. Oil Chem. Soc.
  doi: 10.1007/BF00000015
  contributor:
    fullname: Naughton
– volume: 3
  start-page: 1332
  issue: 10
  year: 2011
  ident: 10.1016/j.fsir.2020.100127_bib0015
  article-title: Ricinus communis intoxications in human and veterinary medicine—a summary of real cases
  publication-title: Toxins
  doi: 10.3390/toxins3101332
  contributor:
    fullname: Worbs
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Snippet Here, samples of castor oil were extracted from Australian Ricinus communis seeds. The extracted oils were esterified and the derivatives characterised by gas...
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SubjectTerms castor oil
Chemical attribution
Fatty acid methyl esters
Multivariate analysis
Ricin
Title Negative result: Chemical forensic attribution of ricin preparations using fatty acids analysed with gas chromatography-mass spectrometry
URI https://dx.doi.org/10.1016/j.fsir.2020.100127
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