Metal-free efficient thiolation of C(sp(2)) functionalization via in situ-generated NHTS for the synthesis of novel sulfenylated 2-aminothiazole and imidazothiazole
A direct metal-free approach for the synthesis of novel sulfenylated 2-aminothiazole and imidazothiazole derivatives at room temperature is reported via an in situ-generated electrophilic thiolating agent. The present protocol provides mild and selective access for the insertion of C-S bond function...
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Published in | New journal of chemistry Vol. 45; no. 10; pp. 4632 - 4637 |
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Main Authors | , , , , , , , |
Format | Journal Article |
Language | English |
Published |
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Royal Soc Chemistry
15.03.2021
Royal Society of Chemistry |
Subjects | |
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Abstract | A direct metal-free approach for the synthesis of novel sulfenylated 2-aminothiazole and imidazothiazole derivatives at room temperature is reported via an in situ-generated electrophilic thiolating agent. The present protocol provides mild and selective access for the insertion of C-S bond functionalization with good yield. The mechanistic path was justified via density functional theory (DFT) calculations, which explore the role of the solvent in the reaction mechanism. |
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AbstractList | A direct metal-free approach for the synthesis of novel sulfenylated 2-aminothiazole and imidazothiazole derivatives at room temperature is reported via an in situ-generated electrophilic thiolating agent. The present protocol provides mild and selective access for the insertion of C–S bond functionalization with good yield. The mechanistic path was justified via density functional theory (DFT) calculations, which explore the role of the solvent in the reaction mechanism. A direct metal-free approach for the synthesis of novel sulfenylated 2-aminothiazole and imidazothiazole derivatives at room temperature is reported via an in situ -generated electrophilic thiolating agent. The present protocol provides mild and selective access for the insertion of C–S bond functionalization with good yield. The mechanistic path was justified via density functional theory (DFT) calculations, which explore the role of the solvent in the reaction mechanism. |
Author | Gaikwad, Milind V. Dawane, Bhaskar S. Kamble, Rahul D. Ambhore, Ajay N. Kadam, Shuddhodan N. Wakhradkar, Mahesh G. Gavhane, Priya D. Gunturu, Krishna Chaitanya |
Author_xml | – sequence: 1 givenname: Shuddhodan N. surname: Kadam fullname: Kadam, Shuddhodan N. organization: Vidnyan Mahavidyalay Sangola, Solapur 413307, MS, India – sequence: 2 givenname: Ajay N. surname: Ambhore fullname: Ambhore, Ajay N. organization: Padmabhushan Dr Vasantraodada Patil Mahavidyalay, Tasgaon Sangli 416312, MS, India – sequence: 3 givenname: Rahul D. surname: Kamble fullname: Kamble, Rahul D. organization: Amruteshwar ACS Coll, Vinzar Pune 412213, MS, India – sequence: 4 givenname: Mahesh G. surname: Wakhradkar fullname: Wakhradkar, Mahesh G. organization: Swami Ramanand Teerth Marathwada Univ, Sch Chem Sci, Nanded 431606, MS, India – sequence: 5 givenname: Priya D. surname: Gavhane fullname: Gavhane, Priya D. organization: Swami Ramanand Teerth Marathwada Univ, Sch Chem Sci, Nanded 431606, MS, India – sequence: 6 givenname: Milind V. surname: Gaikwad fullname: Gaikwad, Milind V. organization: Swami Ramanand Teerth Marathwada Univ, Sch Chem Sci, Nanded 431606, MS, India – sequence: 7 givenname: Krishna Chaitanya surname: Gunturu fullname: Gunturu, Krishna Chaitanya email: krishnachaitanya.gunturu@gmail.com organization: Swami Ramanand Teerth Marathwada Univ, Sch Chem Sci, Nanded 431606, MS, India – sequence: 8 givenname: Bhaskar S. orcidid: 0000-0003-2359-9012 surname: Dawane fullname: Dawane, Bhaskar S. email: bhaskardawane@rediffmail.com organization: Swami Ramanand Teerth Marathwada Univ, Sch Chem Sci, Nanded 431606, MS, India |
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Snippet | A direct metal-free approach for the synthesis of novel sulfenylated 2-aminothiazole and imidazothiazole derivatives at room temperature is reported via an in... A direct metal-free approach for the synthesis of novel sulfenylated 2-aminothiazole and imidazothiazole derivatives at room temperature is reported via an in... |
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SubjectTerms | Chemistry Chemistry, Multidisciplinary Density functional theory Physical Sciences Reaction mechanisms Room temperature Science & Technology Synthesis |
Title | Metal-free efficient thiolation of C(sp(2)) functionalization via in situ-generated NHTS for the synthesis of novel sulfenylated 2-aminothiazole and imidazothiazole |
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