Synthesis and Hg2+ removal ability of renewable furfurylamine-derived bio-polythioureas
[Display omitted] •Bio-based polythioureas (BioPTUs) was prepared from renewable furfurylamine.•BioPTUs with high molecular weight were synthesized via catalyst-free strategy.•Properties of bioPTU were tunable by changing the spacer of diamine monomers.•BioPTUs showed excellent absorption ability to...
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| Published in | European polymer journal Vol. 213; p. 113144 |
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| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier Ltd
10.06.2024
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| Subjects | |
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| Abstract | [Display omitted]
•Bio-based polythioureas (BioPTUs) was prepared from renewable furfurylamine.•BioPTUs with high molecular weight were synthesized via catalyst-free strategy.•Properties of bioPTU were tunable by changing the spacer of diamine monomers.•BioPTUs showed excellent absorption ability to Hg2+ ions.
Petroleum-derived polythioureas (PTUs) are typical functional polymers that have been applied as essential materials in the optoelectric and environmental fields. The design and preparation of sustainable PTUs are the current focus in this field. In the present study, we first proposed that PTUs can be prepared from bisfuran diamines by solution polymerisation with CS2 without any catalyst. The diamine monomers were prepared from renewable furfurylamine, which enabled the final PTUs to be sustainable. The highest molecular weight of the resulting PTUs was 86.64 kg/mol, with a polydispersity of 1.32. The glass transition temperature (Tg) of PTU can be tuned by changing the spacer of monomers. All synthesised PTUs showed excellent thermal stability, and the char yield at 800 °C was > 40 %. Attractively, these PTUs are excellent Hg2+ ion capturers due to their thiourea structure. |
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| AbstractList | [Display omitted]
•Bio-based polythioureas (BioPTUs) was prepared from renewable furfurylamine.•BioPTUs with high molecular weight were synthesized via catalyst-free strategy.•Properties of bioPTU were tunable by changing the spacer of diamine monomers.•BioPTUs showed excellent absorption ability to Hg2+ ions.
Petroleum-derived polythioureas (PTUs) are typical functional polymers that have been applied as essential materials in the optoelectric and environmental fields. The design and preparation of sustainable PTUs are the current focus in this field. In the present study, we first proposed that PTUs can be prepared from bisfuran diamines by solution polymerisation with CS2 without any catalyst. The diamine monomers were prepared from renewable furfurylamine, which enabled the final PTUs to be sustainable. The highest molecular weight of the resulting PTUs was 86.64 kg/mol, with a polydispersity of 1.32. The glass transition temperature (Tg) of PTU can be tuned by changing the spacer of monomers. All synthesised PTUs showed excellent thermal stability, and the char yield at 800 °C was > 40 %. Attractively, these PTUs are excellent Hg2+ ion capturers due to their thiourea structure. |
| ArticleNumber | 113144 |
| Author | Fang, Xiu-Qin Liu, Cheng-Mei Shu, Hong-Hui Liu, Yun Han, Sheng-Li Zhang, Hui-Qin |
| Author_xml | – sequence: 1 givenname: Hong-Hui orcidid: 0009-0002-0348-5966 surname: Shu fullname: Shu, Hong-Hui organization: Key Laboratory of Material Chemistry for Energy Conversion and Storage, Ministry of Education, The Innovation and Talent Re-cruitment Base of New Energy Chemistry and Device, Center for Experimental Chemistry, School of Chemistry and Chemical Engineering, Huazhong University of Science and Technology, Wuhan 430074, China – sequence: 2 givenname: Hui-Qin surname: Zhang fullname: Zhang, Hui-Qin organization: Key Laboratory of Material Chemistry for Energy Conversion and Storage, Ministry of Education, The Innovation and Talent Re-cruitment Base of New Energy Chemistry and Device, Center for Experimental Chemistry, School of Chemistry and Chemical Engineering, Huazhong University of Science and Technology, Wuhan 430074, China – sequence: 3 givenname: Sheng-Li surname: Han fullname: Han, Sheng-Li organization: Key Laboratory of Material Chemistry for Energy Conversion and Storage, Ministry of Education, The Innovation and Talent Re-cruitment Base of New Energy Chemistry and Device, Center for Experimental Chemistry, School of Chemistry and Chemical Engineering, Huazhong University of Science and Technology, Wuhan 430074, China – sequence: 4 givenname: Yun surname: Liu fullname: Liu, Yun organization: School of Chemical and Environmental Engineering, Jianghan University, Wuhan 430056, China – sequence: 5 givenname: Xiu-Qin surname: Fang fullname: Fang, Xiu-Qin organization: Key Laboratory of Material Chemistry for Energy Conversion and Storage, Ministry of Education, The Innovation and Talent Re-cruitment Base of New Energy Chemistry and Device, Center for Experimental Chemistry, School of Chemistry and Chemical Engineering, Huazhong University of Science and Technology, Wuhan 430074, China – sequence: 6 givenname: Cheng-Mei surname: Liu fullname: Liu, Cheng-Mei email: liukui@mail.hust.edu.cn organization: Key Laboratory of Material Chemistry for Energy Conversion and Storage, Ministry of Education, The Innovation and Talent Re-cruitment Base of New Energy Chemistry and Device, Center for Experimental Chemistry, School of Chemistry and Chemical Engineering, Huazhong University of Science and Technology, Wuhan 430074, China |
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| Keywords | Catalyst-free polymerisation Furfurylamine Hg (Ⅱ) removal Bio-polythiourea Bisfuranic dimethanamine |
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•Bio-based polythioureas (BioPTUs) was prepared from renewable furfurylamine.•BioPTUs with high molecular weight were synthesized via... |
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| SubjectTerms | Bio-polythiourea Bisfuranic dimethanamine Catalyst-free polymerisation Furfurylamine Hg (Ⅱ) removal |
| Title | Synthesis and Hg2+ removal ability of renewable furfurylamine-derived bio-polythioureas |
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